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DOE OSTI2025

Design of a correlation reflectometer radiometer diagnostic and measurements of the electron density–temperature cross-phase angle in the H-mode pedestal with small edge localized modes at ASDEX Upgrade

This work presents the hardware design and first results from a newly commissioned correlation reflectometer radiometer diagnostic that measures the cross-phase angle between electron density and temperature fluctuations in ASDEX Upgrade plasmas. This diagnostic employs cross correlations between signals measured by a tunable, continuous wave, perpendicular incidence, fluctuation reflectometer, and a 24-channel radiometer sharing the same line of sight. Novel measurements in the pedestal of a helium H-mode plasma with small edge localized modes show changes in the cross-phase angle between the electron density and temperature fluctuations from ∼90° to 120°, suggesting changes in the properties of the turbulence driving transport in the plasma edge.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

DOE OSTI2023

Gas-Phase Composition as a Predictive Metric for Calendar Life Behavior of Next-Generation Silicon Anodes

The expansion of renewable technologies and electrification of the transportation sector is driving increased demand for next-generation battery materials that provide higher power and energy density with superior cycling and calendar life stability. Silicon (Si) has a theoretical capacity nearly 10x that of graphite, and is therefore a promising anode material candidate to meet these rigorous performance demands. While leading Si anode battery demonstrations are approaching target metrics for cycle life, a series of complex and interrelated modes of reactivity lead to reduced calendar life and therefore challenge practical adoption of these materials. Deconvoluting the degradation processes that impact Si calendar life is critical to informing the rational and accelerated design of improved Si materials. In the present work, we employ novel sampling techniques and GC-MS-FID characterization to measure gas-phase composition during initial Si cycling, which we tie to selective mechanisms of Si passivation. We utilize a tiered analysis approach to identify and quantify the gas-phase reaction products associated with three advanced Si material candidates under practical operating conditions. Ex situ analysis of Si powders (pure chemical reactivity) is coupled with nondestructive in situ sampling of Si electrodes in a practical pouch-cell format (coupled chemical and electrochemical reactivity). We link the observed gas-phase species evolution to electrochemical behavior and measured calendar life of the three Si materials. Further, we evaluate the voltage-resolved evolution of gas-phase species for one such Si nanomaterial, where nonmonotonic gas generation implies competition between passivating reaction pathways. The measured gas-phase compositional data serves as a critical input for our advanced electrochemical SEI models to identify favorable vs unfavorable reaction pathways to stabilize Si. In addition to bolstering a fundamental understanding of Si reactivity, the present approach informs specific and quantifiable gas-phase metrics tied to calendar life improvements in Si, which can streamline and accelerate the process of next-generation material development.

DIRECT ENERGY CONVERSION,ENERGY STORAGE↗

NASA NTRS2004

Phase Contrast Wavefront Sensing for Adaptive Optics

Most ground-based adaptive optics systems use one of a small number of wavefront sensor technologies, notably (for relatively high-order systems) the Shack-Hartmann sensor, which provides local measurements of the phase slope (first-derivative) at a number of regularly-spaced points across the telescope pupil. The curvature sensor, with response proportional to the second derivative of the phase, is also sometimes used, but has undesirable noise propagation properties during wavefront reconstruction as the number of actuators becomes large. It is interesting to consider the use for astronomical adaptive optics of the "phase contrast" technique, originally developed for microscopy by Zemike to allow convenient viewing of phase objects. In this technique, the wavefront sensor provides a direct measurement of the local value of phase in each sub-aperture of the pupil. This approach has some obvious disadvantages compared to Shack-Hartmann wavefront sensing, but has some less obvious but substantial advantages as well. Here we evaluate the relative merits in a practical ground-based adaptive optics system.

adaptive optics↗

DOE OSTI2022

Magnetic properties of Fe-substituted NiBr 2 single crystals

NiBr 2 is a multiferroic material with an incommensurate magnetic ground state that has easy-plane anisotropy. This manuscript reports how the magnetic properties evolve with Fe substitution in Ni 1-x Fe x Br 2 single crystals for 0 0.17. A particular emphasis is placed on the = 0.055 crystal, for which magnetic phase diagrams were developed on the basis of anisotropic magnetization measurements. The observed phase evolution reveals a phase transition in the x = 0.055 crystal that is not present in NiBr 2 . The data also demonstrate that the easy-plane anisotropy of NiBr is altered by Fe substitution, with a finite easy-axis anisotropy developing at even the low concentration of x = 0.055. Overall, these results demonstrate that Fe substitution enables a fine-tuning of the magnetism in NiBr 2 , especially the magnetic anisotropy, and may therefore promote complex magnetic phases.

36 MATERIALS SCIENCE↗

NASA NTRS1974

Interplanetary navigation using pulsating radio sources

Radio beacons with distinguishing signatures exist in nature as pulsating radio sources (pulsars). These objects radiate well determined pulse trains over hundreds of megahertz of bandwidth at radio frequencies. Since they are at known positions, they can also be used as navigation beacons in interplanetary space. Pulsar signals are weak and dispersive when viewed from earth. If an omnidirectional antenna is connected to a wideband receiver (200 MHz bandwidth centered at 200 MHz) in which dispersion effects are removed, nominal spacecraft position errors of 1500 km can be obtained after 24 h of signal integration. An antenna gain of 10 db would produce errors as low as 150 km. Since the spacecraft position is determined from the measurement of the phase of a periodic signal, ambiguities occur in the position measurement. Simultaneous use of current spacecraft navigation schemes eliminates these ambiguities.

Downs, G. S.↗

NASA NTRS1991

The albedo, effective temperature, and energy balance of Neptune, as determined from Voyager data

Data from the Voyager infrared spectrometer and radiometer (IRIS) investigation are used in determining the albedo, effective temperature, and energy balance of Neptune. From broadband radiometric observations made at phase angles of 14 deg and 134 deg, together with measurements at intermediate phase angles from the literature, an orbital mean value of 0.290 +/-0.067 is obtained for the bolometric Bond albedo. This yields an equilibrium temperature Teq = 46.6 +/-1.1 K. From thermal spectra obtained over latitudes from pole to pole an effective temperature Teff = 59.3 +/-0.8 K is derived. This represents a substantial improvement over previously determined values. The energy balance of Neptune is therefore E = 2.61 +/-0.28, which is in agreement with previous results. The reduced uncertainty in this value is due to the improved determination of the effective temperature.

Pearl, J. C.↗

DOE OSTI2026

Observation of Synchronization between Two Quantum van der Pol Oscillators in Trapped Ions

Synchronization is a hallmark of collective behavior that emerges when nonlinear systems interact, spanning scales from mechanical oscillators to planetary orbits. As a universal phenomenon, it underpins the study of complex systems and has far-reaching technological implications. While classical synchronization has a long and rich history, it has not been observed experimentally between multiple quantum limit-cycle oscillators despite a decade of theoretical investigations. We realize synchronization between two quantum van der Pol oscillators by engineering dissipation in a mixed-isotope trapped-ion quantum simulator. The synchronized state is encoded in a fixed relative phase between the oscillators that is inaccessible to individual measurements and revealed only through joint readout of both oscillators, in stark contrast to the system in the (deterministic) classical limit where synchronization can be observed via individual phase measurements. We further show that the relative phase can be precisely controlled and that the chain of two oscillators can synchronize to an external field, suggesting applications in sensing. Our results provide a promising pathway for studying more complex synchronized quantum dynamics beyond two oscillators, where a theoretical treatment becomes increasingly challenging, and it remains to be understood whether genuinely quantum features persist in such cases.

Liu, Jiarui↗

DOE OSTI2020

Peculiarities of the phase transformation dynamics in bulk FeRh based alloys from magnetic and structural measurements

We analyze coexistence of antiferromagnetic and ferromagnetic phases in bulk iron-rhodium and its alloys with palladium, Fe 50,4 Rh 49,6 , Fe 49,7 Rh 47,4 Pd 2,9 and Fe 48,3 Rh 46,8 Pd 4,9 , using neutron diffraction, magnetization and scanning Hall probe imaging. Temperature dependencies of the lattice parameters, AFM and FM phase weight fractions, and Fe magnetic moment values were obtained on cooling and heating across the AFM-FM transition. Substantial thermomagnetic hysteresis for the phases’ weight fractions and a relatively narrow one for the unit cell volume has been observed on cooling-heating. Furthermore, a clear dependence of hysteretic behavior on Pd concentration has been traced. Additional direct magnetic measurements of the spatial distribution of the phase transition are acquired using scanning Hall probe microscopy, which reveals the length scale of the phase coexistence and the spatial progression of the transition in the presence of external magnetic field. Also, the magnetic phase diagram has been constructed for a series of Pd-doped FeRh alloys.

36 MATERIALS SCIENCE↗

NASA NTRSDate not supplied

Analysis of the Amplitude Response of a Two-Point and a Multi-Point Focused Laser Differential Interferometer

Experiments were performed with two different focused laser differential interferometer (FLDI) instruments to assess the relative amplitude response of each instrument to a traveling shockwave generated by a laser spark in air. The first FLDI instrument generated two slightly-separated measurement points, with each measurement point providing sensitivity to density fluctuations induced by the shockwave. By performing a cross-correlation between the signals obtained from each measurement point, the phase velocity of density fluctuations can be obtained. The second FLDI instrument generated a measurement line that was oriented parallel to the shockwave direction of travel with the resulting interference pattern sampled at multiple equally-spaced points along the line. As a result, this instrument provides density fluctuation measurement capability at multiple points simultaneously. When the measurement line is oriented parallel to the shockwave direction of travel, the phase velocity, rate of change of the phase velocity, and acceleration of density fluctuations traveling along each line can be obtained by performing a cross-correlation between points along the line. Numerical computations of the shockwave generated by the laser spark are used to simulate the response of each instrument and are compared to the experimental results. High-speed schlieren imaging has also been performed and is compared with the FLDI measurements and computational results.

Brett F. Bathel↗

NASA NTRSDate not supplied

Analysis of the Amplitude Response of a Two-Point and a Multi-Point Focused Laser Differential Interferometer

Interferometry↗

DOE OSTI2022

Measurement of shock roughness due to phase plate speckle imprinting relevant for x-ray diffraction experiments on 3rd and 4th generation light sources

Laser-shock compression experiments at 3rd and 4th generation light sources generally employ phase plates, which are inserted into the beamline to achieve a repeatable intensity distribution at the focal plane. Here, the laser intensity profile is characterized by a high-contrast, high-frequency laser speckle. Without sufficient smoothing, these laser non-uniformities can translate to a significant pressure distribution within the sample layer and can affect data interpretation in x-ray diffraction experiments. Here, we use a combination of one- and two-dimensional velocity interferometry to directly measure the extent to which spatial frequencies within the laser focal spot intensity pattern are smoothed out during propagation within the laser plasma and a polyimide ablator. We find that the use of thicker polyimide layers results in spatially smoother shock fronts, with the greatest degree of smoothing associated with the highest spatial frequencies. Focal spots with the smallest initial speckle separation produce the most rapid smoothing. Laser systems that employ smoothing by spectral dispersion techniques to rapidly modulate the focal plane intensity distribution are shown to be the most effective ones in producing a spatially smooth shock front. We show that a simple transport model combined with the known polyimide Hugoniot adequately describes the extent of shock smoothness as a function of polyimide thickness. Finally, our results provide a description of spatial structure smoothing across a shock front, which can be used to design targets on x-ray free electron laser facilities.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

NASA NTRS1977

Fluorine in meteorites

Microanalysis using a resonant nuclear reaction was used to measure F concentrations in USGS standard rocks and 21 meteorites. The F appears to be a moderately depleted element, but there were significant variations within each sample. Measurements on separated metal phases suggest that about 20% of meteoritic F is in the metal or in a phase closely associated with it. Simultaneous measurements of F, Mg, Na, Al and Si in the nonmagnetic fractions of meteorites suggest plagioclase as a F containing phase.

Allen, R. O., Jr.↗

DOE OSTI2024

Dynamics and phases of nonunitary Floquet transverse-field Ising model

Inspired by current research on measurement-induced quantum phase transitions, we analyze the nonunitary Floquet transverse-field Ising model with complex nearest-neighbor couplings and complex transverse fields. Unlike its unitary counterpart, the model shows a number of steady phases, stable to integrability-breaking perturbations. Some phases have robust edge modes and/or spatiotemporal long-range orders in the bulk. The transitions between the phases have extensive entanglement entropy, whose scaling with the system size depends on the number of the real quasiparticle modes in the spectrum at the transition. In particular, the volume-law scaling appears on some critical lines, protected by pseudo-Hermiticity. Both the scaling of entanglement entropy in steady states and the evolution after a quench are compatible with the non-Hermitian generalization of the quasiparticle picture of Calabrese and Cardy at least qualitatively. Published by the American Physical Society 2024

Su, Lei (ORCID:0009000455290786)↗

NASA NTRS1980

Optimization of solar cells for air mass zero operation and study of solar cells at high temperatures, phase 4

The Pd contact to GaAs was studied using backscattering, Auger analysis, and sheet resistance measurements. Several metallurgical phases were present at low temperatures, but PdGa was the dominant phase in samples annealed at 500 C. Ti/Pd/Ag contacts appeared to have the lowest contact resistance. Etchback epitaxy (EBE) was compared to saturated melt epitaxy (SME) method of growing liquid phase epitaxial layers. The SME method resulted in a lower density of Ga microdroplets in the grown layer, although the best solar cells were made by the EBE method. Photoluminescence was developed as a tool for contactless analysis of GaAs cells. Efficiencies of over 8 percent were measured at 250 C.

Hovel, H. J.↗

NASA NTRS2010

High Angular Resolution Observations of Episodic Dust Emission from Long Period Variable Stars Twenty Years of Observations with the Berkeley Infrared Spatial Interferometer

Over the past twenty years the U. C. Berkeley Infrared Spatial Interferometer has observed a number of Long Period Variable stars in the mid-infrared, obtaining information on the spatial distribution of dust around these stars with resolutions of the order of a few tens of milliarcseconds. The ISI is a heterodyne interferometer operating mostly at 11.15 microns, initially with two telescopes. In the last decade, it has been taking data regularly with three telescopes, thus obtaining visibility data on three baselines and also a closure phase. Over the course of the years, the ISI has been able to measure the physical properties of the dust shells surrounding these stars, in particular the inner radii of the dust shells, as well as the temperature and density distribution. For some stars, the ISI has also made precision measurements of their diameters in the mid-infrared. Closure phase measurements have revealed asymmetries in the dust distributions around many stars. Most surprisingly the ISI data has shown evidence for substantial changes in the amount of dust on time scales of 5-10 years, rather than being directly correlated with the stellar pulsation periods, which are of the order of one year. We discuss past results and new results from the ISI that highlight the dynamic environment around these stars.

Danchi, William↗

NASA NTRS1975

Phase correction for a Michelson interferometer with misaligned mirrors

The phase correction for a Michelson interferometer with misaligned mirrors in converging light is shown to give rise to a quadratic phase shift. In general, the calculation of a spectrum from the measured interferogram needs phase correction. Phase corrections have been well worked out for the cases of a linear phase shift and a phase that is slowly varying. The standard procedures for correcting calculated spectra need to be modified, however, to remove any phase errors resulting from misaligned mirrors.

Goorvitch, D.↗

NASA NTRS1988

Mapping of auroral kilometric radiation sources to the aurora

Auroral kilometric radiation (AKR) and optical auroral emissions are observed simultaneously using plasma wave instrumentation and auroral imaging photometers carried on the DE 1 spacecraft. The DE 1 plasma wave instrument measures the relative phase of signals from orthogonal electric dipole antennas, and from these measurements, apparent source directions can be determined with a high degree of precision. Wave data are analyzed for several strong AKR events, and source directions are determined for several emission frequencies. By assuming that the AKR originates at cyclotron resonant altitudes, a candidate source field line is identified. When the selected source field line is traced down to auroral altitudes on the concurrent DE 1 auroral image, a striking correspondece between the AKR source field line and localized auroral features is produced. The magnetic mapping study provides strong evidence that AKR sources occur on field lines associated with discrete auroral arcs, and it provides confirmation that AKR is generated near the electron cyclotron frequency.

Huff, R. L.↗

NASA NTRS1993

Measured space environmental effects to LDEF during retrieval

Data gathered by the Interim Operational Contamination Monitor (IOCM) with regard to the effect of the space environment on the STS-32 Shuttle mission and on the Long Duration Exposure Facility (LDEF) are reported. IOCM measures the deposition of molecular and particulate contamination during all flight phases. It also measures the thermophysical properties of thermal control surfaces by calorimetry, the flux of the ambient atomic oxygen environment, the incident solar flux, and the absolute ambient pressure in the payload bay. The IOCM also provides a structure and sample holders for the exposure of passive material samples to the space environment. One of the more salient results from the STS-32 flight suggests that the LDEF emitted a large number of particulates after berthing into the Shuttle. The mission atomic oxygen fluence was also calculated. Although the fluence was low by normal standards, the Kapton (trademark) passive samples exhibited the onset of erosion. Orbital debris and micrometeoroid impacts also occurred during the retrieval mission. The average perforation diameter was approximately 1.25 micrometers. The largest perforation diameter was measured at 65 micrometers.

Maag, Carl R.↗