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DOE OSTI2018

Tensile and Microstructure Characterization of SNS Target Swirl Bubblers Fabricated by Additive Manufacturing

During operation the mercury facing surfaces of the Spallation Neutron Source target vessel are damaged by cavitation-induced erosion. One option to decrease the erosion damage to the SNS target vessel surfaces is to decrease the intensity of the pressure waves using small bubble mitigation. Injection of small diameter helium bubbles into mercury has been shown in decrease the intensity of proton-induced pressure waves and mitigate erosion damage to mercury/container interface surfaces. Several bubbler designs have been evaluated for implementation in the SNS target. One promising bubbler design is called a swirl bubbler, which is capable of producing a high density of very small diameter helium bubbles in flowing mercury. Due to the complexity of the swirl bubbler design and the geometric restrictions of conventional machining processes, additive manufacturing was considered for fabrication. But there was uncertainty with the mechanical properties of bubblers fabricated with additive manufacturing. A series of experiments were designed to characterize the tensile properties and microstructure of swirl bubblers fabricated using selective laser melting (SLM), both before and after consolidation via hot isostatic pressing (HIPing). This report summarizes the tensile and microstructural characterization of HIPed and non-HIPed swirl bubblers produced via the SLM process. The results show that the as-fabricated material contained appreciable porosity, lack-of-fusion defects, and inconsistent tensile properties with essentially zero ductility. But after a HIPing treatment the microstructure became fully consolidated, and the tensile properties surpassed the requirements specified in the material standard for steel-mill produced 316L plate material used to fabricate the SNS target vessel. While further testing is recommended to evaluate the material’s susceptibility to fatigue fracture, these results indicate 316L bubbler assemblies produced SLM and HIPed are promising candidates for implementation in a future SNS target module.

36 MATERIALS SCIENCE↗

DOE OSTI2018

Explosion Source Models and the Scattering Origin of Regional Phases from SPE Phase 1 Coda Spectral Ratios

The Source Physics Experiment(SPE)explosions provide comprehensive ground truth information,and nearby recordings that are rarely available in typical monitoring scenarios. Here, we look for relationships with local and regional distance data to understand source and propagation effects in an effort to improve monitoring at a distance. We examine source spectral ratios, which can be measured to high precision by taking advantage of many SPE and independently operated stations, as well as the redundancy available from coda waves. Classical source models (Mueller and Murphy, 1971, MM71; Denny and Johnson, 1991, DJ91)predict the source ratios poorly; however, a hybrid model(MM71 with DJ91 cavity radii)performs better, and by varying cavity and elastic radii we obtain models that fit to within measurement precision. Based on this, the best prediction model for the SPE suite is the hybrid model with cavity radius decreased by 95%, and elastic radius decreased by 75%. This works best for mid-range scaled depths of burial (SPE-1, 2, 3, and 5). We do not guarantee transportability to other geologies,depth and scaled depth ranges. Finally, we observe a distinct spectral modulation at 6-9Hzthat is not predicted by classical models, and is most likely the result of interference of short period surface waves(Rg)with those produced by spallation of near surface layers.The same modulationis observed for compressional (P) and shear(S) waves at distance, indicating the origin of these waves as scattered Rg.The scattering process must be accounted for quantitatively when using distant signals to monitor treaty compliance over broad regions.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

DOE OSTI2019

Extreme Temperature Sample Environment for Materials Research Using Neutron Scattering

Extreme temperatures and non-equilibrium materials are both central to Department of Energy’s (DOE) mission of addressing grand challenges in emerging energy and advanced materials technologies. The goal of this project is to develop and perfect a system for studying materials in extreme and non-equilibrium conditions using neutron scattering. Neutron scattering has many advantages in the study of materials structure including the ability to use isotopic substitution to determine partial structure factors. When used at a pulsed neutron source, the potential for event-based detection can enable a stroboscopic technique to interrogate very short lived metastable states in supercooled liquids. The work performed in this Phase I project included: (i) literature reviews and discussions with beamline scientists to establish key requirements for the instrument, (ii) laboratory-based research at Materials Development, Inc. (MDI) to test design concepts, modify control software and model designs, (iii) feasibility experiments and measurements on a prototype sample at the Spallation Neutron Source, and (iv) analysis of the results and design of the proposed Phase II instrument. The results of the work show that the proposed approach is viable and provides a strong basis for the Phase II instrument design and Phase III commercialization. MDI participated in the DOE Commercialization Assistance Program with the Larta Institute (Larta) to accelerate commercial sales of the instruments. The market research identified a served available market of ~13M including sales to beamlines, university research laboratories, and industrial glass and materials businesses. Over the ca. 10 year product life cycle, MDI expects to sell instruments with a cumulative net present value profit of approximately 5M.

47 OTHER INSTRUMENTATION↗

DOE OSTI2019

Laser Line Scan Characterization of Cavitation-Induced Erosion to SNS Mercury Target Vessels

The mercury-facing surfaces of the Spallation Neutron Source target vessel are damaged during operation by a phenomenon called cavitation-induced erosion. To date, erosion damage has caused leaks to develop in two target modules, which necessitated interruptions in operation to replace the target module. Samples are routinely removed from the beam entrance region of SNS targets after removal from service and analyzed to learn about the damage processes occurring in the targets during operation. A laser line scan system was used to produce point-cloud models of the target samples, which were used to calculate various erosion metrics and characterize the erosion damage to each sample. The scans revealed the maximum depth of erosion and the location where the maximum erosion occurred for each sample. The results quantified and illustrated the difference in erosion patterns between different target designs. Data from the scans also showed the maximum depth of erosion was greatly reduced at all locations examined in the SNS targets operated with gas injection. The data produced by these scans will be used to compare erosion damage to future targets in order to quantify the erosion in targets with different design features and operational histories.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

DOE OSTI2019

Explosion Source Models and the Scattering Origin of Regional Phases from SPE Phase 1 Coda Spectral Ratios: Monitoring Implications –Discrimination and Yield Estimation

The Source Physics Experiment (SPE) explosions provide comprehensive ground truth information, and near-source recordings that are rarely available in typical monitoring scenarios. Here, we analyze these data together with local and regional distance recordings to isolate source and propagation effects, and to potentially improve monitoring at distance. We examine source spectral ratios, which can be measured to high precision by taking advantage of many SPE and independently operated stations, as well as the redundancy available from coda waves. Classical source models (Mueller and Murphy, 1971, MM71; Denny and Johnson, 1991, DJ91) predict the source ratios poorly; however, a hybrid model (MM71 with DJ91 cavity radii) performs better. We observe a distinct spectral modulation at 6-9 Hz that is not predicted by classical models, most likely caused by short period surface waves (Rg) interfering with those produced by spallation of near surface layers. The same modulation is observed for compressional (P) and shear (S) waves at distance, indicating that local and regional phases originate as near-source Rg that is scattered into body waves. The scattering process must be accounted for quantitatively to best use remotely recorded signals to monitor treaty compliance, discriminate event types, and estimate explosion yields over broad regions.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

DOE OSTI2014

Multi-depth Measurement of Fast Neutrons

A spallation based multiplicity detector has been constructed and deployed to the Kimballton Underground Research Facility to measure the cosmogenic fast neutron flux anti-coincident from the initiating muon. Two of the three planned measurements have been completed (~380 and ~600 m.w.e) with sufficient statistics. The third measurement at level 14 (~4450 m.w.e.) is currently being performed. Current results at ~600 m.w.e. compare favourably to the one previous measurement at 550 m.w.e. For neutron energies between 100 and 200 MeV measurements at ~380 m.w.e. produce fluxes between 1e -8 and 7e -9 n/cm 2 /s/MeV and at ~600 m.w.e. measurements produce fluxes between 7e -9 and 1e -11 n/cm 2 /s/MeV.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2019

High-Intensity Linear Accelerator with Ribbon Beam

We propose a solution of the fundamental problem in accelerator physics: significant increase of peak beam power in linear accelerator with conservation of beam brightness. It is of primary importance for operation of existing high-power accelerators (LANSCE, Spallation Neutron Source), for development of the next generation of high-power accelerators for basic scientific research and Accelerator-Driven Systems applications (Transmutation of Waste, Nuclear Reactor-Driver), and national security applications, which are all $1B-class facilities. The concept utilizes acceleration of beam with ribbon geometry instead of traditional circular beam. High value of beam current is reached using large width of the beam. Acceleration and focusing is achieved using alternative-focusing principle, which does not require traditional focusing elements (quadrupoles, solenoids). The concept utilizes advantage of 2D plane geometry which excludes beam distortion along beam width and results in conservation of high-value of beam brightness.

43 PARTICLE ACCELERATORS↗

DOE OSTI2017

Demonstration of High Efficiency Laser-Assisted H - Charge Exchange for Microsecond Duration Beams

Laser-assisted stripping is a novel approach to H - charge exchange that overcomes longstanding limitations associated with the traditional, foil-based method of producing high intensity, time structured beams of protons. This paper reports on the first successful demonstration of the laser stripping technique for microseconds duration beams. The experiment represents a factor of one thousand increase in stripped pulse duration compared with the previous proof-of-principle (POP) demonstration. The central theme of the experiment is the implementation of methods to reduce the required average laser power such that high efficiency stripping can be accomplished for microsecond duration beams using conventional laser technology. The experiment was performed on the Spallation Neutron Source (SNS) 1 GeV H - beam using a 1 MW peak power UV laser, and resulted in ~ 95% stripping efficiency.

43 PARTICLE ACCELERATORS↗

DOE OSTI2019

Yearly report for the period Jan. 2018 – Jan. 2019 IC Project: w17_unedetection - “Simulation of underground nuclear explosions using the combined finite discrete element method” and “Fracture Formation and Permeability Evolution at in situ Pressure, Temperature and Stress Conditions”

Understanding the underlying physical processes associated with an underground nuclear explosion (UNE) can help with detection and identification of a suspected event. The Underground Nuclear Explosion Signatures Experiment (UNESE) is a collaborative effort between national laboratories aimed towards improving our understanding of physical and radiochemical signatures associated with a UNE. One primary objective of this effort is to perform hydrodynamic modeling of a UNE, with the purpose of estimating the extent of damage caused by such an event. Estimating the damage associated with an event is important for: a) detection of possible physical signatures at the surface of the earth such as fractures, spallation, and cratering and (b) damage to subsurface structures such as tunnels. Additionally, the damage produced by the hydrodynamic models play can be used to inform subsurface flow and transport models. The Combined Finite-Discrete Element Method (FDEM), implemented as an in-house code known as HOSS (Hybrid Optimization Software Suite), is used to model the damage associated with a UNE in various geological settings.

42 ENGINEERING↗

DOE OSTI2019

Demonstration and Feasibility Analyses of using the Dual-Purpose Canister Drain Pipe to Support the Filling Process

This report documents experiments that are being used to determine the feasibility of filling dual-purpose canisters (DPCs) using the existing drain pipe. Mercury was identified as a surrogate filler for the initial experiments. Oak Ridge National Laboratory’s Target Test Facility (TTF), which is a full-scale Spallation Neutron Source (SNS) prototypical mercury loop, is being used for the planned pipe experiments using mercury. The pipe experiments were divided into two phases to provide a separate effects approach to the problem and to allow for development of system scalability. The first phase included taking strain measurements in a short length pipe, as well as measurements of flow-induced vibration. The second phase consists of the design and construction of a separated mercury flow loop capable of hosting exchangeable test sections and more localized instrumentation. Data acquisition of Phase I was performed during this reporting time period, and subsequent data reduction and data analysis will be performed in the future.

36 MATERIALS SCIENCE↗

DOE OSTI2016

Novel Materials and Devices for Solid-State Neutron Detection

Neutron sensing is critical in civilian, military, industrial, biological, medical, basic research, and environmental applications. Conventional neutron sensors are limited by size, weight, cost, portability, and helium supply. Here the microfabrication of Gd conversion material-based heterojunction diodes is described for detecting thermal neutrons using electrical signals produced by internal conversion electrons (ICE). Films with negligible stress were produced at the tensile-compressive crossover point, enabling Gd coatings of any desired thickness by controlling the radiofrequency sputtering power and using the zero-point near p(Ar) of 50 mTorr at 100 W. Post-deposition Gd oxidation-induced spallation was eliminated by growing a residual stress-free 50 nm neodymium-doped aluminum cap layer atop Gd. Resultant coatings were stable for at least six years demonstrating excellent product shelf life. Depositing Gd on the diode surface eliminated air gap, leading to improved efficiency and facilitating monolithic microfabrication. The conversion electron spectrum was dominated by ICE with energies of 72, 132, and 174 keV. Results are reported on neutron reflection and moderation by polyethylene for enhanced sensitivity and γ- and X-ray elimination for improved specificity. Optimal Gd thickness was 10.4 μm with 300 μm thick partially depleted diode of 300 mm2 active surface area. Fast detection within 10 minutes at a neutron source-to-diode distance of 11.7 cm was achieved using this configuration. All ICE energies along with γ-ray and Kα X-ray were modeled to emphasize correlations between experiment and theory and to calculate efficiencies. Semiconductor thermal neutron detectors offer advantages for field-sensing of radioactive neutron sources.

47 OTHER INSTRUMENTATION↗

DOE OSTI2016

Verification of the Prompt Radiation Shielding Design of the ESS Accelerator

Fermilab will perform prompt radiation and shielding verification studies for the European Spallation Source ERIC (ESS) accelerator tunnel and existing penetration layouts using the latest information on the beam line and existing models of magnets and cryomodules. The input information about the assumptions, geometry layout, etc. will be provided by the Safety Group (accelerator division, ESS). The MEDT department of the Accelerator Division, Fermilab will provide the results of the studies. MARS15, a Fermilab a multi-purpose Monte-Carlo code developed since 1974, is at the heart of this effort. MARS15 is used for detailed simulation of hadronic and electromagnetic cascades in an arbitrary 3-D geometry of shielding, accelerator, detector and spacecraft components with energy ranging from a fraction of an electronvolt to 100 TeV. This work will provide additional validation of recent additions to the physical models in the code, including the code capabilities to simulate cascades and generate a variety of results in complex media.

43 PARTICLE ACCELERATORS↗

DOE OSTI2019

Low RF Power Plasma Ignition and Detection for In-Situ Cleaning of 1.3 GHz 9-Cell Cavities

Superconducting Radio Frequency (SRF) cavities performance preservation is crucial, from vertical test to accelerator operation. Field Emission (FE) is still one of the performance limiting factors to overcome and plasma cleaning has been proven successful by the Spallation Neutron Source (SNS), in cleaning field emitters and increasing the work function of Nb. A collaboration has been established between Fermi National Accelerator Laboratory (FNAL), SLAC National Accelerator Lab- oratory and Oak Ridge National Laboratory (ORNL) with the purpose of applying plasma processing to the Linac Coherent Light Source-II (LCLS-II) cavities, in order to minimize and overcome field emission without affecting the high Q of nitrogen-doped cavities. The cleaning for LCLS-II will follow the same plasma composition adopted at SNS, which allows in-situ processing of cavities installed in cryomod-ules from hydrocarbon contaminants. A novel method for plasma ignition has been developed at FNAL: a plasma glow discharge is ignited using high order modes to overcome limitations imposed by the fundamental power coupler, allowing in-situ cleaning for cavities in cryomodule. The plasma can be easily ignited and tuned in each of the cavity cells using low RF power. A method for plasma detection has been developed as well, which allows the detection of the plasma location in the cavity without the need of cameras at both cavity ends. The presented method can be applied to other multi-cell cavity designs, even for accelerators where the coupling for the fundamental modes at room temperature is very weak.

43 PARTICLE ACCELERATORS↗

DOE OSTI2019

Analysis of MARS 2018 Data

In this technical note, we present the analysis and results of neutron data collected in 2018 at the Spallation Neutron Source (SNS) by the MARS neutron detector and spectrometer. MARS has been deployed at the SNS "neutrino alley' basement with the purposed of monitoring and characterizing the neutron backgrounds for the COHERENT collaboration. The measured beam neutron rates at the MARS deployment location near some of the COHERENT neutrinos detectors are presented and we discuss what the measured rate and spectra can tell us about the incoming beam neutron flux and energy distribution.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2020

Determination of Stress-Free Lattice Spacing (D₀) for Residual Stress Relaxation Measurement in Ni-based Superalloys by Neutron Diffraction

The residual stress and its relaxation in critical engineering components are key to structural materials reliability. The determination of residual stress in bulk engineering structures like Ni-based superalloys can be conducted by measuring the lattice strain with penetrating neutron diffraction. The state-of-the-art engineering diffraction beamline VULCAN at the Oak Ridge National Laboratory (ORNL) Spallation Neutron Source (SNS) provides the critical capability to evaluate the residual strain/stress relaxation in engineering component thanks to the high flux and event data features. By the means of residual stress/strain calculation, it is critical to accurately determine the stress-free lattice spacing d₀, which can be altered by the change of chemistry, unrelieved stress, and measurement scheme. Here we reported d₀ determination for determining residual stress relaxation and distribution in Alloy 718 superalloys after different quenching treatments. Selection of locations for d₀ measurement was discussed by considering the neutron path, attenuation and sample alignment. A dynamic d₀ that resulted from atom diffusion and chemistry change was estimated as function of time for the in-situ relaxation characterization. It demonstrated how the dynamic d₀ values may influence on the strain calculation in different thermally treated samples. The results highlight the importance of dynamic d₀ for in-situ relaxation involving chemical changes and provide guidance to the dynamic d₀ measurement and simulation.

36 MATERIALS SCIENCE↗

DOE OSTI2020

Thermal Neutron Scattering Evaluation of Yttrium Hydride (FY2020 Progress)

This paper details the thermal neutron scattering measurements of yttrium hydride for various hydrogen concentrations and temperatures that were conducted at the Spallation Neutron Source at Oak Ridge National Laboratory. Measurements at a temperature range of 5 to 1,200 K were conducted to determine the change in inelastic scattering as a function of temperature and to probe for any anharmonic effects known to exist in other metallic hydrides. Additionally, hydrogen concentrations of YH x that range from x = 1.62 to 1.90 were measured to determine the effects of varying hydrogen concentration on the inelastic neutron spectra. Changes in temperature affected the inelastic spectra in unanticipated ways, indicating that there are anharmonic effects, whereas hydrogen concentration does not significantly affect the inelastic spectra. These measurements were compared against the ENDF/B-VIII.0 thermal scattering files of hydrogen in YH 2 and yttrium in YH 2 , as well as a new thermal scattering file created by using the stochastic temperature-dependent effective potential (s-TDEP). Both libraries were found to be in good agreement with the experimental data at lower temperatures. At higher temperatures, the s-TDEP method is better at predicting the experimentally observed softening of phonon modes in acoustic and optical regions.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

DOE OSTI2020

Status Report on Development of a Cask to Enable Pulsed Neutron Characterization of Irradiated Fuel

We present the design of a shielding cask that allows pulsed neutron characterization of irradiated fuel rodlets prior to their destructive examination in hot cells. The goal is to provide complementary and informative measurements that will inform subsequent hot cell PIE examinations by identifying typical and atypical regions with respect to microstructure, tomographic data, or isotope densities. Time-of-flight neutron diffraction has the potential to offer efficient, non-destructive and non-contact microstructural characterization of irradiated fuel pins with spatial resolution of 1 mm3 to 1 cm3 while for energy-resolved neutron imaging (and by extension tomography) a resolution of 100 μm was demonstrated. The potential results include crystallinity vs. amorphous volumes and microstructural information such as phase compositions and textures from the diffraction data as well as distances (e.g. pellet to cladding), cracks, and isotopic distributions of minor actinides, fission products as well as fission gas partial pressures e.g. in the plenum from energy resolved neutron imaging. The capability will identify regions of atypical behavior and provide cost effective bulk characterization of entire samples prior to destructive evaluation in hot cells. This effort is a collaboration between LANL, INL, ORNL, and UC Berkeley. A key facet of the initiative is the ability to cost effectively ship irradiated fuels from INL to the pulsed spallation neutron source at LANSCE. The irradiated fuel would be loaded in the custom designed cask (designated RaMHaM) at INL hot cells which then could be shipped in a BRR Type B shipment container between INL and LANL. No hot cell is required after the loading of the sample at INL in the pathway laid out in this report, greatly simplifying handling at LANL.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

DOE OSTI2020

Natural Resources Assessment for the SNS Second Target Station, Oak Ridge, Tennessee

The US Department of Energy’s Oak Ridge National Laboratory (ORNL) is a leading institution in advanced materials, supercomputing, neutrons, and nuclear science. As a research laboratory managed by UT-Battelle, LLC for DOE, ORNL has national priorities in energy, security, and scientific discovery that necessitate facility improvements and expansions. DOE is also committed to environmental stewardship. The laboratory is located on the ~32,000-acre Oak Ridge Reservation (ORR), much of which is categorized as a National Environmental Research Park and a state Wildlife Management Area. DOE works with the Tennessee Wildlife Resources Agency (TWRA), Tennessee Department of Environment and Conservation (TDEC), US Fish and Wildlife Service (USFWS), US Department of Agriculture, and other agencies to serve as an effective steward of the ORR. Accordingly, project managers must conform to environmental regulations, agreements, and policies at the federal, state, and institutional levels. Per 40 CFR (Code of Federal Regulations) 1508.14, potential effects on research and science education on the National Environmental Research Park represent potential impacts of federal actions. Moreover, federal actions that affect the quantity and quality of hunting opportunities and deer reduction harvest on the Oak Ridge Wildlife Management Area must be considered whenever other aspects of the human environment (as defined by NEPA) are affected. The Spallation Neutron Source (SNS) is a premiere facility at ORNL that provides advanced capabilities in neutron scattering to promote new discoveries and research opportunities in material sciences, physics, chemistry, biological sciences, and others. A conceptual design for a Second Target Station (STS) has been in consideration for several years. The STS is intended to complement and enhance existing ORNL capabilities, notably research and exploration of complex materials. The proposed STS will involve development of existing natural areas on the ORR, which might contain sensitive resources that require mitigation or avoidance in accordance with existing policies and regulation. This report summarizes current knowledge of natural and cultural resources within the STS project area. At the time of this report, the proposed STS project consisted of an operations area comprising 55.4 acres (22.4 ha) and a total review area for potential construction comprising ~224 acres (90.6 ha). The review area is located primarily within forested natural areas of the ORR with minor development in the form of power-line rights-of-way and secondary/graveled roads (Figure 1). The primary goal was to evaluate potential effects on sensitive resources that might result from development of the STS. In addition to onthe-ground surveys during summer 2009 and fall 2019 to summer 2020 by ORNL Natural Resources Management Program and Aquatic Ecology Group staff, this report makes use of historical (pre-1995) and contemporary (1995 to present) data from additional confirmed sources (e.g., TDEC). Likewise, forest conditions were compiled primarily from a 2013 forest inventory effort for Forest Management Compartment 17 and supplemented with limited ground observations in 2019. The individuals who obtained and compiled the data that are presented here are familiar with and routinely assess sensitive resources on the ORR.

54 ENVIRONMENTAL SCIENCES↗