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At least 991 records · Page 55
All sourcesNASA NTRSDOE OSTI
DOE OSTI2023

Evaluation of Electron Tomography Capabilities for Shale Imaging

Despite the advantageous resolution of electron tomography (ET), reconstruction of three-dimensional (3D) images from multiple two-dimensional (2D) projections presents several challenges, including small signal-to-noise ratios, and a limited projection range. This study evaluates the capabilities of ET for thin sections of shale, a complex nanoporous medium. A numerical phantom with 1.24 nm pixel size is constructed based on the tomographic reconstruction of a Barnett shale. A dataset of 2D projection images is numerically generated from the 3D phantom and studied over a range of conditions. First, common reconstruction techniques are used to reconstruct the shale structure. The reconstruction uncertainty is quantified by comparing overall values of storage and transport metrics, as well as the misclassification of pore voxels compared to the phantom. We then select the most robust reconstruction technique and we vary the acquisition conditions to quantify the effect of artifacts. We find a strong agreement for large pores over the different acquisition workflows, while a wider variability exists for nanometer-scale features. Furthermore, the limited projection range and reconstruction are identified as the main experimental bottlenecks, thereby suggesting that sample thinning, advanced holders, and advanced reconstruction algorithms offer opportunities for improvement.

3D scanning transmission electron microscopy↗
DOE OSTI2023

Learning heterogeneous reaction kinetics from X-ray videos pixel by pixel

Reaction rates at spatially heterogeneous, unstable interfaces are notoriously difficult to quantify, yet are essential in engineering many chemical systems, such as batteries and electrocatalysts. Experimental characterizations of such materials by operando microscopy produce rich image datasets, but data-driven methods to learn physics from these images are still lacking because of the complex coupling of reaction kinetics, surface chemistry and phase separation. Here we show that heterogeneous reaction kinetics can be learned from in situ scanning transmission X-ray microscopy (STXM) images of carbon-coated lithium iron phosphate (LFP) nanoparticles. Combining a large dataset of STXM images with a thermodynamically consistent electrochemical phase-field model, partial differential equation (PDE)-constrained optimization and uncertainty quantification, we extract the free-energy landscape and reaction kinetics and verify their consistency with theoretical models. We also simultaneously learn the spatial heterogeneity of the reaction rate, which closely matches the carbon-coating thickness profiles obtained through Auger electron microscopy (AEM). Across 180,000 image pixels, the mean discrepancy with the learned model is remarkably small (<7%) and comparable with experimental noise. Our results open the possibility of learning nonequilibrium material properties beyond the reach of traditional experimental methods and offer a new non-destructive technique for characterizing and optimizing heterogeneous reactive surfaces.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2023

Binary pseudo-random array (BPRA) for inspection and calibration for cylindrical wavefront interferometry

High-accuracy metrology is vitally important in manufacturing ultra-high-quality free-form mirrors designed to manipulate X-ray light with nanometer-scale wavelengths. However, surface topography measurements are instrument dependent, and without the knowledge of how the instrument performs under the practical usage conditions, the measured data contain some degree of uncertainty. Binary Pseudo Random Array (BPRA) “white noise” artifact are effective and useful for characterizing the Instrument Transfer Function (ITF) of surface topography metrology tools and wavefront measurement instrument. BPRA artifact contains features with all spatial frequencies in the instrument bandpass with equal weight. As a result, power spectral density of the patterns has a deterministic white-noise-like character that allows direct determination of the ITF with uniform sensitivity over the entire spatial frequency range. The application examples include electron microscopes, x-ray microscopes, interferometric microscopes, and large field-of-view Fizeau Interferometers. Furthermore, we will introduce the application of BPRA method to characterizing the ITF of Cylindrical Wavefront Interferometry (CWI), by developing the BPRA artifact which matches the radius of curvature of the cylindrical wavefront. The data acquisition and analysis procedures for different applications of the ITF calibration technique developed are also discussed.

Munechika, K↗
NASA NTRS1977

A region of intense plasma wave turbulence on auroral field lines

Plasma wave measurements from the Hawkeye 1 and Imp 6 satellites show that a region of intense plasma wave turbulence occurs on high-latitude auroral field lines at altitudes ranging from a few thousand kilometers in the ionosphere to greater than 40 R-E in the distant magnetotail. Two distinct components are evident in the spectrum of this turbulence: (1) an intense quasi-electrostatic component called broadband electrostatic noise and (2) a weak whistler mode electromagnetic component called magnetic noise bursts. It is suggested that the plasma wave turbulence occurs on magnetic field lines which connect with regions of intense inverted V electron precipitation at low altitudes and with regions of intense earthward plasma flow in the distant magnetotail.

Gurnett, D. A.↗
NASA NTRS1977

Self-scanned anode array with a microchannel plate electron multiplier - The SSANACON

A photoelectron counting detector utilizing a 128-element linear self-scanned anode array to collect the output of a dual microchannel plate electron multiplier is described. The operation of the detector, its spatial resolution and detection efficiency, and radiation behavior are discussed. The low-noise detector was developed for the Mariner Jupiter/Saturn mission UV spectrometer, and offers a large dynamic range and count rate of 0.003 per anode-sec. It can measure simultaneously two spatially separated signals differing by more than six orders of magnitude in count rate.

Broadfoot, A. L.↗
NASA NTRS1988

An electronically tuned, stable 8415-MHz dielectric resonator FET oscillator for space applications

A voltage-controlled 8415 MHz FET oscillator stabilized by a dielectric resonator is described. The oscillator provides a linear electronic tuning range of over 3.2 MHz with a flat power output equal to +1.8 dBm (27 C nominal), a single-sideband noise to carrier ratio of -68 dBc/Hz at 1 kHz off carrier, and a frequency temperature coefficient of 0.54 part per million/C over a -24 to 75 C range. The oscillator withstood 150 krads(Si) of gamma radiation with no significant performance degradation. The overall performance of the oscillator is in many ways far superior to that of an equivalent bipolar oscillator for space applications.

Lakshminarayana, M.↗
NASA NTRS1992

High bandwidth electro-optic technology for intersatellite optical communications

The research and development of electronic and electro-optic components for geosynchronous and low earth orbiting satellite optical high bandwidth communications at the NASA-Goddard Space Flight Center is reviewed. Intersatellite optical communications retains a strong reliance on microwave circuit technology in several areas - the microwave to optical interface, the laser transmitter modulation driver and the optical receiver. A microwave to optical interface is described requiring high bandwidth electronic downconverters and demodulators. Electrical bandwidth and current drive requirements for the laser modulation driver for three laser alternatives are discussed. Bandwidth and noise requirements are presented for optical receiver architectures.

Krainak, Michael A.↗
NASA NTRS1999

Coherent Doppler Wind Lidar Technology for Space Based Wind Measurements Including SPARCLE

It has been over 30 years since coherent lidar systems first measured wind velocity, and over 20 years since the "ultimate application" of measuring Earth's winds from space was conceived. Coherent or heterodyne optical detection involves the combination (or mixing) of the returned optical field with a local oscillator (LO) laser's optical field on the optical detector. This detection technique yields the benefits of dramatically improved signal-to-noise ratios; insensitivity to detector noise, background light and multiply scattered light; reduction of the returned signal's dynamic range; and preservation of the optical signal spectrum for electronic and computer processing. (Note that lidar systems are also referred to as optical radar, laser radar, and LADAR systems.) Many individuals, agencies, and countries have pursued the goal of space-based wind measurements through technology development, experiments, field campaigns and studies.

Kavaya, Michael J.↗
NASA NTRS1999

Electrical Properties and Power Considerations of a Piezoelectric Actuator

This paper assesses the electrical characteristics of piezoelectric wafers for use in aeronautical applications such as active noise control in aircraft. Determination of capacitive behavior and power consumption is necessary to optimize the system configuration and to design efficient driving electronics. Empirical relations are developed from experimental data to predict the capacitance and loss tangent of a PZT5A ceramic as nonlinear functions of both applied peak voltage and driving frequency. Power consumed by the PZT is the rate of energy required to excite the piezoelectric system along with power dissipated due to dielectric loss and mechanical and structural damping. Overall power consumption is thus quantified as a function of peak applied voltage and driving frequency. It was demonstrated that by incorporating the variation of capacitance and power loss with voltage and frequency, satisfactory estimates of power requirements can be obtained. These relations allow general guidelines in selection and application of piezoelectric actuators and driving electronics for active control applications.

Jordan, T.↗
NASA NTRS2006

A compact 600 GHz electronically tunable vector measurement system for submillimeter wave imaging

A compact submillimeter wave transmission/reflection measurement system has been demonstrated at 560-635 GHz, with electronic tuning over the entire band. Maximum dynamic range measured at a single frequency is 100 dB (60 dB typical), and typical phase noise is less than +/- 1°. By using a frequency steerable lens at the source output and mixer input, the frequency agility of the system can be used to scan the source and receive beams, resulting in near realtime imaging capability using only a single pixel

Siegel, Peter H.↗
NASA NTRS2021

On-Orbit Calibration and Performance Assessments of Terra and Aqua Modis Thermal Emissive Bands

Terra and Aqua MODIS have successfully operated for more than 20 and 18 years, respectively, and far exceeded their designed lifetimes of 6 years. MODIS has 36 spectral bands, among which 16 are the thermal emissive bands (TEB) covering a wavelength range from 3.75 to 14.24 μm. Observations from the MODIS TEB have been used to generate a number of data products, such as surface/cloud/atmospheric temperatures, cloud top altitude, and water vapor properties. To a large extent, the quality of the MODIS L1B radiance product has been maintained through the entirety of each mission via extensive on-orbit calibration and validation efforts. MODIS TEB calibration uses a quadratic algorithm and is referenced to an on-board blackbody with its temperature measurements traceable to the NIST standard. We provide an overview of the MODIS instrument operations, key TEB calibration activities, and algorithms used in the latest L1B data Collection 6.1 (C6.1) and describe the TEB on-orbit performance for both Terra and Aqua MODIS. The TEB gain trends have been stable to within 5% over the Terra mission after 2003 under the same electronic configuration, except for bands 27 to 30, and within 3% over the Aqua mission. The Terra MODIS optical crosstalk correction implemented right after launch has been very effective in removing the ghost images in its photoconductive detector bands 32 to 36. Starting from C6.1, an electronic crosstalk correction algorithm has also been applied to the Terra MODIS photovoltaic detector long-wave infrared bands 27 to 30. The noise characterization performance remains stable with most TEB detectors continuously meeting their design requirements. A gradual loss of the Aqua MODIS radiative cooler margin reached its maximum in 2013 and has been slowly recovering since then. On-orbit changes in TEB response versus scan angle are extremely small based on pitch maneuver observations and assessments using vicarious approaches. The remaining challenges in TEB calibration and proposed improvements for the upcoming data collection with L1B data production and reprocessing are discussed.

Terra↗
DOE OSTI2023

Learning heterogeneous reaction kinetics from X-ray movies pixel-by-pixel

Reaction rates at spatially heterogeneous, unstable interfaces are notoriously difficult to quantify, yet are essential in engineering many chemical systems, such as batteries 1 and electrocatalysts 2. Experimental characterizations of such materials by operando microscopy produce rich image datasets 3–6, but data-driven methods to learn physics from these images are still lacking because of the complex coupling of reaction kinetics, surface chemistry and phase separation 7. Here we show that heterogeneous reaction kinetics can be learned from in situ scanning transmission X-ray microscopy (STXM) images of carbon-coated lithium iron phosphate (LFP) nanoparticles. Combining a large dataset of STXM images with a thermodynamically consistent electrochemical phase-field model, partial differential equation (PDE)-constrained optimization and uncertainty quantification, we extract the free-energy landscape and reaction kinetics and verify their consistency with theoretical models. We also simultaneously learn the spatial heterogeneity of the reaction rate, which closely matches the carbon-coating thickness profiles obtained through Auger electron microscopy (AEM). Across 180,000 image pixels, the mean discrepancy with the learned model is remarkably small (<7%) and comparable with experimental noise. Our results open the possibility of learning nonequilibrium material properties beyond the reach of traditional experimental methods and offer a new non-destructive technique for characterizing and optimizing heterogeneous reactive surfaces.

Chueh, William↗
NASA NTRS1995

16 Infrared Hot Electron Transistor

Very long wavelength infrared (VWIR) photodetectors, 14 20 , are of a great interest for variety of space-borne applications. These space applications have placed stringent requirements on the performance of the infrared detectors and arrays including high detectivity, low dark current, uniformity, radiation hardness and lower power dissipation. I will discuss the development and progress of AlxGal- xAs/GaAs VWIR quantum well infrared photodetectors (QWIPs) to meet those stringent requirements and the demonstration of a 15 128x128 QWIP focal plane array camera. The noise equivalent temperature difference of the focal plane array is 30 mK at 300 K background, and operating temperature is 45 K.

Electron Transistor↗
NASA NTRS2010

EPR Imaging at a Few Megahertz Using SQUID Detectors

An apparatus being developed for electron paramagnetic resonance (EPR) imaging operates in the resonance-frequency range of about 1 to 2 MHz well below the microwave frequencies used in conventional EPR. Until now, in order to obtain sufficient signal-to-noise radios (SNRs) in conventional EPR, it has been necessary to place both detectors and objects to be imaged inside resonant microwave cavities. EPR imaging has much in common with magnetic resonance imaging (MRI), which is described briefly in the immediately preceding article. In EPR imaging as in MRI, one applies a magnetic pulse to make magnetic moments (in this case, of electrons) precess in an applied magnetic field having a known gradient. The magnetic moments precess at a resonance frequency proportional to the strength of the local magnetic field. One detects the decaying resonance-frequency magnetic- field component associated with the precession. Position is encoded by use of the known relationship between the resonance frequency and the position dependence of the magnetic field. EPR imaging has recently been recognized as an important tool for non-invasive, in vivo imaging of free radicals and reduction/oxidization metabolism. However, for in vivo EPR imaging of humans and large animals, the conventional approach is not suitable because (1) it is difficult to design and construct resonant cavities large enough and having the required shapes; (2) motion, including respiration and heartbeat, can alter the resonance frequency; and (3) most microwave energy is absorbed in the first few centimeters of tissue depth, thereby potentially endangering the subject and making it impossible to obtain adequate signal strength for imaging at greater depth. To obtain greater penetration depth, prevent injury to the subject, and avoid the difficulties associated with resonant cavities, it is necessary to use lower resonance frequencies. An additional advantage of using lower resonance frequencies is that one can use weaker applied magnetic fields: For example, for a resonance frequency of 1.4 MHz, one needs a magnetic flux density of 0.5 Gauss approximately the flux density of the natural magnetic field of the Earth.

Hahn, Inseob↗
NASA NTRS2014

Aeroacoustics of Space Vehicles

While for airplanes the subject of aeroacoustics is associated with community noise, for space vehicles it is associated with vibro-acoustics and structural dynamics. Surface pressure fluctuations encountered during launch and travel through lower part of the atmosphere create intense vibro-acoustics environment for the payload, electronics, navigational equipment, and a large number of subsystems. All of these components have to be designed and tested for flight-certification. This presentation will cover all three major sources encountered in manned and unmanned space vehicles: launch acoustics, ascent acoustics and abort acoustics. Launch pads employ elaborate acoustic suppression systems to mitigate the ignition pressure waves and rocket plume generated noise during the early part of the liftoff. Recently we have used large microphone arrays to identify the noise sources during liftoff and found that the standard model by Eldred and Jones (NASA SP-8072) to be grossly inadequate. As the vehicle speeds up and reaches transonic speed in relatively denser part of the atmosphere, various shock waves and flow separation events create unsteady pressure fluctuations that can lead to high vibration environment, and occasional coupling with the structural modes, which may lead to buffet. Examples of wind tunnel tests and computational simulations to optimize the outer mold line to quantify and reduce the surface pressure fluctuations will be presented. Finally, a manned space vehicle needs to be designed for crew safety during malfunctioning of the primary rocket vehicle. This brings the subject of acoustic environment during abort. For NASAs Multi-Purpose Crew Vehicle (MPCV), abort will be performed by lighting rocket motors atop the crew module. The severe aeroacoustics environments during various abort scenarios were measured for the first time by using hot helium to simulate rocket plumes in the Ames unitary plan wind tunnels. Various considerations used for the helium simulation and the final confirmation from a flight test will be presented.

launch vehicle↗
NASA NTRS1995

Sequences of correlated hard X-ray and type III bursts during solar flares

Acceleration and injection of electron beams in solar flares can be traced from radio type III (or type U) bursts and correlated hard X-ray pulses with similar timescales and nonthermal spectra. We perform a systematic survey of such correlated radio and hard X-ray (HXR) pulses with timescales of less than or approximately 2 s in flares simultaneously observed with the radio spectrometer Ikarus and the Hard X-Ray Burst Spectrometer (HXRBS) on solar maximum mission (SMM). We applied an epoch-folding technique to enhance correlated time patterns in burst sequences at the two wavelengths. We present the results from the strongest (10) flares with a HXRBS count rate greater than or = 3000 counts/s, which have a satisfactory signal-to-noise ratio for subsecond pulses. The major findings of this study are presented. These observations strongly suggest that particle acceleration in solar flares occurs in a pulsed mode where electron beams are simultaneously injected in upward and downward directions. Since the sequences of correlated HXR and radio bursts show identical durations and intervals at the two wavelengths, they are believed to reflect most directly the temporal dynamics of the underlying common accelerator. As a consequence, thick-target models should be reconsidered under the aspect of electron injection with pulse durations of 0.2-2.0 s and duty cycles of approximately = 50%.

Aschwanden, Markus J.↗
DOE OSTI2026

Startup regime of high-efficiency tapering-enhanced FEL oscillator

In this paper, we present a design of a high-efficiency high-gain free-electron laser oscillator based on the use of a strongly tapered undulator for extracting energy from high-brightness electron beams. We provide an analytical model of the setup followed by numerical simulations for lasing at the wavelength of 13.5 nm. We discuss the optimization of the system in steady state and the conditions necessary for the pass-per-pass buildup of the power from shot noise level. We propose the use of fast phase shifters as a way to accelerate the buildup. Finally, we present time-dependent simulations of the oscillator and discuss the role of spectral filtering. The optimized working point yields a total energy conversion efficiency from the electron beam to output radiation above 1% at the wavelength of 13.5 nm.

Beam dynamics↗
DOE OSTI2023

TEAMER - Acoustic Particle Velocity Measurements - CRADA 601 (Abstract)

With relatively few deployments of tidal turbines, the extent and effect of underwater sounds generated from these turbines is not well understood. The University of Washington (UW) is deploying a cross-flow turbine system, the Turbine Lander, in the entrance channel to Sequim Bay. The deployment of this system provides an opportunity to understand the noise radiated by the turbine and its sources. There are three hypothesized sound sources associated with operation of the turbine: 1) a continuous tone associated with energized power electronics; 2) sound associated with the generator when the turbine is rotating; and 3) sound associated with the bearing pack that supports the rotor. PNNL is collaborating with UW and Integral Consulting Inc. (Integral) to simultaneously measure sound sources using three different devices. The NoiseSpotter®, an acoustic sensor system designed by Integral, measures acoustic pressure and a three-dimensional particle velocity vector. The NoiseSpotter, along with a commercial-off-the-shelf acoustic particle motion and pressure sensor (M20-105, Geospectrum Technologies Inc.) owned by PNNL will be deployed on the seabed approximately 50-100 m from the Turbine Lander. UW will concurrently deploy Drifting Acoustic Instrumentation SYstems (DAISYs) to characterize acoustic pressure near the Turbine Lander and localize sounds using a Time Delay of Arrival (TDOA) algorithm. Integral, UW, and PNNL will collaborate on data analysis and interpretation, with the intention of jointly authoring an archival paper on the results. The noise generated from the Turbine Lander is not expected to be significant, yet this experiment will help to evaluate the efficacy of combining technologies to characterize noise and provide insights for approaches to consider for future turbine deployments at other locations.

16 TIDAL AND WAVE POWER↗