A compendium of sources of fracture toughness and fatigue crack growth data for metallic alloys, part 4
A collection of sources is presented of fracture toughness and fatigue crack growth data for metallic alloys.
SEARCH · Engineering Papers
Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.
Quote a phrase for an exact phrase match. Source license links do not imply unrestricted reuse.
A collection of sources is presented of fracture toughness and fatigue crack growth data for metallic alloys.
A new computational simulation method is presented to evaluate the dynamic aspects of composite structural response and durability that have not been simulated previously. Composite structural behavior under any loading condition, geometry, composite system, laminate configuration, and boundary conditions can now be simulated. Structural degradation, delamination, fracture, and damage propagation are included in the simulation. An angle-plied composite plate structure under normal impact loading is used as an example to demonstrate the versatility of the simulation method.
The effects of dissolved hydrogen on the mechanical properties of 2090 and 2219 alloys are studied. The work done during this semi-annual period consists of the hydrogen charging study and some preliminary mechanical tests. Prior to SIMS analysis, several potentiostatic and galvanostatic experiments were performed for various times (going from 10 minutes to several hours) in the cathodic zone, and for the two aqueous solutions: 0.04N of HCl and 0.1N NaOH both combined with a small amount of As2O3. A study of the surface damage was conducted in parallel with the charging experiments. Those tests were performed to choose the best charging conditions without surface damage. Disk rupture tests and tensile tests are part of the study designed to investigate the effect of temperature, surface roughness, strain rate, and environment on the fracture behavior. The importance of the roughness and environment were shown using the disk rupture test as well as the importance of the strain rate under hydrogen environment. The tensile tests, without hydrogen effects, have not shown significant differences between low and room temperature.
The fundamental principles allowing design of stainless bearing steels with enhanced toughness and stress corrosion resistance has involved both investigation of basic phenomena in model alloys and evaluation of a prototype bearing steel based on a conceptual design exercise. Progress in model studies has included a scanning Auger microprobe (SAM) study of the kinetics of interfacial segregation of embrittling impurities which compete with the kinetics of alloy carbide precipitation in secondary hardening steels. These results can define minimum allowable carbide precipitation rates and/or maximum allowable free impurity contents in these ultrahigh strength steels. Characterization of the prototype bearing steel designed to combine precipitated austenite transformation toughening with secondary hardening shows good agreement between predicted and observed solution treatment response including the nature of the high temperature carbides. An approximate equilibrium constraint applied in the preliminary design calculations to maintain a high martensitic temperature proved inadequate, and the solution treated alloy remained fully austenitic down to liquid nitrogen temperature rather than transforming above 200 C. The alloy can be martensitically transformed by cryogenic deformation, and material so processed will be studied further to test predicted carbide and austenite precipitation behavior. A mechanistically-based martensitic kinetic model was developed and parameters are being evaluated from available kinetic data to allow precise control of martensitic temperatures of high alloy steels in future designs. Preliminary calculations incorporating the prototype stability results suggest that the transformation-toughened secondary-hardening martensitic-stainless design concept is still viable, but may require lowering Cr content to 9 wt. pct. and adding 0.5 to 1.0 wt. pct. Al. An alternative design approach based on strain-induced martensitic transformation during cryogenic forming, thus removing the high martensitic constraint, may permit alloy compositions offering higher fracture roughness.
Two aromatic polyimides and an aromatic polyamide-imide were tested in single edge notched tension. Fracture toughnesses, normalized to 25 micron film thickness ranged from 1.65 to 5.4 MPa m sup 1/2. LARC-TPI, a thermoplastic polyimide, showed evidence of crazing ahead of a growing crack whereas the other materials formed a shear yielded zone.
A new computational simulation method is presented to evaluate the dynamic aspects of composite structural response and durability that could not be simulated previously. Composite structural behavior under any loading, geometry, composite system, laminate configuration, and boundary conditions can now be simulated. Structural degradation, delamination, fracture, and damage propagation are included in the simulation. An angle-plied composite plate structure under normal impact loading is used as an example to demonstrate the versatility of the simulation method.
The calculation of shape and scale parametes of the two-parameter Weibull distribution is described using the least-squares analysis and maximum likelihood methods for volume- and surface-flaw-induced fracture in ceramics with complete and censored samples. Detailed procedures are given for evaluating 90 percent confidence intervals for maximum likelihood estimates of shape and scale parameters, the unbiased estimates of the shape parameters, and the Weibull mean values and corresponding standard deviations. Furthermore, the necessary steps are described for detecting outliers and for calculating the Kolmogorov-Smirnov and the Anderson-Darling goodness-of-fit statistics and 90 percent confidence bands about the Weibull distribution. It also shows how to calculate the Batdorf flaw-density constants by using the Weibull distribution statistical parameters. The techniques described were verified with several example problems, from the open literature, and were coded in the Structural Ceramics Analysis and Reliability Evaluation (SCARE) design program.
The spall velocities produced by nine experimental impacts of 1 to 6.5 km/sec into San Marcos gabbro targets, using projectiles of Fe, Al, Pb, and basalt of various sizes, have been measured in conjunction with fragment-velocity high-speed filmings of the events. A detailed comparison is made between measured spall velocities and those predicted by the model of Melosh (1984), with a view to the compatibility of small-scale results and large planetary impacts. Attention is also given to the patterns of internal fracture generated by impact within the targets.
Mode I interlaminar fracture toughness was determined on a series of unidirectional poly(phenylene oxide)/carbon fiber composites using the double cantilever beam test. Initial toughness for growth of a delamination from an insert depends on fiber type, and ranges from 190 to 440 J/sq m, with intermediate modulus fibers tending to give lower values than high-strain fibers. Low toughness values are attributed to poor fiber-matrix adhesion. As a delamination progress down the beam, fiber bridging increases the apparent toughness by up to a factor of 7, depending on the fiber.
Test specimen and loading frame developed for fatigue and fracture testing of materials under mode-II (sliding-mode) loading. Assembly placed in compression-testing machine. Loads directed oppositely along centerline cause self-similar crack to propagate. Enables consistently accurate alignment of specimens before insertion of specimen/frame assemblies into compression-testing machine. Makes design attractive for testing in hostile environments in which access to machine or furnace limited. Additional feature, with little or no modification, placed horizontally into impact testing machine and subjected to loading at high speeds.
The near-crack-tip stresses in any planar coupon of arbitrary geometry subjected to mode 1 loading may be equated to those in an infinite center-cracked panel subjected to the appropriate equivalent remote biaxial stresses (ERBS). Since this process can be done for all such mode 1 coupons, attention may be focused on the behavior of the equivalent infinite cracked panel. To calculate the ERBS, the constant term in the series expansion of the crack-tip stress must be retained. It is proposed that the ERBS may be used quantitatively to explain different fracture phenomena such as crack branching.
Fiber/matrix (F/M) cracking was analyzed to provide better understanding and guidance in developing F/M interface fracture toughness tests. Two configurations, corresponding to F/M cracking at a broken fiber and at the free edge, were investigated. The effects of mechanical loading, thermal cooldown, and friction were investigated. Each configuration was analyzed for two loadings: longitudinal and normal to the fiber. A nonlinear finite element analysis was performed to model friction and slip at the F/M interface. A new procedure for fitting a square-root singularity to calculated stresses was developed to determine stress intensity factors (K sub I and K sub II) for a bimaterial interface crack. For the case of F/M cracking at a broken fiber with longitudinal loading, crack tip conditions were strongly influenced by interface friction. As a result, an F/M interface toughness test based on this case was not recommended because nonlinear data analysis methods would be required. For the free edge crack configuration, both mechanical and thermal loading caused crack opening, thereby avoiding frictional effects. A F/M interface toughness test based on this configuration would provide data for K(sub I)/K(sub II) ratios of about 0.7 and 1.6 for fiber and radial normal loading, respectively. However, thermal effects must be accounted for in the data analysis.
The fusion of the probabilistic finite element method (PFEM) and reliability analysis for probabilistic fracture mechanics (PFM) is presented. A comprehensive method for determining the probability of fatigue failure for curved crack growth was developed. The criterion for failure or performance function is stated as: the fatigue life of a component must exceed the service life of the component; otherwise failure will occur. An enriched element that has the near-crack-tip singular strain field embedded in the element is used to formulate the equilibrium equation and solve for the stress intensity factors at the crack-tip. Performance and accuracy of the method is demonstrated on a classical mode 1 fatigue problem.
Plane strain fracture toughness (K sub IC) was evaluated for Weldalite (tm) 049 with and without TiB2 reinforcement. For the nonreinforced variant, changes in toughness were measured for various aging conditions and lithium levels. Toughness testing was carried out on fatigue precracked compact tension (CT) specimens at 24 C, as per ASTM standard E-399. Toughness was measured as a function of aging time at 160 C for the two Weldalite 049(1.3) heats. The composition of these heats differed only in that 0.03 wt pct. Ti was added to one as an additional grain refiner. Both heats showed a decrease in toughness with increasing aging time, although toughness values for one were significantly higher than for the other. This greater toughness may be due to a subtle change in the grain size resulting for the presence of Ti or, alternatively, to differences in texture or substructure formed during extrusion.
Studies of oxygen-strengthened titanium alloys have indicated that while hydrogen has little effect on tensile properties, it causes a marked decrease in impact strength. It is presently established experimentally that the presence of hydrogen has essentially no effect on the fracture-toughness factor at the onset of crack propagation, in commercial-grade titanium alloys containing either low or high concentrations of oxygen. These findings are congruent with other study results on the tensile properties of these alloys, but contrast with the previously noted pronounced effect of hydrogen on impact resistance.
Experiments were performed on center-notched specimens of unidirectional AS4/3501-6 graphite-epoxy subjected to varied far-field loading conditions. Specimens tested include on-axis and off-axis tensile coupons and Iosipescu shear specimens, allowing the study of normal, shear, and combined far-field loading conditions. From the tests, the direction of initial crack extension and the far-field stresses at crack initiation and fracture are obtained. The normal stress ratio theory is subsequently applied within a macroscopic-level homogeneous anisotropic stress solution to predict the direction of crack extension, critical stresses, and other crack growth behavior for the experiments. Comparison between experimental results and theoretical predictions indicates that application of the normal stress ratio theory within a macroscopic-level stress analysis has significant potential as an approach to modeling composite crack growth.
The room temperature and 300 C tensile behavior of a single crystal superalloy, PWA 1480, has been studied as a function of internal hydrogen concentration and microstructure. Hydrogen is trapped at the porosity and eutectic gamma/gamma in the microstructure, and the effect of these trapping sites on the tensile behavior will be discussed. There is no effect of hydrogen on strength, however, the strain to failure decreases steadily with increasing hydrogen content up to 200 ppm. Cleavage of the eutectic gamma/gamma occurs without hydrogen, but the presence of internal hydrogen causes cracking in the eutectic gamma/gamma at a much earlier stage of deformation leading to a small total strain. In contrast to many superalloys with a high volume fraction of gamma precipitates, there was no evidence of shearing of the gamma, and it was found that at all strains the dislocations are trapped in the gamma matrix. The effect of hydrogen on this behavior and its relation to fracture is described.
A stochastic damage model is proposed to quantify the inherent statistical distribution of the fracture toughness of a brittle, multi-phase solid. The model, based on the macrocrack-microcrack interaction, incorporates uncertainties in locations and orientations of microcracks. Due to the high concentration of microcracks near the macro-tip, a higher order analysis based on traction boundary integral equations is formulated first for an arbitrary array of cracks. The effects of uncertainties in locations and orientations of microcracks at a macro-tip are analyzed quantitatively by using the boundary integral equations method in conjunction with the computer simulation of the random microcrack array. The short range interactions resulting from surrounding microcracks closet to the main crack tip are investigated. The effects of microcrack density parameter are also explored in the present study. The validity of the present model is demonstrated by comparing its statistical output with the Neville distribution function, which gives correct fits to sets of experimental data from multi-phase solids.