Studies on the Module Structure for the NOvA Liquid Scintillator Neutrino Detector
This thesis contains studies pertinent to the construction of modules for the NOνAexperiment detectors. The tensile strength of acrylic and epoxy adhesives used in construction of the detector was studied over time and with various surface preparations. Sanding and corona discharge surface treatments increased the bond strength of the acrylic by 10-20%; aging in oil did not affect the acrylic bond strength while aging in air at 50°C for 9 months (equivalent to approximately 5 years at room temperature) increased the acrylic bond strength by 25%. For the epoxy, corona discharge treated samples’ strength increased slightly after aging while the strength of sanded samples in air remained consistent and sanded samples in oil decreased by 17% when aged at 50°C for 1.5 years (equivalent to approximately 10 years at room temperature).All materials used in the detector were studied to determine if degrading interaction would occur with the pseudocumene liquid scintillator. Substances such as acrylic adhesive and PTFE paste were found to interact with the scintillator while materials such as a variety of PVCs, epoxy adhesives, and PTFE tape were found to be non-reactive with the scintillator. Following the appearance of cracks on manifold covers in installed modules, studies were carried out to help to determine the cause and mitigation of these cracks. Manifold covers that had been pressure tested at various pressures during the check of the seals during the manufacturing process were examined for the formation of cracks. “Containment units” were used to constrain the swelling of the manifold covers during pressure testing. Internal cracks were visible on the majority of manifold covers tested at 1.4 bar with the original containment units. It was found that reducing the pressure testing of the modules from 1.4 bar to 0.7 bar and increasing the rigidity of the pressure test containment units eliminated the formation of visible cracks in the manifold covers. Stress concentration in small fillet radius injection molded PVC was studied. GeonM3500 PVC has a yield strength 12% greater than Geon M3800 PVC originally used for the manifold covers but increased the stress concentrated failure time by 6600% and was thus chosen to mold new manifold covers after a redesign to eliminate stress concentrating features.