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At least 1,045 records · Page 58

Optimized Microwave Digestion and Quantification Procedure for Boron Carbide samples

A microwave-assisted HNO3-H2SO4-HF digestion system was explored/optimized for the total dissolution of Boron Carbide samples followed by multi-elemental determination using ICP-MS and ICP OES, in order to improve the methods used in a previous try using a microwave-assisted H2O2-HNO3-HF digestion system. The samples were microwave digested to accomplish complete dissolution needed to perform quantitative analysis of their metal content. Two Boron Carbide samples were provided to us: JM10 and JM11. The Boron Carbide samples were completely dissolved at the end of the optimized microwave digestion procedure that was developed. The digested samples were analyzed for metals mostly by ICP MS; few elements were analyzed by ICP-OES. Microwave digestion reactions were performed in a Titan MPS instrument (Perkin Elmer, USA). Titan MPS instrument is equipped with Temperature and Pressure regulations and controlled by software. Each microwave digestion batch contained the samples of interest along with a reagent blank and one certified standard (1632e) in order to (i) compensate for the contaminations present in the reagents, (ii) ensure that the digestion was complete and (iii) that there was a good recovery of all the constituents. The certified standard used (1632e) was provided with USGS certificates of analysis.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Specification of Radionuclide Classes for MELCOR Molten Salt Reactor Simulations

MELCOR has been used extensively to facilitate virtual investigations into severe nuclear accidents for light-water reactors (LWRs). Non-light water reactors (non-LWRs) render some LWR-centric approaches potentially unsuitable. MELCOR has been instrumental in analyzing source terms for LWRs and has recently expanded its applicability to non-LWRs. To simplify radionuclide (RN) tracking, MELCOR currently groups elements into 17 classes, each containing representative species. This grouping, optimized for LWRs, is not appropriate for non-LWRs due to the different chemistry. This necessitates a reevaluation of radionuclide transport modeling. This report introduces a new class scheme for MELCOR tailored to MSR modeling, expanding the current 17 classes to 32 and are explained in the context of a UF 4 fueled FLiBe carrier MSR. It provides a discussion and justification for the new groupings and outlines a methodology for discovering and defining additional classes in MELCOR using a sample calculated RN inventory and a Gibbs energy minimizer (GEM).

22 GENERAL STUDIES OF NUCLEAR REACTORS↗

Vapor compression distillation module

A Vapor Compression Distillation (VCD) module was developed and evaluated as part of a Space Station Prototype (SSP) environmental control and life support system. The VCD module includes the waste tankage, pumps, post-treatment cells, automatic controls and fault detection instrumentation. Development problems were encountered with two components: the liquid pumps, and the waste tank and quantity gauge. Peristaltic pumps were selected instead of gear pumps, and a sub-program of materials and design optimization was undertaken leading to a projected life greater than 10,000 hours of continuous operation. A bladder tank was designed and built to contain the waste liquids and deliver it to the processor. A detrimental pressure pattern imposed upon the bladder by a force-operated quantity gauge was corrected by rearranging the force application, and design goals were achieved. System testing has demonstrated that all performance goals have been fulfilled.

Nuccio, P. P.↗

Development of high reliability, high frequency power conditioning models of converter regulators

High efficiency conversion, regulation, and filtering techniques are discussed for power using high conversion frequencies; i.e., in the order of 1 to 5 MHz for converters having total output power capability in the order of 20 watts and 200 to 500 KHz for converters having total output powers in excess of 200 watts. Work centered on areas of component selection, material selection, optimization of the various types of circuits required, and the selection of materials for and design of magnetic components. These techniques were then applied to the design of two sample converters, one a medium power instrument type converter and the second a high power converter representative of a primary spacecraft converter regulator. The configuration and performance of the two converters is reported and discussed.

Rochussen, A. W.↗

Research pressure instrumentation for NASA Space Shuttle main engine, modification no. 5

Research concerning the development of pressure instrumentation for the space shuttle main engine is reported. The following specific topics were addressed: (1) transducer design and materials, (2) silicon piezoresistor characterization at cryogenic temperatures, (3) chip mounting characterization, and (4) frequency response optimization.

Anderson, P. J.↗

Technology development program for the Space Infrared Telescope Facility (SIRTF) science instruments

A coordinated technology program for the Space Infrared Telescope Facility (SIRTF) is described. The program encompasses detector technology, cryogenic mechanisms technology, and an adiabatic demagnetization refrigerator. Discrete detectors, detector arrays, detector readouts, and testing of engineering models under simulated flight environment conditions are considered. Several focal planes will be optimized at a particular wavelength range to make up over 247,000 detector pixels from about 1.8 to 1000 microns.

Ramos, Ruben↗

Compact drilling and sample system

The Compact Drilling and Sample System (CDSS) was developed to drill into terrestrial, cometary, and asteroid material in a cryogenic, vacuum environment in order to acquire subsurface samples. Although drills were used by the Apollo astronauts some 20 years ago, this drill is a fraction of the mass and power and operates completely autonomously, able to drill, acquire, transport, dock, and release sample containers in science instruments. The CDSS has incorporated into its control system the ability to gather science data about the material being drilled by measuring drilling rate per force applied and torque. This drill will be able to optimize rotation and thrust in order to achieve the highest drilling rate possible in any given sample. The drill can be commanded to drill at a specified force, so that force imparted on the rover or lander is limited. This paper will discuss the cryo dc brush motors, carbide gears, cryogenic lubrication, quick-release interchangeable sampling drill bits, percussion drilling and the control system developed to achieve autonomous, cryogenic, vacuum, lightweight drilling.

Gillis-Smith, Greg R.↗

Development of a Sunspot Tracking System

Large solar flares produce a significant amount of energetic particles which pose a hazard for human activity in space. In the hope of understanding flare mechanisms and thus better predicting solar flares, NASA's Marshall Space Flight Center (MSFC) developed an experimental vector magnetograph (EXVM) polarimeter to measure the Sun's magnetic field. The EXVM will be used to perform ground-based solar observations and will provide a proof of concept for the design of a similar instrument for the Japanese Solar-B space mission. The EXVM typically operates for a period of several minutes. During this time there is image motion due to atmospheric fluctuation and telescope wind loading. To optimize the EXVM performance an image motion compensation device (sunspot tracker) is needed. The sunspot tracker consists of two parts, an image motion determination system and an image deflection system. For image motion determination a CCD or CID camera is used to digitize an image, than an algorithm is applied to determine the motion. This motion or error signal is sent to the image deflection system which moves the image back to its original location. Both of these systems are under development. Two algorithms are available for sunspot tracking which require the use of only one row and one column of image data. To implement these algorithms, two identical independent systems are being developed, one system for each axis of motion. Two CID cameras have been purchased; the data from each camera will be used to determine image motion for each direction. The error signal generated by the tracking algorithm will be sent to an image deflection system consisting of an actuator and a mirror constrained to move about one axis. Magnetostrictive actuators were chosen to move the mirror over piezoelectrics due to their larger driving force and larger range of motion. The actuator and mirror mounts are currently under development.

Taylor, Jaime R.↗

Robotic Recon for Human Exploration

Robotic reconnaissance has the potential to significantly improve scientific and technical return from lunar surface exploration. In particular, robotic recon may increase crew productivity and reduce operational risk for exploration. However, additional research, development and field-testing is needed to mature robot and ground control systems, refine operational protocols, and specify detailed requirements. When the new lunar surface campaign begins around 2020, and before permanent outposts are established, humans will initially be on the Moon less than 10% of the time. During the 90% of time between crew visits, robots will be available to perform surface operations under ground control. Understanding how robotic systems can best address surface science needs, therefore, becomes a central issue Prior to surface missions, lunar orbiters (LRO, Kaguya, Chandrayyan-1, etc.) will map the Moon. These orbital missions will provide numerous types of maps: visible photography, topographic, mineralogical and geochemical distributions, etc. However, remote sensing data will not be of sufficient resolution, lighting, nor view angle, to fully optimize pre-human exploration planning, e.g., crew traverses for field geology and geophysics. Thus, it is important to acquire supplemental and complementary surface data. Robotic recon can obtain such data, using robot-mounted instruments to scout the surface and subsurface at resolutions and at viewpoints not achievable from orbit. This data can then be used to select locations for detailed field activity and prioritize targets to improve crew productivity. Surface data can also help identify and assess terrain hazards, and evaluate alternate routes to reduce operational risk. Robotic recon could be done months in advance, or be part of a continuing planning process during human missions.

Deans, Matthew↗

Galvanic Liquid Applied Coating Development for Protection of Steel in Concrete

Corrosion of reinforcing steel in concrete is a major problem affecting NASA facilities at Kennedy Space Center (KSC), other government agencies, and the general public. Problems include damage to KSC launch support structures, transportation and marine infrastructures, as well as building structures. A galvanic liquid applied coating was developed at KSC in order to address this problem. The coating is a non-epoxy metal rich ethyl silicate liquid coating. The coating is applied as a liquid from initial stage to final stage. Preliminary data shows that this coating system exceeds the NACE 100 millivolt shift criterion. The remainder of the paper details the development of the coating system through the following phases: Phase I: Development of multiple formulations of the coating to achieve easy application characteristics, predictable galvanic activity, long-term protection, and minimum environmental impact. Phase II: Improvement of the formulations tested in Phase I including optimization of metallic loading as well as incorporation of humectants for continuous activation. Phase III: Application and testing of improved formulations on the test blocks. Phase IV: Incorporation of the final formulation upgrades onto large instrumented structures (slabs).

Curran, Joseph John↗

Dose Calibration of the ISS-RAD Fast Neutron Detector

The ISS-RAD instrument has been fabricated by Southwest Research Institute and delivered to NASA for flight to the ISS in late 2015 or early 2016. ISS-RAD is essentially two instruments that share a common interface to ISS. The two instruments are the Charged Particle Detector (CPD), which is very similar to the MSL-RAD detector on Mars, and the Fast Neutron Detector (FND), which is a boron-loaded plastic scintillator with readout optimized for the 0.5 to 10 MeV energy range. As the FND is completely new, it has been necessary to develop methodology to allow it to be used to measure the neutron dose and dose equivalent. This talk will focus on the methods developed and their implementation using calibration data obtained in quasi-monoenergetic (QMN) neutron fields at the PTB facility in Braunschweig, Germany. The QMN data allow us to determine an approximate response function, from which we estimate dose and dose equivalent contributions per detected neutron as a function of the pulse height. We refer to these as the "pSv per count" curves for dose equivalent and the "pGy per count" curves for dose. The FND is required to provide a dose equivalent measurement with an accuracy of 10% of the known value in a calibrated AmBe field. Four variants of the analysis method were developed, corresponding to two different approximations of the pSv per count curve, and two different implementations, one for real-time analysis onboard ISS and one for ground analysis. We will show that the preferred method, when applied in either real-time or ground analysis, yields good accuracy for the AmBe field. We find that the real-time algorithm is more susceptible to chance-coincidence background than is the algorithm used in ground analysis, so that the best estimates will come from the latter.

Zeitlin, C.↗

Electric Field Conjugation in the Presence of Model Uncertainty

The Wide-Field Infrared Survey Telescope (WFIRST) is a 2.4-meter-diameter space telescope NASA program. The payload will include a coronagraph instrument (CGI). The CGI designs under development use deformable mirrors (DM) to create a point spread function (PSF) with a dark region around the obscured star object. Electric field conjugation (EFC) is an iterative nonlinear optimization procedure that uses measurements of the electric field at the image to determine the DM displacements to modify the PSF to create the region of high contrast in the image. EFC requires a numerical model of the coronagraph to calculate the Jacobian of the system, which is used, along with regularization, to solve for the DM displacements for each iteration of the nonlinear optimization. Ideally, the coronagraph is aligned and calibrated, and the calibration data are used in the numerical model for calculating the Jacobian. However, calibration and alignment measurements always contain uncertainty resulting in calibration error. Therefore, the Jacobian calculated from the numerical model is not an exact representation of the physical coronagraph, and the resulting DM solution for an EFC iteration does not have the exact impact on the electric field of the coronagraph as predicted by the EFC. The result is slow convergence, and, as will be shown, drives the use of more restrictive regularization. Using Monte Carlo trials, we investigate the effect of calibration error on EFC convergence and regulatization. Comparison to results from the High Contrast Imaging Testbed Hybrid Lyot Coronagraph are also presented.

Marx, David↗

Leveraging Optimal Sparse Sensor Placement to Aggregate a Network of Digital Twins for Nuclear Subsystems

Nuclear power plants (NPPs) require continuous monitoring of various systems, structures, and components to ensure safe and efficient operations. The critical safety testing of new fuel compositions and the analysis of the effects of power transients on core temperatures can be achieved through modeling and simulations. They capture the dynamics of the physical phenomenon associated with failure modes and facilitate the creation of digital twins (DTs). Accurate reconstruction of fields of interest (e.g., temperature, pressure, velocity) from sensor measurements is crucial to establish a two-way communication between physical experiments and models. Sensor placement is highly constrained in most nuclear subsystems due to challenging operating conditions and inherent spatial limitations. This study develops optimized data-driven sensor placements for full-field reconstruction within reactor and steam generator subsystems of NPPs. Optimized constrained sensors reconstruct field of interest within a tri-structural isotropic (TRISO) fuel irradiation experiment, a lumped parameter model of a nuclear fuel test rod and a steam generator. The optimization procedure leverages reduced-order models of flow physics to provide a highly accurate full-field reconstruction of responses of interest, noise-induced uncertainty quantification and physically feasible sensor locations. Accurate sensor-based reconstructions establish a foundation for the digital twinning of subsystems, culminating in a comprehensive DT aggregate of an NPP.

42 ENGINEERING↗

MARIE Dose and Flux Measurements in Mars Orbit

We present results from the Martian Radiation Environment Experiment (MARIE), aboard the 2001 Mars Odyssey spacecraft in orbit around Mars. MARIE operated successfully from March 2002 through October 2003. At the time of this writing, the instrument is off due to a loss of communications during an extremely intense Solar Particle Event. Efforts to revive MARIE are planned for Spring 2004, when Odyssey's role as a communications relay for the MER rovers is completed. During the period of successful operation, MARIE returned the first detailed energetic charged particle data from Mars. Due to limitations of the instrument, normalizing MARIE data to flux or dose is not straightforward - several large corrections are needed. Thus normalized results (like dose or flux) have large uncertainties and/or significant model-dependence. The problems in normalization are mainly due to inefficiency in detecting high-energy protons (signal-to-noise problems force the trigger threshold to be higher than optimal), to the excessively high gains employed in the signal processing electronics (many ions deposit energy sufficient to saturate the electronics, and dE/dx information is lost), and to artifacts associated with the two trigger detectors (incomplete registration of dE/dx). Despite these problems, MARIE is efficient for detecting helium ions with kinetic energies above about 30 MeV/nucleon, and for detecting high-energy ions (energies above about 400 MeV/nucleon) with charges from 5 to 10. Fluxes of these heavier ions can be compared to fluxes obtained from the ACE/CRIS instrument, providing at least one area of direct comparison between data obtained at Earth and at Mars; this analysis will be presented as a work in progress. We will also present dose-rate data, with a detailed explanation of the many sources of uncertainty in normalization. The results for both flux and dose will be compared to predictions of the HZETRN model of the GCR.

Zeitlin, C.↗

Development of a fast ion mass spectrometer for space research

An ion mass spectrometer having a cylindrical E bar x B bar analyzer and either a cylindrical or spherical electrostatic analyzer is described. The instrument has two nested channels and a postacceleration between the electrostatic and E bar x B bar analyzers for wide ranges of energy and mass responses. It is noted that the dual-channel construction not only doubles the data acquisition rate but also permits a reversal of the electrostatic field orientation in the inner channel for lighter ions. The outer channel is then optimized for ions of medium to high mass numbers, resulting in increased mass resolution for such heavy ions. When combined with a cylindrical E bar x B bar analyzer, a 90-deg-deflection angle spherical electrostatic analyzer provides an extremely wide viewing angle. The angular distribution of ions can be derived from such geometry if a position-sensitive resistive anode or a detector array is used at the exit aperture. Details on the principles of operation, the instrument design, and calibration are presented.

Hahn, S. F.↗

Design, Manufacturing, and Validation of an Optimized Electric Machine Enabled by 3D Printing

The collaboration between the National Laboratory of the Rockies (NLR) and LaunchPoint Electric Propulsion Solutions, Inc. (LaunchPoint) focuses on manufacturing and additive design of electric machines enabled by DOE’s program for three-dimensional printing (MADE3D) as applied to advanced drivetrains and their impact on turbine capital cost and lifetime energy production. Initial efforts will focus on the rotor structure and rotor core of the drivetrain including the active materials (electrical steel and magnets) and could later expand to the stator. The verification activities will be conducted with an instrumented electric machine and a small dynamometer.

17 WIND ENERGY↗

CIRCLEZ : Reliable photometric redshifts for active galactic nuclei computed solely using photometry from Legacy Survey Imaging for DESI

Photometric redshifts for galaxies hosting an accreting supermassive black hole in their center, known as active galactic nuclei (AGNs), are notoriously challenging. At present, they are most optimally computed via spectral energy distribution (SED) fittings, assuming that deep photometry for many wavelengths is available. However, for AGNs detected from all-sky surveys, the photometry is limited and provided by a range of instruments and studies. This makes the task of homogenizing the data challenging, presenting a dramatic drawback for the millions of AGNs that wide surveys such as SRG/eROSITA are poised to detect. This work aims to compute reliable photometric redshifts for X-ray-detected AGNs using only one dataset that covers a large area: the tenth data release of the Imaging Legacy Survey (LS10) for DESI. LS10 provides deep grizW1-W4 forced photometry within various apertures over the footprint of the eROSITA-DE survey, which avoids issues related to the cross-calibration of surveys. We present the results from CIRCLEZ, a machine-learning algorithm based on a fully connected neural network. CIRCLEZ is built on a training sample of 14 000 X-ray-detected AGNs and utilizes multi-aperture photometry, mapping the light distribution of the sources. The accuracy (σNMAD) and the fraction of outliers (η) reached in a test sample of 2913 AGNs are equal to 0.067 and 11.6%, respectively. The results are comparable to (or even better than) what was previously obtained for the same field, but with much less effort in this instance. We further tested the stability of the results by computing the photometric redshifts for the sources detected in CSC2 and Chandra-COSMOS Legacy, reaching a comparable accuracy as in eFEDS when limiting the magnitude of the counterparts to the depth of LS10. The method can be applied to fainter samples of AGNs using deeper optical data from future surveys (for example, LSST, Euclid), granting LS10-like information on the light distribution beyond the morphological type. Along with this paper, we have released an updated version of the photometric redshifts (including errors and probability distribution functions) for eROSITA/eFEDS.

79 ASTRONOMY AND ASTROPHYSICS↗

Filtered Backprojection in Compton Imaging using a Spherical Harmonic Wiener Filter with Pixelated CdZnTe

Filtered backprojection is an image reconstruction technique for Compton imaging that provides reasonably high resolution at much lower computational costs when compared to iterative methods. Here, this work applies a Wiener filter that has been derived for spherical harmonics on Compton imaging using the OrionUM pixelated CdZnTe imaging-spectrometer. To regularize the filter, an investigation is made into the power spectral density of the signal and noise to develop an appropriate spectral signal-to-noise ratio model for the restoration process. Experimental measurements were conducted with two 228Th sources placed 30° apart. The resulting filtered image of the two sources have an average full-width-at-half-maximum (FWHM) of 9.8° or 7.5° when using a mean squared error and structural similarity optimization approach respectively; an improvement from the 29.0° FWHM image when using simple backprojection.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗