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NASA NTRS2003

Residual Gases in Crystal Growth Systems

Residual gases present in closed ampoules may affect different crystal growth processes. That seems to be particularly true under microgravity conditions where, due to weightlessness of the melt, the gases may lead to detached solidification and/or formation of voids and bubbles, as observed in the past. For that reason a good understanding and control of formation of residual gases is important for an optimum design and meaningful interpretation of crystal growth experiments. Our extensive experimental and theoretical studies of the subject, summarized in this paper, include degassing of silica glass and generation of gases from different source materials. Different materials processing conditions, like outgassing under vacuum, annealing in hydrogen, resublimation, different material preparation procedures, multiple annealings, different processing times, and others were applied and their effect on the amount and composition of gas were analyzed. The experimental results were interpreted based on theoretical calculations on diffusion in silica glass and source materials and thermochemistry of the system. Procedures for a reduction of the amount of gas are also discussed.

Palosz, W.↗
NASA NTRS2004

Brake Failure from Residual Magnetism in the Mars Exploration Rover Lander Petal Actuator

In January 2004, two Mars Exploration Rover spacecraft arrived at Mars. Each safely delivered an identical rover to the Martian surface in a tetrahedral lander encased in airbags. Upon landing, the airbags deflated and three Lander Petal Actuators opened the three deployable Lander side petals enabling the rover to exit the Lander. Approximately nine weeks prior to the scheduled launch of the first spacecraft, one of these mission-critical Lander Petal Actuators exhibited a brake stuck-open failure during its final flight stow at Kennedy Space Center. Residual magnetism was the definitive conclusion from the failure investigation. Although residual magnetism was recognized as an issue in the design, the lack of an appropriately specified lower bound on brake drop-out voltage inhibited the discovery of this problem earlier in the program. In addition, the brakes had more unit-to-unit variation in drop-out voltage than expected, likely due to a larger than expected variation in the magnetic properties of the 15-5 PH stainless steel brake plates. Failure analysis and subsequent rework of two other Lander Petal Actuators with marginal brakes was completed in three weeks, causing no impact to the launch date.

Jandura, Louise↗
NASA NTRS2003

Constraints on the Within Season and Between Year Variability of the North Residual Cap from MGS-TES

There is a long history of telescopic and spacecraft observations of the polar regions of Mars. The finely laminated ice deposits and surrounding layered terrains are commonly thought to contain a record of past climate conditions and change. Understanding the basic nature of the deposits and their mineral and ice constituents is a continued focus of current and future orbited missions. Unresolved issues in Martian polar science include a) the unusual nature of the CO2 ice deposits ("Swiss Cheese", "slab ice" etc.) b) the relationship of the ice deposits to underlying layered units (which differs from the north to the south), c) understanding the seasonal variations and their connections to the finely laminated units observed in high-resolution images and d) the relationship of dark materials in the wind-swept lanes and reentrant valleys to the surrounding dark dune and surface materials. Our work focuses on understanding these issues in relationship to the north residual ice cap. Recent work using Mars Global Surveyor (MGS) data sets have described evolution of the seasonal CO2 frost deposits. In addition, the north polar residual ice cap exhibits albedo variations between Mars years and within the summer season. The Thermal Emission Spectrometer (TES) data set can augment these observations providing additional constraints such as temperature evolution and spectral properties associated with ice and rocky materials. Exploration of these properties is the subject of our current study.

Calvin, W. M.↗
NASA NTRS2003

Analysis of the Effects of Residual Strains and Defects on Skin/Stiffener Debonding using Decohesion Elements

Delamination is one of the predominant forms of failure in laminated composites especially when there is no reinforcement in the thickness direction. To develop composite structures that are more damage tolerant, it is necessary to understand how delamination develops and how it can affect the residual performance. A number of factors such as residual thermal strains, matrix curing shrinkage, and manufacturing defects affect how damage will grow in a composite structure. It is important to develop analysis methods that are computationally efficient that can account for all such factors. The objective of the current work is to apply a newly developed decohesion element to investigate the debond strength of skin/stiffener composite specimens. The process of initiation of delaminations and the propagation of delamination fronts is investigated. The numerical predictions are compared with published experimental results.

Davila, Carlos G.↗
NASA NTRS1996

Single residue substitutions that change the gating properties of a mechanosensitive channel in Escherichia coli

MscL is a channel that opens a large pore in the Escherichia coli cytoplasmic membrane in response to mechanical stress. Previously, we highly enriched the MscL protein by using patch clamp as a functional assay and cloned the corresponding gene. The predicted protein contains a largely hydrophobic core spanning two-thirds of the molecule and a more hydrophilic carboxyl terminal tail. Because MscL had no homology to characterized proteins, it was impossible to predict functional regions of the protein by simple inspection. Here, by mutagenesis, we have searched for functionally important regions of this molecule. We show that a short deletion from the amino terminus (3 amino acids), and a larger deletion of 27 amino acids from the carboxyl terminus of this protein, had little if any effect in channel properties. We have thus narrowed the search of the core mechanosensitive mechanism to 106 residues of this 136-amino acid protein. In contrast, single residue substitutions of a lysine in the putative first transmembrane domain or a glutamine in the periplasmic loop caused pronounced shifts in the mechano-sensitivity curves and/or large changes in the kinetics of channel gating, suggesting that the conformational structure in these regions is critical for normal mechanosensitive channel gating.

Non-NASA Center↗
NASA NTRS2005

Effects of Atmospheric Dust on Residual South Polar Cap Stability

The Martian polar caps have been studied from the time of Herschel. Neither polar cap normally disappears in summer. The Residual North Polar Cap (portion that remains through summer) is composed of a mixture of water ice and dust, and its interannual stability is due to its low sublimation rate at the summer temperatures in the North Polar Region. The Residual South Polar Cap (RSPC) is more enigmatic, surviving the relatively hot perihelic summer season despite being composed of much more volatile CO2. It is able to do so because of its unusually high albedo, which is larger than that of other bright regions in the seasonal cap (e.g. Mountains of Mitchel). The proximity of the albedo of the RSPC to the critical albedo for stability raises the question of whether the RSPC exists in every Martian year. The ground based record is somewhat ambivalent. Douglass and Lowell reported that RSPC suddenly vanished at Ls=297deg in 1894 and did not reappear until Ls=0deg [1], and Kuiper reported that it disappeared in 1956 [2]; but both observations were questioned by contemporaries, who tended to attribute them to obscuring dust. Barker [3] reported a large amount of water vapor over the south polar cap in 1969 that could be attributed to exposure of near surface water ice during partial removal of the CO2 in the RSPC in 1969.

Bonrv, B. P.↗
NASA NTRS2005

Jim Starnes' Contributions to Residual Strength Analysis Methods for Metallic Structures

A summary of advances in residual strength analyses methods for metallic structures that were realized under the leadership of Dr. James H. Starnes, Jr., is presented. The majority of research led by Dr. Starnes in this area was conducted in the 1990's under the NASA Airframe Structural Integrity Program (NASIP). Dr. Starnes, respectfully referred to herein as Jim, had a passion for studying complex response phenomena and dedicated a significant amount of research effort toward advancing damage tolerance and residual strength analysis methods for metallic structures. Jim's efforts were focused on understanding damage propagation in built-up fuselage structure with widespread fatigue damage, with the goal of ensuring safety in the aging international commercial transport fleet. Jim's major contributions in this research area were in identifying the effects of combined internal pressure and mechanical loads, and geometric nonlinearity, on the response of built-up structures with damage. Analytical and experimental technical results are presented to demonstrate the breadth and rigor of the research conducted in this technical area. Technical results presented herein are drawn exclusively from papers where Jim was a co-author.

Young, Richard D.↗
NASA NTRS2004

Probabilistic Residual Strength Model Developed for Life Prediction of Ceramic Matrix Composites

For the next generation of reusable launch vehicles, NASA is investigating introducing ceramic matrix composites (CMCs) in place of current superalloys for structural propulsion applications (e.g., nozzles, vanes, combustors, and heat exchangers). The higher use temperatures of CMCs will reduce vehicle weight by eliminating and/or reducing cooling system requirements. The increased strength-to-weight ratio of CMCs relative to superalloys further enhances their weight savings potential. However, in order to provide safe designs for components made of these new materials, a comprehensive life prediction methodology for CMC structures needs to be developed. A robust methodology for lifing composite structures has yet to be adopted by the engineering community. Current industry design practice continues to utilize deterministic empirically based models borrowed from metals design for predicting material life capabilities. The deterministic nature of these models inadequately addresses the stochastic character of brittle composites, and their empirical reliance makes predictions beyond the experimental test conditions a risky extrapolation. A team of engineers at the NASA Glenn Research Center has been developing a new life prediction engineering model. The Probabilistic Residual Strength (PRS) model uses the residual strength of the composite as its damage metric. Expected life and material strength are both considered probabilistically to account for the observed stochastic material response. Extensive experimental testing has been carried out on C/SiC (a candidate aerospace CMC material system) in a controlled 1000 ppm O2/argon environment at elevated temperatures of 800 and 1200 C. The test matrix was established to allow observation of the material behavior, characterization of the model, and validation of the model's predictive capabilities. Sample results of the validation study are illustrated in the graphs.

Thomas, David J.↗
NASA NTRS2006

On detecting a trend in the residual circulation from observations of column HCl

The troposphere is the part of the atmosphere where people live. The troposphere goes up to about 12 km above the earth over places at middle latitudes like Washington, D.C. The next layer of air up in the atmosphere is called the stratosphere. The tropopause separates the troposphere and stratosphere. Most of the ozone in the atmosphere is in the stratosphere where it protects people from the harmful rays in sunlight. Near the earth s surface, ozone is a pollutant. In general, air travels from the troposphere to the stratosphere through upward motion in the tropics. Most of the air comes back down to the troposphere at middle latitudes. The so-called "stratospheric residual circulation" moves the air in the stratosphere from the tropics to the middle latitudes. In this way, the amount of air that moves out of the stratosphere into the troposphere at middle latitudes depends on the strength of the residual circulation. This overturning of the atmosphere is important as it brings chemicals produced by the activities of people into the stratosphere. Most notable are chlorofluorocarbons (CFCs) that destroy stratospheric ozone. The transport of air out of the stratosphere removes ozone-destroying chemicals, but also brings ozone into the troposphere.

Olsen, M. A.↗
NASA NTRS2002

Residual wave front phase estimation in the reimaged lyot plane for the eclipse coronographic telescope

Coronagraphs for extra-solar planet detection remove diffracted stellar light through the combination of a coronagraphic mask and a Lyot stop. When the entrance pupil contains a nearly perfect wave fiont, most of the stellar light is absorbed at the mask. Light scattered around the spot due to mid- and high-spatial frequency phase errors in the pupil appears at the Lyot plane as speckles whose amplitudes are proportional to the local wave front phase residuals. The speckles scale with optical wavelength but are not radially smeared. The Eclipse deformable mirror (DM) can be used to modify the Lyot amplitude distribution, providing a simple means of estimating the residual phase content and controlling the wave front. To reduce the detrimental noise carried by uncontrollable high-spatial frequency wave front components, theLyot plane signal is filtered at the science plane to pass only the controllable spatial frequencies that contribute to the dark hole. The Lyot stop is then reimaged onto a detector. We demonstrate through simulations that this approach signiscantly improves the signal-to-noise ratio of the planet measurement.

coronagraph wave front sensing wave front control↗
NASA NTRS2006

The High Resolution Tropospheric Ozone Residual

The co-flight of the MLS stratospheric limb sounder and the Ozone Monitoring Instrument (OMI) provides the capability of computing the Tropospheric Ozone Residual (TOR) in much greater detail [Ziemke et al., 2006]. Using forward trajectory calculations of MLS ozone measurements combined with OMI column ozone we have developed a high horizontal resolution tropospheric ozone residual (HTOR) which can provide even more detail than the standard TOR product. HTOR is especially useful for extra-tropical studies of tropospheric ozone transport. We find that both the Pacific pollution corridor (East Asia to Alaska) and the Atlantic pollution corridor (North America east coast to Europe) are also preferred locations for strat-trop folds leading to systematic overestimates of pollution amounts. In fact, fold events appear to dominate extra-tropical Northern Hemisphere day-to-day maps of HTOR. Model estimates of the tropospheric column are in reasonable agreement with the HTOR amounts when offsets due to different tropopause height calculations are taken into consideration.

Schoeberl, Mark R.↗
NASA NTRS2008

Transmission Electron Microscopy of Cometary Residues from Micron-Sized Craters in the Stardust Al-Foils

We report Transmission Electron Microscopy (TEM) investigations of micro-craters that originated from hypervelocity impacts of comet 81P/Wild 2 dust particles on the aluminium foil of the Stardust collector. The craters were selected by Scanning Electron Microscopy (SEM) and then prepared by Focused Ion Beam (FIB) milling techniques in order to provide electron transparent cross-sections for TEM studies. The crater residues contain both amorphous and crystalline materials in varying proportions and compositions. The amorphous component is interpreted as resulting from shock melting during the impact and the crystalline phases as relict minerals. The latter show evidence for shock metamorphism. Based on the residue morphology and the compositional variation, the impacting particles are inferred to have been dominated by mixtures of submicron olivine, pyroxene and Fe-sulfide grains, in agreement with prior results of relatively coarse-grained mineral assemblages in the aerogel collector.

Leroux, Hugues↗
NASA NTRS2008

Weld Residual Stress and Distortion Analysis of the ARES I-X Upper Stage Simulator (USS)

An independent assessment was conducted to determine the critical initial flaw size (CIFS) for the flange-to-skin weld in the Ares I-X Upper Stage Simulator (USS). The Ares system of space launch vehicles is the US National Aeronautics and Space Administration s plan for replacement of the aging space shuttle. The new Ares space launch system is somewhat of a combination of the space shuttle system and the Saturn launch vehicles used prior to the shuttle. Here, a series of weld analyses are performed to determine the residual stresses in a critical region of the USS. Weld residual stresses both increase constraint and mean stress thereby having an important effect on fatigue and fracture life. While the main focus of this paper is a discussion of the weld modeling procedures and results for the USS, a short summary of the CIFS assessment is provided.

Raju, Ivatury↗
NASA NTRS2008

Ares I-X Upper Stage Simulator Residual Stress Analysis

The structural analyses described in the present report were performed in support of the NASA Engineering and Safety Center (NESC) Critical Initial Flaw Size (CIFS) assessment for the Ares I-X Upper Stage Simulator (USS) common shell segment. An independent assessment was conducted to determine the critical initial flaw size (CIFS) for the flange-to-skin weld in the Ares I-X Upper Stage Simulator (USS). The Ares system of space launch vehicles is the US National Aeronautics and Space Administration s plan for replacement of the aging space shuttle. The new Ares space launch system is somewhat of a combination of the space shuttle system and the Saturn launch vehicles used prior to the shuttle. Here, a series of weld analyses are performed to determine the residual stresses in a critical region of the USS. Weld residual stresses both increase constraint and mean stress thereby having an important effect on fatigue and fracture life. The results of this effort served as one of the critical load inputs required to perform a CIFS assessment of the same segment.

Raju, Ivatury S.↗
NASA NTRS2009

Analytic Confusion Matrix Bounds for Fault Detection and Isolation Using a Sum-of-Squared- Residuals Approach

Given a system which can fail in 1 or n different ways, a fault detection and isolation (FDI) algorithm uses sensor data in order to determine which fault is the most likely to have occurred. The effectiveness of an FDI algorithm can be quantified by a confusion matrix, which i ndicates the probability that each fault is isolated given that each fault has occurred. Confusion matrices are often generated with simulation data, particularly for complex systems. In this paper we perform FDI using sums of squares of sensor residuals (SSRs). We assume that the sensor residuals are Gaussian, which gives the SSRs a chi-squared distribution. We then generate analytic lower and upper bounds on the confusion matrix elements. This allows for the generation of optimal sensor sets without numerical simulations. The confusion matrix bound s are verified with simulated aircraft engine data.

Simon, Dan↗
NASA NTRS2010

Environmental Stress Testing of the Single Sample Cylinder: A Proven Consensus Standard for Internal Gas Analysis (IGA) or Residual Gas Analysis (RGA)

In August 2008, Schuessler Consulting was contracted by NASA GSFC in support of the NASA Electronic Parts and Packaging (NEPP) program to perform two separate studies on moisture laden air in a stainless steel cylinder that had been designed to become a consensus standard for Test Method 1018. This Test Method was originally released for hybrids under Mil. Std. 883 but was quickly utilized on other microelectronic devices under the auspice of Mil. Std. 750. The cylinder had subsequently been fabricated for the 750 community. It was back-filled with moist air and subsequently analyzed over a period of time under a previous NASA contract. It had been shown that moisture in the 4000 - 5000 ppm range could be analyzed rather precisely with a mass spectrometer, commonly referred to as a Residual Gas Analyzer (RGA). The scope of this study was to ascertain if the composition and precision varied as a function of thermal shock at sub-zero temperatures and whether there was consensus when the standard was submitted to other RGA units. It was demonstrated and published that the consensus standard would yield precise RGA data for moisture within +/- 1% when optimized for a given RGA unit. It has been subsequently shown in this study at Oneida Research Services, that sub-zero storage did not affect that precision when a well-defined protocol for the analysis was followed. The consensus standard was taken to a second facility for analysis where it was found that moisture adsorption on the transfer lines caused precision to drop to +/- 12%. The Single Sample Cylinder (SSC) is a one liter stainless steel cylinder with associated sampling valves and has considerable weight and volume. But this considerable size allows for approximately 300 gas samples of the same composition to be delivered to any RGA unit. Lastly, a smaller cylinder, approximately 75 cc, of a second consensus standard was fabricated and tested with a different mix of fixed gases where moisture was kept in the 100 ppm range. This second standard has the potential of providing 30 gaseous samples and can be readily shipped to any analytical facility that desires to generate comparison RGA data. A series of comparison residual gas analyses was performed at the Honeywell Federal Manufacturing & Technologies facility in the National Nuclear Facility Administration s plant in Kansas City to complete this project. It was shown that improvements in the precision of a given RGA unit can be done by controlling the cycle time for each analysis and increasing analysis temperatures to minimize moisture adsorption. It was also found that a "one time event" in the subzero storage of the large SSC did not effect the units ability to continuously supply precise samples of the same chemistry, however the "event" caused a permanent +8% shift in the reported value of the moisture content. Lastly, a set of SSC RGA results was plotted on a common graph with DSCC "correlation study" RGA data. The result demonstrates the ability of the SSC to remove many of the individual variances that single, individual samples introduce. The consensus standards are now in storage at Oneida Research Services, one of the DSCC certified houses that does RGA to Military Standards, where they await future studies. The analytical data and the operational parameters of the instruments used are provided in the following discussion. Limitations and suggested means for improvement of both precision and accuracy are provided.

Schuessler, Philipp WH↗
NASA NTRS2011

Adaptive Control of Non-Minimum Phase Modal Systems Using Residual Mode Filters2

Many dynamic systems containing a large number of modes can benefit from adaptive control techniques, which are well suited to applications that have unknown parameters and poorly known operating conditions. In this paper, we focus on a direct adaptive control approach that has been extended to handle adaptive rejection of persistent disturbances. We extend this adaptive control theory to accommodate problematic modal subsystems of a plant that inhibit the adaptive controller by causing the open-loop plant to be non-minimum phase. We will modify the adaptive controller with a Residual Mode Filter (RMF) to compensate for problematic modal subsystems, thereby allowing the system to satisfy the requirements for the adaptive controller to have guaranteed convergence and bounded gains. This paper will be divided into two parts. Here in Part I we will review the basic adaptive control approach and introduce the primary ideas. In Part II, we will present the RMF methodology and complete the proofs of all our results. Also, we will apply the above theoretical results to a simple flexible structure example to illustrate the behavior with and without the residual mode filter.

Balas, Mark J.↗
NASA NTRS2012

Estimating Model Error Using Observation Residuals

This presentation discusses an approach to estimate model error using observation residuals. Based on the sequential fixed-lag smoother; we introduce a diagnostic procedure to allow estimating model error over a dense observing system. Optimality considerations are examined in light of the sequential results. The procedure is re-interpreted in the language of variational assimilation, such as 4d-Var. Illustrations of the approach are given by studying both identical-twin and fraternal-twin experimental settings for a system governed by Lorenz-type dynamics. Preliminary results by looking at observation residual statistics for the ECMWF data assimilation system are also shown. The presentation will be part of a series of discussions on issues related to four-dimensional data assimilation under weak-constraint and methodologies to estimate model error.

Todling, Ricardo↗