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NASA NTRS2022

Qualification and Performance of a High-Efficiency Laser Transmitter for Deep-Space Optical Communications

A high-power Laser Transmitter Assembly (LTA) was developed to support the Deep Space Optical Communications (DSOC) technology demonstration being developed by the Jet Propulsion Laboratory. NASA’s Psyche Mission plans to host the DSOC flight subsystem for testing space-to-ground high-bandwidth laser communications en route to the 16 Psyche asteroid. We review the design, performance, and qualification of the LTA Engineering Model and Flight Model (EM and FM) delivered to JPL. The LTA uses a master-oscillator power amplifier (MOPA) design and delivers up to 4.5 W at 1550 nm, with a highly efficient, cladding-pumped, polarization-maintaining erbium-ytterbium fiber amplifier. The master oscillator generates a range of pulse widths and repetition rates to support modulation formats from 16- to 128-PPM for optical data transmission at >100 Mbps. The LTA was designed for high reliability and radiation hardness, and includes redundant signal and pumping paths to reduce single points of failure, hardware interlocks to ensure safe operation and protection against damage, closed-loop control of optical power, and detailed health and status via telemetry. The LTA EM and FM were subjected to unit-appropriate space qualification testing. We describe the performance testing of the EM and FM, for the characterization of key metrics such as wavelength stability, signal linewidth, optical pulse width, jitter, and extinction ratio, and polarization extinction ratio. The management of optical nonlinearities (self-phase modulation, Brillouin scattering, or pulse-to-pulse energy variation), which could result in an optical link penalty or damage to the LTA, is also detailed, and factors affecting the power efficiency are discussed.

Jaques, J.↗

NASA NTRS1988

High-speed analog fiber optic links for satellite communication

Large-aperture phased array antennas operating at millimeter wave frequencies are designed for space-based communications and imaging. Array elements are comprised of active transmit/receive (T/R) modules which are linked to the central processing unit through a high-speed fiberoptic network. This paper demonstrates optical control of active modules for satellite communication at 24 GHz. An approach called T/R level data mixing, which utilizes fiberoptic transmission of a data signal to individual T/R modules to be upconverted by an optically synchronized local oscillator, is demonstrated at 24 GHz. A free-running HEMT oscillator, used as local oscillator at 24 GHz, is synchronized using indirect subharmonic optical injection locking over a locking range of 14 MHz. Results of data link performance over 500-1000 MHz is also reported in terms of gain-bandwidth, linearity and third-order intercept, sensitivity, and dynamic range.

Daryoush, A. S.↗

DOE OSTI2024

Trifluoromethylation of 2D Transition Metal Dichalcogenides: A Mild Functionalization and Tunable p‐Type Doping Method

Chemical modification is a powerful strategy for tuning the electronic properties of 2D semiconductors. Here, in this study, we report the electrophilic trifluoromethylation of 2D WSe2 and MoS 2 under mild conditions using the reagent trifluoromethyl thianthrenium triflate (TTT). Chemical characterization and density functional theory calculations reveal that the trifluoromethyl groups bind covalently to surface chalcogen atoms as well as oxygen substitution sites. Trifluoromethylation induces p-type doping in the underlying 2D material, enabling the modulation of charge transport and optical emission properties in WSe 2 . This work introduces a versatile and efficient method for tailoring the optical and electronic properties of 2D transition metal dichalcogenides.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2020

Degradation in photovoltaic encapsulation strength of attachment: Results of the first PVQAT TG5 artificial weathering study

Delamination of the encapsulant in photovoltaic (PV) module technology results in immediate optical loss and may enable subsequent corrosion or mechanical damage. The effects of artificial weathering were not previously known; therefore, an empirical study was performed to survey the factors most affecting adhesion, including the ultraviolet (UV) source (ie, Xe or fluorescent lamp[s]), the optical filters for the lamp, the chamber temperature, and the relative humidity. Natural weathering was also performed at locations, including the following: Golden, Colorado; Miami, Florida; Phoenix, Arizona; QiongHai, China; Riyadh, Saudi Arabia; and Turpan, China. Specimens were constructed using a laminated glass/poly (ethylene-co-vinyl acetate)/glass geometry. The compressive shear test (CST) was used to quantify the mechanical strength of attachment, taken as a proxy for adhesion. The fractography of select specimens (including cross-sectional optical microscopy) was used to verify the failure mode (delamination or decohesion). Additional analysis of the local solar spectrum as well as the specimen temperature was performed to interpret the results of natural weathering. The goals of this study include to identify the most significant stressors, clarify where strong coupling may occur between stressors, and validate accelerated test results relative to natural weathering. The importance of specimen conditioning (for moisture) and hygrometric degradation as well as the effects of UV degradation are identified in this paper.

14 SOLAR ENERGY↗

DOE OSTI2024

Poly(cyclosilane) Postpolymerization Hydrosilylation

Postpolymerization functionalization is a key strategy in the diversification of polymeric materials for the conferral of tailored properties. Poly(cyclosilane)s are structurally complex polymers with an all-silicon backbone, featuring a periodic array of hydrido (Si–H) side chains that are potentially suitable for postpolymerization functionalization via hydrosilylation. At the same time, classical methods for hydrosilylation employing Pt- or Pd-based catalysts can result in Si–Si bond scission. In this work, we demonstrate borane-catalyzed hydrosilylation reactions between α-olefins and small molecules or three distinct poly(cyclosilane) architectures. We investigate chemoselectivity for end group versus internal Si–H groups and find that 29 Si cross-polarization magic angle spinning can provide insight on site-selectivity in the functionalization of a complex poly(cyclosilane). Furthermore, we show that postpolymerization hydrosilylation, converting oxidatively sensitive Si–H groups to Si–alkyl chains, modulates solubility and physical characteristics, optical properties, pyrolytic reactivity, and air sensitivity.

36 MATERIALS SCIENCE↗

DOE OSTI2026

Dynamically tunable membrane metasurfaces for infrared spectroscopy and strong light-matter interactions

Mid-infrared spectroscopy enables biochemical sensing by identifying vibrational molecular fingerprints, but it faces limitations in instrumentation portability and analytical sensitivity. Optical metasurfaces with strong mid-infrared photonic resonances provide an attractive solution towards on-chip spectrometry and sensitive molecular detection, yet their static nature hinders their anticipated impact. Here, we introduce and demonstrate dynamically tunable silicon membrane metasurfaces exhibiting high-Q transmissive resonances in the fingerprint region. By harnessing silicon’s thermo-optical properties, we achieve continuous modulation of coupling-induced transparency (CIT) modes that emerge upon the interference of quasi-bound states in the continuum (q-BICs) and surface lattice modes (SLMs). We measure a spectral tuning rate of 0.06 cm −1 K −1 by continuously sweeping the sharp CIT resonances over a 23.5 cm −1 spectral range across a temperature range of 300–700 K. In the current proof‑of‑concept implementation, the dynamic transmission control enables non-contact chemical analysis of polymer films by detecting characteristic absorption bands of polystyrene (1450 and 1492 cm −1 ) and poly(methyl methacrylate) (1730 cm −1 ) without requiring conventional spectrometers. When analyte molecules fill the metasurface-generated photonic cavities, we demonstrate vibrational strong coupling between the poly(methyl methacrylate)’s carbonyl band and the CIT mode, manifested in a Rabi splitting of ~43 cm −1 . Our results establish a new photonic platform that unites spectral precision, strong field enhancement, and reconfigurability, offering diverse potential for compact mid-infrared spectroscopy, molecular sensing, and programmable polaritonic photonics.

74 ATOMIC AND MOLECULAR PHYSICS↗

DOE OSTI2024

Quantitative modeling of gate-tunable cavity exciton-polaritons in transition-metal dichalcogenides

We performed a comprehensive real-space simulation study of propagative exciton-polaritons (EPs) of tungsten disulfide (WS 2 ) inside a Fabry–Pérot cavity. Through our simulations, we were able to construct the dispersion relation and determine the propagation length (L p ) of EPs, both of which show sensitive dependence on the applied gate voltage. We found that L p increases at higher gate voltages when excited at the exciton energy but shows opposite gate dependence at the trion energy. These observations are direct evidence of the coupling between the cavity mode with excitons and trions of WS 2 . Furthermore, we demonstrate a proof-of-concept device based on the tunable cavity EPs of WS 2 , which is promising for application as photonic transistors, modulators, or electrical-to-optical converters. Furthermore, our work unveils the real-space transport properties of gate-tunable cavity EPs and paves the way for future applications of EPs in nanophotonic devices and circuits.

42 ENGINEERING↗

DOE OSTI2024

Switching of electrochemical selectivity due to plasmonic field-induced dissociation

Electrochemical reactivity is known to be dictated by the structure and composition of the electrocatalyst–electrolyte interface. Here, we show that optically generated electric fields at this interface can influence electrochemical reactivity insofar as to completely switch reaction selectivity. We study an electrocatalyst composed of gold–copper alloy nanoparticles known to be active toward the reduction of CO 2 to CO. However, under the action of highly localized electric fields generated by plasmonic excitation of the gold–copper alloy nanoparticles, water splitting becomes favored at the expense of CO 2 reduction. Real-time time-dependent density functional tight binding calculations indicate that optically generated electric fields promote transient-hole-transfer-driven dissociation of the O─H bond of water preferentially over transient-electron-driven dissociation of the C─O bond of CO 2 . These results highlight the potential of optically generated electric fields for modulating pathways, switching reactivity on/off, and even directing outcomes.

Alcorn, Francis M.↗

DOE OSTI2021

NACHOS, a CubeSat-based high-resolution UV-Visible hyperspectral imager for remote sensing of trace gases: system overview and science objectives

Here, the Nano-satellite Atmospheric Chemistry Hyperspectral Observation System (NACHOS) is a high-throughput (f/2.9), high spectral resolution (~1.3 nm optical resolution, 0.6 nm sampling) Offner-design hyperspectral imager operating in the 300-500 nm spectral region. The 1.5U instrument payload (1U optical system, 0.5U electronics module) is hosted by a 1.5U LANL-designed CubeSat bus to comprise a 3U complete satellite. Spectroscopically similar to NASA’s Ozone Monitoring Instrument (OMI), which provides wide-field global mapping of ozone and other gases at coarse spatial resolution, NACHOS fills the complementary niche of targeted measurements at much higher spatial resolution. With 350 across-track spatial pixels and a 15-degree across-track field of view, NACHOS will provide spectral imaging at roughly 0.4 km per pixel from 500 km altitude. NACHOS incorporates highly streamlined gas-retrieval algorithms for rapid onboard processing, alleviating the need to routinely downlink massive hyperspectral data cubes. We will discuss the instrument design, challenges in achieving mechanical robustness to launch vibration in such a compact instrument, the onboard calibration system, and gas-retrieval data downlink strategy. We will also discuss potential science missions, including monitoring of NO 2 as an easily detected proxy for anthropogenic fossil-fuel greenhouse gases, monitoring lowlevel SO 2 degassing at pre-eruptive volcanoes, H 2 CO from wildfires, and characterization of aerosols. The long-term vision is for a many-satellite constellation that could provide both high spatial resolution and frequent revisits for selected targets of interest. As an initial technology demonstration of this vision, the NACHOS project is currently slated to launch two CubeSats in early 2022.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2025

Hurtado summer 2025 REDWOODS PWFS code

This release includes code developed by Benjamin Gerard and Joel Hurtado in summer 2025 to model the performance of different modes of the reflective three-sided pyramid wavefront sensor instrument within the REDWOODS module of the Shane Adaptive Optics system at Lick observatory.

Gerard, BenjaminL [Lawrence Livermore National Lab↗

NASA NTRS1973

Ultraviolet proximity focussed converters for use in a satellite SEC-TV system.

Performance characteristics of Bendix type BX08025-4522 proximity-focussed vacuum-ultraviolet to visible-light image converters are presented. The converters are to be used with SEC vidicons as detectors for an echelle spectrograph on the International Ultraviolet Explorer astronomical satellite. Magnesium fluoride input windows with Cs-Te photocathodes are used in the converters, with P-11 phosphors on the fiber optic output windows. Quantum efficiencies, modulation transfer function, background, geometric distortion, and environmental test results are presented for the wavelength region from 1150 to 3500 A.-

Feibelman, W. A.↗

NASA NTRS1976

Bit error rate measurement for evaluation of a fiber optic link

Digital fiber-optic data-link terminal modules are being developed in a number of laboratories, and often the modules take the form of black boxes without convenient access to internal signals. This paper discusses types of measurements which can be made using only the digital terminals of the link. Bit-error-rate (BER) vs signal-power data can, of course, provide a means for proving overall link performance, but it can also be used to determine certain internal parameters of the receiver. The theoretical dependence of the BER-vs-light-signal-power curve shape on receiver input-noise equivalent power and comparator slicing level is discussed. BER-vs-light-signal-power measurements obtained with an experimental link are presented and interpreted with the aid of the theoretical curves. The effects of other problems, such as hum or oscillation, on the BER data are mentioned. Sensitivity of the system BER to bit rate is also discussed, with application to determining system operating limits. Since BER measurements are simple to make and can easily be automated, they may prove to be a useful means for either laboratory evaluation or production-line acceptance testing of sealed terminal modules.

Bergman, L. A.↗

NASA NTRS1978

'Smart', remote holographic processor based on the materials characteristics of LiNbO3

A class of 'Smart' remote holographic processors based on the material characteristics of LiNbO3 is introduced. The processors rely on holographic subtraction to detect differences in optical wavefronts that are spatially modulated to reflect either incoming or reference information. The state of the art of their fabrication and performance is described in the following paper. This paper outlines the principles of holography and photorefractivity that make these processors possible. Particular emphasis is placed on a potential mode of operation termed self-subtraction, in which the holographic processor is able to adapt to changes in reference information without the need for commands from an external operator.

Vahey, D. W.↗

NASA NTRS1981

Fiber optics transmit clock signal more reliably

Optical automatic gain control smooths maser clock amplitude fluctuations without phase shift. Uncomplicated optical system is more reliable than electrical transmission circuits which require phase-locked loops to compensate for shift. Maser feeds reference signal to linear fiber-optic analog transmitter which emits modulated laser beam directed to splitter. Splitter consists of dichroic mirrors and associated lenses for distributing beam to output ports. Cables attached there guide signals to receiving station.

Lutes, G. F., Jr.↗

NASA NTRS1979

Spacelab science

The Spacelab/Shuttle system will offer a new capability for investigating the earth's environment, solar-terrestrial relationships, and the physics of the solar system and beyond. Many Spacelab science and applications programs have been identified for the 1980s. These include the Solar Optical Telescope, the Chemical Release Module, a variety of materials processing facilities, the Atmospheric Cloud Physics Laboratory, and the Spacelab Infrared Telescope Facility. Experiments carried out by these payloads will range from passive observation of remote astronomical sources to in situ active probing of the earth's atmosphere and magnetosphere to the examination of the processing of materials in space.

Chappell, C. R.↗

NASA NTRS1986

A synchronization technique for optical PPM signals

A technique for maintaining synchronization between optical PPM (pulse-position modulation) pulses and a receiver clock by means of a delay-tracking loop is described and analyzed. The tracking loop is driven by a doubly stochastic Poisson process that contains information about the location of the desired slot boundaries. The slot boundaries are subject to slowly varying random delays that are ultimately tracked by the loop. The concept of fractional rms delay error is introduced to quantify the effects of signal and background induced shot noise on the performance of the delay-tracking loop.

Vilnrotter, V. A.↗

NASA NTRS1986

A synchronization technique for optical PPM signals

Vilnrotter, V. A.↗

NASA NTRS1987

Single-tone and two-tone AM-FM spectral calculations for tunable diode laser absorption spectroscopy

A generalized theory for optical heterodyne spectroscopy with phase modulated laser radiation is used which allows the calculation of signal line shapes for frequency modulation spectroscopy of Lorentzian gas absorption lines. In particular, synthetic spectral line shapes for both single-tone and two-tone modulation of lead-salt diode lasers are presented in which the contributions from both amplitude and frequency modulations are included.

Chou, Nee-Yin↗