Field ionization data using a graphite emitter
Field ionization yield with single graphite whisker lateral surface as ionizer, using helium, ammonia, carbon monoxide and carbon dioxide
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Field ionization yield with single graphite whisker lateral surface as ionizer, using helium, ammonia, carbon monoxide and carbon dioxide
Highly ordered pressure-annealed pyrolytic graphite majority carrier electrons and holes locations in Brillouin zone from measurements in magnetic fields
Crack opening mechanism for high temperature creep of polycrystalline graphite
Graphite fiber resin composites physical and mechanical properties at ambient and cryogenic temperatures, discussing unidirectional ring and bar specimens and filament wound pressure vessels
Graphite ablation under high temperatures for large outer planets entry probes, correlating mass loss rates with surface temperatures and specimen nose cone radii
Graphite properties in high and ultrahigh vacuum, suggesting use as electrode material in vacuum gages and residual gas analyzers
Solid lubricant film consisting of polyimide varnish as binder and graphite fluoride as lubricant is described. Comparative wear tests with other solid lubricants were conducted and results are shown in graph form. Test equipment used in conducting wear tests is reported.
A friction and wear life study was conducted on the use of a polyimide (PI) varnish as a binder for the solid lubricant, graphite fluoride (CF(1.1))N. Also studied were the lubricating properties of PI thin films with no solid lubricant additives. For comparison, similar experiments on PI-bonded MoS2 and burnished films of MoS2 or (CF(li))N were conducted. The best results were obtained with the PI-bonded (CF(1.1))N films. The polyimide thin films (with no solid lubricant additives) did not lubricate well at 25 C; however, when heated to 100 C, low friction and long wear lives were obtained.
A static and buckling analysis of the ATS-F&G spacecraft reflector support truss (RST) and bridge truss assembly using NASTRAN was conducted. The RST is fabricated from a new material, graphite fiber reinforced plastic. A comparison is made with the NASTRAN results and the results of a similar analysis conducted using the stardyne program. The results of an actual static load test are also compared.
It is demonstrated that there are (at least) two sets of minority carriers in graphite, which are essentially the same for both natural single crystals and for pyrolytic samples. Both materials have similar minority carrier de Haas-van Alphen periods as a function of the angle between the C axis and the magnetic field.
Quantum oscillations as a function of magnetic field in the Hall effect and thermoelectric power are studied in two samples of pressure-annealed pyrolytic graphite. Only the oscillations originating from minority-Fermi-surface carriers are discussed. Frequencies of the de Haas-van Alphen type are measured over a wide range of angles between the magnetic field and the c axis of the Brillouin zone. Results are given graphically and analyzed.
Comparison of graphite ablation experiment results in the diffusion-controlled oxidation and sublimation regimes with results of an equilibrium chemistry, film coefficient ablation analysis. Mass transfer and energy transfer effects are considered. Tests were conducted in an arcjet facility at convective heating rates of 600 to 800 W/sq cm, radiative heating rates up to 2900 W/sq cm, with test specimen surface pressures of 0.06, 0.1, and 0.3 atm in an air stream. The experimental and analytical mass loss and surface temperature results agreed well when the carbon vapor thermodynamic properties from the JANAF tables are used in the analysis.
This paper discusses a resin developed for use in autoclave molding of polyimide graphite composite stiffened, titanium alloy structures. Both primary and secondary bonded structures were evaluated that were produced by autoclave processing. Details of composite processing, adhesive formulary, and bonding processes are provided in this paper, together with mechanical property data for structures. These data include -65 F, room temperature, and 600 F shear strengths; strength retention after aging; and stress rupture properties at 600 F under various stress levels for up to 1000 hours duration. Typically, shear strengths in excess of 16 ksi at room temperature with over 60% strength retention at 600 F were obtained with titanium alloy substrates.
The first crystal X-ray polarimeter to be used for X-ray astronomy is described. Polarization is measured by modulation of the X rays diffracted at an average 45 deg glancing angle from large, curved graphite crystal panels as these rotate about an axis parallel to the incident X-ray flux. Arrangement of the crystal panels, the design of the detector, and the signal-processing circuitry were optimized to minimize systematic effects produced by off-axis pointing of the rocket and cosmic ray induced events. The in-flight performance of the instrument in relation to the observed background signal is discussed.
Powdered polymer is finely ground. Second polymer, soluble, is mixed with appropriate solvent. Milled polymer and graphite filaments are added to soluble polymer-solvent solution to create slurry. Slurry is dried, and when ready for processing, the soluble, binder-polymer is removed by heat during precure or cure cycle.
The state-of-the-art of graphite/polyimide structures was evaluated and key design and fabrication issues to be considered in future hardware programs are defined. The fabrication and testing at 500 F of a graphite/polyimide center wing box beam using OV-10A aircraft criteria was accomplished. The baseline design of this box was developed in a series of studies of other advanced composite materials: glass/epoxy, boron/epoxy, and boron/polyimide. The use of this basic design permits ready comparison of the performance of graphite/polyimide with these materials. Modifications to the baseline composite design were made only in those areas effected by the change of materials. Processing studies of graphite fiber polyimide resins systems resulted in the selection of a Modmor II/Gemon L material.
Filament wound NOL rings, 4-inch and 8-inch diameter closed-end vessels involving three epoxy resin systems and three graphite fibers were tested to develop property data and fabrication technology for filament wound graphite/epoxy pressure vessels. Vessels were subjected to single-cycle burst tests at room temperature. Manufacturing parameters were established for tooling, winding, and curing that resulted in the development of a pressure/vessel performance factor (pressure x volume/weight) or more than 900,000 in. for an oblate spheroid specimen.
Sliding friction experiments were conducted with amorphous and fully graphitized carbons sliding on copper and on films of chromium and aluminum on copper. Auger emission spectroscopy analysis was used to monitor carbon transfer to the metal surfaces. Friction and wear were also measured. Metal surfaces were examined both in the clean state and with normal oxides present. Results indicate that different metals have an important effect on friction, wear, and transfer characteristics. With amorphous carbon, the least chemically active metal gave the highest wear and amount of carbon transfer. Both forms of carbon gave lower friction and wear and lower transfer rates when in contact with clean, as opposed to oxide-covered, chromium surfaces. With copper, the reverse was true; cleaning was detrimental.