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DOE OSTI2021

End-to-End Simulations of a 3.4-Meter Detector Wall for Neutron-Diagnosed Subcritical Experiments

The Nevada National Security Site, together with Los Alamos National Laboratory and Lawrence Livermore National Laboratory, is developing a novel diagnostic to measure the reactivity of subcritical experiments. This capability is known as neutron-diagnosed subcritical experiments. The decay of the fission gamma rays from the neutron-interrogated subcritical experiment is measured as a function of time with a large (~3-meter diameter) detector wall consisting of 151 individual detector pixels. The data from this current mode measurement inform the neutron multiplication factor, keff, and thus the relative reactivity of the subcritical experiment. The Nevada National Security Site developed the Gamma Array Simulation Toolkit initially to help inform the design of the individual detector pixels and the 3.4-meter diameter detector wall to be fielded as part of neutron-diagnosed subcritical experiments. This toolkit is now being used to simulate and predict the performance of the final design of the individual detector pixels and the aggregate detector wall. Key detector characteristics evaluated from these simulations include impulse response, pulse height spectrum, number of photoelectrons per MeV, detector efficiency, and cross talk between detector pixels. Collectively, the results of these simulations inform how well the fission gamma ray die-off distribution from a neutron-diagnosed subcritical experiment measurement can be resolved. This is critical to determining the relative reactivity of the experiment. Furthermore, the Gamma Array Simulation Toolkit can be used to aid in the analysis of the experimental data from a neutrondiagnosed subcritical experiment measurement once the simulation has been benchmarked.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2021

System, algorithm, and method using short pulse interrogation with neutrons to detect and identify matter

A system, method, and algorithm for detecting and identifying special nuclear material (SNM) (including fissionable material), explosives, or drugs is disclosed. This material detection system relies on active interrogation of material using a short, intense neutron pulse, and characterization of the resulting prompt gamma response in two short time windows, the first concurrent with and the second immediately following the end of the neutron pulse, optionally subject to a total transit delay time of the neutrons from the neutron source to the target and from the target to the gamma detector. A high data rate analysis system implements data stream analysis and statistical correlations of the two short time window gamma responses to rapidly detect or identify SNM, explosives, or drugs. The duration of the neutron pulse is so short that minimal dose results. Various shields help to minimize the background signal falling on the gamma detector to improve sensitivity.

Derzon, Mark S.↗

DOE OSTI2020

The Accelerator Neutrino Neutron InteractionExperiment: Design, Construction and Preparationfor First Physics

This thesis covers work performed for the Accelerator Neutrino Neutron Interaction Experiment (ANNIE) between 2015 and 2020. ANNIE is a beamline neutrino experiment located at the Fermi National Accelerator Laboratory in Chicago. Its primary physics goals are the measurement of neutrino interaction cross-sections on oxygen, and a measurement of the multiplicity of final state neutrons from these interactions, both as functions of final state kinematics. In order to achieve these goals ANNIE will be pioneering the use of Large Area Picosecond Photodetectors and the use of gadolinium doping to enhance neutron visibility in a water Cherenkov detector. Over the time period of this thesis the ANNIE detector was constructed, an initial 'Phase I' background run was completed, the detector was decommissioned and then substantially upgraded in preparation for the main 'Phase II' physics run. At the time of writing ANNIE is being re-commissioned, with Phase II data taking anticipated to begin in 2021. During this time I spent 21/2 years on-site contributing to almost all aspects of hardware work, while performing software development for the simulation and analysis frameworks. As my first software task I developed Monte Carlo simulations of the detector response, based on the WCSim framework. While thismore » framework provided a starting point for the tank simulation significant modifications were required to implement the complete ANNIE detector system. This included a rewrite of the geometry, along with modifications to the photosensor definitions, hit collections, digitization, triggering, input and output interfaces, etc. To take advantage of improved modelling of neutrons in Geant4.10 the physics lists were also reimplemented in the new version format. As part of this work I determined performance metrics based on the output files, calculating kinematic acceptance, detector efficiency and expected event rates. My contributions on reconstruction focused primarily on the MRD, for which I implemented two track reconstruction algorithms, specialised for high and low energy muons. The high energy algorithm achieves >90% efficiency for tracks with at least 8 hits, and is robust against dead paddles and unrelated hits. The low energy algorithm performs a search in combination with tank information to provide sensitivity down to a single MRD hit. Early data handling work for the Phase I background run included writing the code for handling TDC hits and performing studies on neutron detection without the requirement of multi-hit coincidence. As the collaboration moved to a new framework for the Phase II analysis I performed a substantial amount of work to develop the codebase, implementing tools to perform tasks such as file IO, data parsing, waveform processing, event building, timestamp alignment, time clustering, hit residual calculation, event visualisation etc. I helped develop the python API for integrating multi-language tools, and ported the framework into a Singularity container to provide a self-contained environment that…« less

43 PARTICLE ACCELERATORS↗

DOE OSTI2023

Interactive automated Bragg peak identification with 3D neutron scattering data

Neutron scattering experiments have undergone significant technological development through large area detectors with concurrent enhancements in neutron transport and electronic functionality. Data collected for neutron events include detector pixel location in 3D, time and associated metadata, such as, sample orientation, neutron wavelength, and environmental conditions. RadiaSoft and Oak Ridge National Laboratory personnel are considering single-crystal diffraction data from the TOPAZ instrument. We are leveraging a new method for rapid, interactive analysis of neutron data using NVIDIA’s IndeX 3D volumetric visualization framework. We have implemented machine learning techniques to automatically identify Bragg peaks and separate them from diffuse backgrounds and analyze the crystalline lattice parameters for further analysis. The implementation of automatic peak identification into IndeX allows scientists to visualize and analyze data in real-time. Our methods include a robust comparison with current analysis techniques which show improvement in a variety of aspects. These improvements will be incorporated into IndeX for visualization to allow scientists an interactive tool for crystal analysis.

Kilpatrick, Matthew↗

DOE OSTI2024

Overview of Shielding Analyses at Oak Ridge National Laboratory’s Spallation Neutron Source Second Target Station

The Neutronics Group of the Second Target Station project at Oak Ridge National Laboratory is responsible for all neutronics analyses related to design and construction. This paper provides an overview of four neutronics analyses performed for the Second Target Station project, which is representative of all the ongoing work but especially tasks related to shielding. These analyses extend from the proton accelerator through the target monolith and bunker to the end of a neutron beamline. Each example highlights the tools and methods the Neutronics Group uses for analysis. The primary tool is the Monte Carlo radiation transport code MCNP 6.2, but this is augmented by other codes that supplement the input of MCNP. The other codes specifically highlighted in this paper include Attila4MC, ADVANTG, and AARE.

Miller, Thomas↗

DOE OSTI2024

Photoneutron Production Using an Electron Linear Accelerator for Applications in Neutron Imaging

Photoneutron production is possible using an electron linear accelerator and a target capable of generating photonuclear reactions. A short pulse neutron source can be useful for neutron imaging dynamic experiments. This study is aimed at the feasibility of photoneutron production using a 20 MeV electron linear accelerator and tungsten and depleted uranium targets of various thicknesses. MCNP6 (Monte Carlo N-Particle) code will be used to develop a computational model to estimate total neutron yield, and this will be verified at the Idaho State University’s Accelerator Center. After verification of the neutron yield and energy spectra, an additional MCNP6 model will be developed to analyze the neutron imaging processes. This study will potentially prove it is possible to conduct multi-mode imaging experiments on the anticipated Scorpius electron linear accelerator at the Nevada National Security Sites.

43 PARTICLE ACCELERATORS↗

DOE OSTI2024

MEASUREMENT OF THE NEUTRON FLUENCE-RATES IN THE ADVANCED TEST REACTOR

The axial neutron fluence-rate distribution at the Advanced Test Reactor (ATR) is determined using a combination of pure nickel and cobalt-aluminium alloy dosimeter wires. Most irradiation programs at ATR need to know the fast neutron fluence-rate surrounding their experiment to correlate post-irradiation examination results with neutron dose. The activated dosimeter wires, which extend beyond the full fuelled region of the reactor core, are highly radioactive following the full cycle in ATR and must therefore be measured in the ATR canal. The system that is employed for these measurements is mechanical scanning mechanism is used to scan the activated wires across the face of a columnated shield and a NaI detector. This detector is not sufficiently calibrated to provide absolute activity measurements, therefore, the count-rate is recorded and normalized to the highest activity for that wire. Then, an approximately 3-mm long portion of the wire is removed from the highest activity region in the wire. The wires are then transferred, and an absolute activity measurement is made using a calibrated ionization chamber. These measurements are combined with corrections for decay, neutron energy spectrum, burnup, dosimeter composition, reactor power fluctuations, and reactor outages to determine the average axial neutron fluence-rate at various locations within ATR during the cycle.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

DOE OSTI2024

Precise Measurement of the Neutron Magnetic Form Factor Using Super-BigBite Spectrometer at Jefferson Lab

The GMn experiment (E12-09-019) was conducted at Jefferson Laboratory from late 2021 into early 2022. The goal was to make high-precision measurement of the neutron’s magnetic form factor (GMn) at multiple kinematic points, including Q2 = 3.5, 4.5, 6.5, 8.5, 10, 12, 13.5, 16, and 18 (GeV/c)2. Limited data exist for GMn in the region up to about Q2 = 10 (GeV/c)2, with existing data having large systematic uncertainty. In this experiment, the ratio method was employed to reduce systematic uncertainty by measuring the ratio of neutron and proton yields. The experiment took place at Jefferson Laboratory in Hall A, where the BigBite spectrometer was used to detect the scattered electrons, while the HCal in the SuperBigbite spectrometer was used to detect both neutrons and protons. The protons were deflected slightly upwards with the use of a large-aperture dipole magnet named BigBen, allowing for enhanced particle identification. Extraction of GMn requires taking the ratio of proton and neutron yields. Analysis efforts are still currently underway to refine corrections to the data, including detector efficiencies, radiative corrections, neutron and proton mass identification, and charge exchange.

Lashley-Colthirst, Nathaniel↗

DOE OSTI2025

Search for Neutron-Antineutron Transition in Large Neutrino Detectors

Neutron-antineutron transition is a baryon number violation process with $\Delta B=2$, providing a unique insight into the potential explanation of the baryon asymmetry in our university, especially in the context of post-sphaleron baryogenesis. Studies have been conducted in various neutron-rich environment including free neutron sources, neutron stars, and bound neutrons in large neutrino detectors, among which the large neutrino experiments obtained the most stringent constraints.

Wan, Linyan [Fermilab] (ORCID:0000000155246137)↗

DOE OSTI2026

Primordial Neutron Stars

We propose a novel cosmological scenario in which baryonic neutron stars could plausibly form in the early universe. If baryogenesis initially produces an excessively-large baryon asymmetry, $Y_B \gg 10^{-10},$ the baryonic mass inside the horizon can exceed the minimum neutron star mass before big bang nucleosynthesis (BBN). While this large asymmetry is present, non-relativistic baryons can dominate the universe and enhanced density perturbations on small scales can gravitationally collapse Hubble patches shortly after horizon re-entry. For some initial perturbations, just below the threshold for black hole formation, this collapse will be arrested only by nuclear pressure, possibly resulting in neutron star formation. Afterwards, there must be a large entropy injection to restore the observed baryon asymmetry, $Y_B \sim 10^{-10}$, and preserve the successful predictions of standard BBN. Unlike neutron stars that form from stellar collapse, primordial neutron stars can, in principle, be as light as $\sim 0.1 M_\odot$, limited only by the nuclear equation of state.

Krnjaic, Gordan [Fermilab; Chicago U., Astron. Ast↗

DOE OSTI2026

Measuring the neutrino-oxygen neutral current quasielastic cross section using the accelerator neutrino neutron interaction experiment

The Accelerator Neutrino Neutron Interaction Experiment (ANNIE) is a 26-ton gadolinium-doped water Cherenkov detector located on-axis to Fermilab’s Booster Neutrino Beam (BNB). ANNIE is uniquely positioned to perform high-statistics measurements of neutrino-nucleus interactions in water, benefiting from a large neutrino flux due to a short (100-meter) baseline. A central focus of ANNIE’s physics program is the measurement of both charged current (CC) and neutral current (NC) cross sections on water, including neutral current quasielastic (NCQE) and CC-inclusive channels. The NCQE measurement is particularly critical for constraining uncertainties in rare-event searches such as the Diffuse Supernova Neutrino Background (DSNB), where atmospheric $\nu$NCQE interactions constitute a significant and poorly constrained background. This dissertation presents a measurement of the flux-averaged neutrino-oxygen neutral current quasielastic ($\nu$NCQE) cross section using $2.573 \times 10^{20}$~POT of BNB exposure from the 2022 and 2023 beam years. The $\nu$NCQE interaction is identified through the primary $\gamma$-rays produced by nuclear de-excitation of the residual $^{15}$N$^*$ or $^{15}$O$^*$ nucleus following nucleon knockout from $^{16}$O. A dedicated Monte Carlo (MC) re-tuning campaign was conducted using an americium-beryllium (AmBe) calibration source, Michel electrons from stopped muons, and throughgoing dirt muons originating upstream of the detector. This multi-sample approach provided a wide-ranging $\mathcal{O}(\text{MeV})$--$\mathcal{O}(\text{GeV})$ dataset for tuning the simulated detector response, which was subsequently validated against AmBe neutron and Michel electron data for use in the $\nu$NCQE analysis. A dedicated laser calibration campaign was carried out to reduce timing uncertainties across the PMT system, enabling reconstruction of the BNB bunch substructure with sufficient resolution to serve as a background rejection tool. By selecting events in-time with individual neutrino bunches, beam-correlated $\nu$NCQE events are separated from diffuse and accelerator-induced backgrounds, notably skyshine neutrons and externally-originating events, that would otherwise dominate traditional charge-based selections within a small-scale, surface-level, short-baseline detector. A data-driven estimation of the skyshine neutron and external background rates was performed and incorporated into the systematic uncertainty budget. The flux-averaged $\nu$NCQE cross section on oxygen is measured to be $1.57 \pm 0.06\,(\text{stat.})$ $^{+0.91}_{-0.67}\,(\text{syst.})$ $\times 10^{-38}\ \text{cm}^{2}$. A full systematic budget is constructed by propagating uncertainties in the secondary hadronic interaction modeling, background cross section normalizations, detector response, neutrino flux, and the primary $\gamma$-ray emission probabilities from oxygen nuclear de-excitation. An idealized de-excitation model, constructed from existing measurements in the literature is developed to benchmark the predictions of the \textsc{GENIE} event generator. A comparison reveals that \textsc{GENIE} systematically overpredicts the primary $\gamma$-ray emission probability from oxygen de-excitation by a factor of $1.49\times$ for $E_\gamma > 6$~MeV and $3.07\times$ in the $3$--$6$~MeV band. This comparison motivates the dominant systematic uncertainty in this analysis, where a conservative uncertainty of $^{+39.9\%}_{-0\%}$ on the primary $\gamma$-ray signal prediction is assigned. The ANNIE result is consistent with and complementary to existing flux-averaged $\nu$NCQE cross section measurements from T2K and Super-Kamiokande, providing an independent measurement with a different detector, neutrino beam, and analysis methodology. Looking ahead, an upgrade to the ANNIE DAQ infrastructure enabling continuous extended readout will allow a complementary $\nu$NCQE neutron multiplicity measurement, directly relevant to constraining the NCQE background in DSNB searches, competitive with the recent T2K measurement at SK-Gd. The planned Super-SANDI upgrade, deploying a large Water-based Liquid Scintillator (WbLS) volume, will further extend ANNIE's reach to hadronic final states and exclusive NC channels, and enable joint measurements with liquid argon detectors sharing the BNB beamline ahead of DUNE and Hyper-Kamiokande.

Doran, Steven [Iowa State U.]↗

DOE OSTI2020

Measurement uncertainty of rossi-alpha neutron experiments

Rossi-alpha neutron experiments are used to estimate the prompt neutron decay constant of a fissile assembly, a quantity of widespread interest in applications including in nuclear nonproliferation and criticality safety. This work develops a mathematical model to efficiently estimate measurement uncertainty of Rossi-alpha neutron experiments inferred from a two-exponential fit model with histogram binning. The derived uncertainty estimates were validated using repeated Rossi-alpha measurements of a subcritical, 4.5-kg sphere of weapons-grade, alpha-phase plutonium with nickel, copper, tungsten, and polyethylene reflectors. The estimates of uncertainty for the histogram data produced by the model were conservative and agree with the reference uncertainties within noise. The estimates of the prompt neutron decay constant uncertainty agreed with the reference uncertainties within one standard deviation. In conclusion, the proposed model will reduce total measurement times, ultimately reducing operational and procedural costs in application.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

DOE OSTI2023

Accurate activity determination of a californium neutron source

Accurately counting analog events requires constructing an electronics chain that produces one count for each input pulse. Here, in this work, we review the use of Nuclear Instrumentation Module electronic units for counting neutron capture events in a 3He tube. We identify two unique types of false trigger events in a leading-edge discriminator and show how a dual timer module can be used to produce a veto window to exclude these events. We use the constructed electronics chain to build an apparatus to measure neutron pulses from a 252 Cf neutron source. We compare the measurements with a Monte Carlo N-Particle (MCNP) model to determine the activity of the neutron source. Furthermore, by making additional measurements with borated polyethylene attenuators between the source and detector, we are able to determine the boron concentration of the polyethylene. This technique provides accurate determination of the source activity to a precision of 2.8% at the k=1 level. The method used is simple, inexpensive, and requires no additional calibrated instruments.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2024

Phase stability and microstructure of neutron-irradiated substoichiometric yttrium dihydrides

The impact of the neutron-displacement damage on phase stability and microstructure of substoichiometric yttrium dihydrides (YH x , x <2) were investigated to assess their use as solid moderator in high-temperature nuclear reactors. YH x specimens were, thus, subjected to neutron irradiations in the range of 0.1–2 displacements per yttrium atom (dpa-Y) in the temperature range of 536–878°C at the Oak Ridge National Laboratory's (ORNL's) High Flux Isotope Reactor (HFIR). YH x specimens were initially prepared at stoichiometry (H/Y) ratios of 1.69 and 1.83. HFIR-irradiated specimens were characterized by variety of techniques to investigate H retention characteristics including dimensional analysis, optical microscopy, scanning electron microscopy electron back scatter diffraction (EBSD), transmission electron microscopy, thermal desorption spectroscopy (TDS), and high-energy x-ray diffraction (HE-XRD) characterizations. Overall, YH x exhibited notable structural and phase stability under short-term neutron-irradiation, except for the samples with significant silicon carbide (SiC) interaction at high doses and temperatures. Basic dimensional and mass measurements were misleading for accurate assessment of H retention, as confirmed by EBSD phase maps, XRD line profiles, and TDS signals. Thus, it was discussed that a robust H retention metric is needed to assess irradiated hydrides. Further, nanoscale cavities were observed as a result of the neutron irradiation in all samples. Although no clear impact of dose and irradiation temperature was determined, the initial H/Y ratio had an impact on the cavity number density where low H/Y specimens had high-resistance to cavity formation. The Y-vacancy cluster formation at the collision stage of the displacement cascade and their stabilization by H were considered to be the likely underlying mechanisms for the observed cavity microstructure.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗

DOE OSTI2020

Performance of neutron spectrum unfolding using deuterated liquid scintillator

The performance of the maximum likelihood expectation maximization method for unfolding neutron energy spectra using deuterated liquid scintillator is evaluated for future utilization with rare isotope beams. High-resolution neutron energy spectra as well as the detector response matrix were measured at the Edwards Accelerator Laboratory at Ohio University. Maximum-likelihood expectation maximization (MLEM) unfolded neutron spectra are compared with spectra from neutron time-of-flight. In conclusion, the effects of the MLEM stopping criteria and spectrum statistics are also investigated.

47 OTHER INSTRUMENTATION↗

DOE OSTI2021

New capability for neutron transmission measurements at LANSCE: The DICER instrument

A new capability for neutron transmission measurements has been developed at the Los Alamos Neutron Science Center (LANSCE). The DICER (Device for Indirect Capture Experiments on Radionuclides) instrument is designed to tightly constrain neutron-capture cross sections for short-lived radionuclides that are beyond the reach of direct techniques, via measurement and analysis of neutron transmission resonances on these same radionuclides. The innovative DICER apparatus enables simultaneous sample-in and sample-out measurements, thus minimizing the amount of sample material needed and reducing the measurements time by half. A description of the current status of the new transmission station, along with a performance overview and results from known reactions, will be presented here.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2023

Reconstruction of fast neutron direction in segmented organic detectors using deep learning

A method for reconstructing the direction of a fast neutron source using a segmented organic scintillator-based detector and deep learning model is proposed and analyzed. Here, the model is based on recurrent neural network, which can be trained by a sequence of data obtained from an event recorded in the detector and suitably pre-processed. The performance of deep learning-based model is compared with the conventional double-scatter detection algorithm in reconstructing the direction of a fast neutron source. With the deep learning model, the uncertainty in source direction of 0.301 rad is achieved with 100 neutron detection events in a segmented cubic organic scintillator detector with a side length of 46 mm. To reconstruct the source direction with the same angular resolution as the double-scatter algorithm, the deep learning method requires 75% fewer events. Application of this method could augment the operation of segmented detectors operated in the neutron scatter camera configuration for applications such as special nuclear material detection.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2022

Simultaneous neutron and X-ray tomography for visualization of graphite electrode degradation in fast-charged lithium-ion batteries

Advanced battery characterization using neutron and X-ray-based imaging modalities is crucial to reveal fundamental degradation modes of lithium-ion batteries (LIBs). Taking advantage of the sensitivity of neutrons to some low-Z (Li) and X-rays to high-Z materials (Cu), here we demonstrate the viability of simultaneous neutron and X-ray tomography (NeXT) as a non-destructive imaging platform for ex-situ 3D visualization of graphite electrode degradation following extreme fast charging (XFC). In addition, we underscore the benefits of the simultaneous of NeXT by combining the neutron and X-ray tomography data from the same sample location for material identification and segmentation of one pristine and two XFC-cycled graphite electrodes (9C charge for 450 cycles). Our ex-situ results and methodology development pave the way for the design of NeXT-friendly LIB geometries that will allow operando and/or in-situ 3D visualization of electrode degradation during XFC.

25 ENERGY STORAGE↗