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Cryogenic, three-terminal device yields current-voltage characteristics of ordinary transistor. Device consists of two superconducting tin rods in a crossed-wire geometry, separated by a thin gold film. New construction technique is described and possible applications are discussed.
Printed circuit board design allows for thermal stressing of the soldered joints during many thermal cycles. Components' leads should be cleaned, tinned, and freed of particles that prevent solder adherence, have a thin conformal coating, and have an air space between the coating and the body of the component.
Tin and copper provide high current and switching time capabilities for high-current resettable fuses. They show the best performance for trip current and degree of reliability, and have low coefficients of thermal expansion.
Quantitative determination of nitrogen in titanium nitride involves dissolution of TiN in 10M hydrofluoric acid containing an oxidant. Released nitrogen is determined as ammonia. Best oxidizers are ferric chloride, potassium iodate, and potassium dichromate.
Test conditions and results are reported for various coatings on a 1 percent zirconium columbium alloy at a temperature of 2000 deg F. Molybdenum silicide over molybdenum is most effective coating, tin-aluminum coating is adequately protective, chromium-molybdenum silicides are not protective.
Tensile properties of irradiated titanium, aluminum, and tin alloy at cryogenic temperature
Electron shielding and bremsstrahlung energy spectra for tin, gold, and silver
Dissociation energy of gaseous TiN molecule at high temperature
Superconducting effects on alpha particle differential energy loss in tin, vanadium, and lead superconductors
Investigation of soldered component failure in plated printed circuit boards consisting of tinned laminate copper, plated copper, and gold overplate
Electrical characteristics of thin films of tin vapor deposited on gold substrates are described. Favorable characteristics of these films include: (1) shiny and smooth finishes; (2) higher Josephson critical currents; (3) smaller electronic mean paths; and (4) consistent current-voltage curve shapes. One unfavorable characteristic is a much steeper increase of the Josephson critical current with decreasing temperature. The functional variation of the Josephson current with the control current is described. Two functional forms have been observed and a brief description as to possible mechanisms for this behavior have been included.
Fabrication of a miniature gas chromatograph column using integrated circuit technology was studied and found to be feasible. A bonding problem of forming a strong, gas tight seal between two wafers of silicon has prevented the completion of the column design. Continuing research using tin or a chromium-gold bond promises to overcome the problems of using the proposed gold-eutectic bond. Specifications for the miniature gas chromatograph column are: a spiral capillary column of semi-circular cross section, 30 micron radius, and a total length of 6.9 meters etched into a silicon structure 50 mm in diameter and 0.625 mm thick.
A summary and updating of previous work on the use of radiation chemistry for the preparation of pure materials are presented. Work was chiefly concerned with the reduction of metal salts in solution to the free metal using 2 MeV electrons. Metals deposited from aqueous solution are copper, silver, zinc, cadmium, thallium, tin, lead, antimony, iron, nickel, cobalt, and palladium. Dry organic solvents were evaluated for the deposition of metals based on a study involving deposition of antimony from soltions of antimony (III) chloride. The use of organic liquids for the preparation of anhydrous metal halides is also presented. Reaction mechanisms for both organic liquids and aqueous system are discussed.
Tin was melted in a heating assembly secured to the arm of a centrifuge. The furnace was allowed to pivot and reach its equilibrium angle of swing for the gravity force being experienced. The crucible was cooled during rotation to allow the growth of single crystals. The crystals were etched for the purpose of observing the growth striations. Slices were removed from some of the crystals to permit observation of the striations in the interior. Visual analyses were made with a scanning electron microscope. Preliminary conclusions relating the appearance of the striations to gravity forces and the affected growth mechanisms are presented. Further experiments that will verify these conclusions and determine other gravity effects are proposed.
The authors have identified the following significant results. As a precursor to the ERTS-1 investigation, the spatial relationship of geostructures seen on Nimbus IDCS photographs to the distribution of mineralized areas in Alaska and western Canada was analyzed to determine the possible metallogenic significance of the geostructures. In Canada, mercury and porphyry molybdenum deposits are closely associated with strong northwest-trending fault systems; the development of mineralized regions seems related to major crustal zones or fractures trending southwestward across the Cordillera from the Precambrian shield. In Alaska, comparison of the northeast- and northwest-trending set of possible crustal structures shown on the Nimbus photo, with the distribution of known mineral deposits suggests a similar relationship. The mineralized region of massive sulfides in Prince William Sound and upper Copper River areas and of porphyry coppers in the Nabesna area forms a broad northeast-trending belt possibly related to the Minto Arch on the Shield. The belt of metalliferous deposits in the western Alaska Range follows a comparable northeast trend. Mercury deposits, suggested by many to be fault-controlled, together with most tin and tungsten deposits, occupy a northeast-trending belt between the Bristol Bay-Mackenzie Bay linear and extensions of a linear along the lower Yukon River. This belt intersects the northwest-trending Canadian belt of similar deposits in the Fairbanks area.
An experimental study of superconductor stabilization has resulted in the successful application of the concepts of filamentary structure and conductor twist to Nb3Sn ribbon. The Nb3Sn is formed in parallel, helical paths, which are continuous around the ribbon. Short lengths (12-18cm) of 1.27 cm wide superconductive ribbon were produced. The filamentary and twist characteristics are incorporated in the ribbon by means of an inert mask formed on the ribbon surface early in the fabrication process. Diffusion reaction of the niobium and tin is prevented at the filament boundaries. Described are the conductor methods of fabrication, and test results obtained. The technology required to adapt the processes for the production of long lengths of ribbon is available.
The parameter values measured are in agreement with those reported by Mazelsky and Lubell (1963) and data of Bis and Dixon (1969). The measurements for SnTe introduce a large amount of data into a defect model analysis that shows that the ratio of the number of holes per tin-vacancy acceptor to the 77 K Hall factor is independent of the apparent hole concentration. The measurements reveal some interesting problems in handling the Sn-rich alloys in fine powder form due to the uptake of oxygen.
The quantum-interference technique developed by Meservey (1965) is used to measure directly the absolute value of the penetration depth in lead in tin superconducting thin films. The technique assumes that the change in phase of the superconducting wave function around any contour within the superconductor must be 2 pi n, where n is a nonnegative integer. Results show that the critical current of a superconducting interferometer with two parallel junctions is not strictly periodic in the applied magnetic flux with a period equal to the flux quantum because of the magnetic field dependence of the critical currents of the junctions.