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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 991 records · Page 55
All sourcesNASA NTRSDOE OSTI
DOE OSTI2014

Room temperature ferromagnetism in a phthalocyanine based carbon material

We report on a simple method to fabricate a magnetic carbon material that contains nitrogen-coordinated transition metals and has a large magnetic moment. Highly chlorinated iron phthalocyanine was used as building blocks and potassium as a coupling reagent to uniformly disperse nitrogen-coordinated iron atoms on the phthalocyanine based carbon material. The iron phthalocyanine based carbon material exhibits ferromagnetic properties at room temperature and the ferromagnetic phase transition occurs at T{sub c} = 490 ± 10 K. Transmission electron microscopy observation, X-ray diffraction analysis, and the temperature dependence of magnetization suggest that the phthalocyanine molecules form three-dimensional random networks in the iron phthalocyanine based carbon material.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2015

Kinetic Alfven wave in the presence of kappa distribution function in plasma sheet boundary layer

The particle aspect approach is adopted to investigate the trajectories of charged particles in the electromagnetic field of kinetic Alfven wave. Expressions are found for the dispersion relation, damping/growth rate and associated currents in the presence of kappa distribution function. Kinetic effect of electrons and ions are included to study kinetic Alfven wave because both are important in the transition region. It is found that the ratio β of electron thermal energy density to magnetic field energy density and the ratio of ion to electron thermal temperature (T{sub i}/T{sub e}), and kappa distribution function affect the dispersion relation, damping/growth rate and associated currents in both cases(warm and cold electron limit).The treatment of kinetic Alfven wave instability is based on assumption that the plasma consist of resonant and non resonant particles. The resonant particles participate in an energy exchange process, whereas the non resonant particles support the oscillatory motion of the wave.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2016

Inelastic x-ray scattering measurements of phonon dynamics in URu 2 Si 2

In this paper, we study high-resolution inelastic x-ray scattering measurements of the acoustic phonons of URu 2 Si 2 . At all temperatures, the longitudinal acoustic phonon linewidths are anomalously broad at small wave vectors revealing a previously unknown anharmonicity. The phonon modes do not change significantly upon cooling into the hidden order phase. In addition, our data suggest that the increase in thermal conductivity in the hidden order phase cannot be driven by a change in phonon dispersions or lifetimes. Hence, the phonon contribution to the thermal conductivity is likely much less significant compared to that of the magnetic excitations in the low temperature phase.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2011

NON-DETECTION OF MAGNETIC FIELDS IN THE CENTRAL STARS OF THE PLANETARY NEBULAE NGC 1360 AND LSS 1362

The presence of magnetic fields is an attractive hypothesis for shaping planetary nebulae (PNe). We report on observations of the central star of the two PNe NGC 1360 and LSS 1326. We performed spectroscopy on circularly polarized light with the Focal Reducer and Low Dispersion Spectrograph at the Very Large Telescope of the European Southern Observatory. Contrary to previous reports, we find that the effective magnetic field, which is the average over the visible stellar disk of longitudinal components of the magnetic fields, is null within errors for both stars. We conclude that direct evidence of magnetic fields on the central stars of PNe is still missing-either the magnetic field is much weaker (<600 G) than previously reported, or more complex (thus leading to cancellations), or both. Certainly, indirect evidence (e.g., MASER emission) fully justify further efforts to point out the strength and morphology of such magnetic fields.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2026

A solid-state extrusion pathway extensible to upcycling aluminum scrap and end-of-life permanent magnets into ductile Al-6061/SmCo 5 structural magnetic composites

Permanent magnets offer strong potential for multifunctional structural components, but their inherent brittleness limits direct integration. Here, SolidStir® Extrusion (SSE) is used to embed SmCo5 powder into AA6061 in the solid state, and the resulting microstructure, interfacial chemistry, mechanical properties, and magnetic response are systematically characterized. SSE fragments the initial SmCo 5 powder into predominantly fine particles dispersed within an ultrafine Al matrix, with a volume fraction of ∼ 4–6 % in this proof-of-concept study. Interfacial reactions form a continuous Al–Co reaction layer, with local atomic-resolution indexing consistent with Al 13 Co 4 , together with Sm–Si-rich reaction products, while the matrix contains Sm–Co–Si-rich precipitates and Mg 2 Si, producing features from nanometers to micrometers. Compared with an Al extrudate, this architecture increases yield strength by ∼ 42 % and tensile strength by ∼ 31 %, while preserving uniform elongation, and it sustains work hardening in compression from 150 to 400 °C. The composite retained hard-magnetic behavior, with axial magnetization of 12.7 A·m 2 kg −1 at 6 T and intrinsic coercivity of 9.6 kOe. These findings demonstrate that SSE can produce Al-based load-bearing magnetic composites while preserving useful SmCo5 functionality.

36 MATERIALS SCIENCE↗
DOE OSTI2015

THE ROLE OF TURBULENCE AND MAGNETIC FIELDS IN SIMULATED FILAMENTARY STRUCTURE

We use numerical simulations of turbulent cluster-forming regions to study the nature of dense filamentary structures in star formation. Using four hydrodynamic and magnetohydrodynamic simulations chosen to match observations, we identify filaments in the resulting column density maps and analyze their properties. We calculate the radial column density profiles of the filaments every 0.05 Myr and fit the profiles with the modified isothermal and pressure-confined isothermal cylinder models, finding reasonable fits for either model. The filaments formed in the simulations have similar radial column density profiles to those observed. Magnetic fields provide additional pressure support to the filaments, making “puffier” filaments less prone to fragmentation than in the pure hydrodynamic case, which continue to condense at a slower rate. In the higher density simulations, the filaments grow faster through the increased importance of gravity. Not all of the filaments identified in the simulations will evolve to form stars: some expand and disperse. Given these different filament evolutionary paths, the trends in bulk filament width as a function of time, magnetic field strength, or density are weak, and all cases are reasonably consistent with the finding of a constant filament width in different star-forming regions. In the simulations, the mean FWHM lies between 0.06 and 0.26 pc for all times and initial conditions, with most lying between 0.1 to 0.15 pc; the range in FWHMs is however, larger than seen in typical Herschel analyses. Finally, the filaments display a wealth of substructure similar to the recent discovery of filament bundles in Taurus.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2022

Probing the hydrolytic degradation of UF 4 in humid air

This manuscript describes the chemical transformations that occur during hydrolysis of uranium tetrafluoride (UF 4 ) due to its storage in humid air (85% and 50% relative humidity) at ambient temperatures. This hydrolysis was previously reported to proceed slowly or not at all (depending on the percent relative humidity); however, previous reports relied primarily on X-ray diffraction methods to probe uranium speciation. Here, we employ a battery of physiochemical probing techniques to explore potential hydrolysis, including Raman spectroscopy, powder X-ray diffraction, 19 F nuclear magnetic resonance spectroscopy, scanning electron microscopy, and focused ion beam microscopy with energy-dispersive X-ray spectroscopy. Of these, only Raman spectroscopy proved to be particularly useful at observing chemical changes to UF 4 . It was found that anhydrous UF 4 slightly oxidizes over the course of thirteen days to Schoepite-like uranium complexes and possibly UO 3 . In contrast, UF 4 exposed to 50% relative humidity slightly decomposes into UO 2 F 2 , Schoepite-like uranium complexes, and possibly a high order uranium oxide that eluded chemical assignment (U x O y ). Despite the rich chemical speciation observed in our Raman spectroscopy measurements, X-ray diffraction and 19 F NMR measurements on the same material showed no changes. Microscopy measurements suggest that the observed reactions between UF 4 and water occur primarily on the surface of UF 4 particulates via a method that is visually similar to surface corrosion of metals. Therefore, we postulate that NMR spectroscopy and X-ray diffraction, which are well-suited for bulk analysis, are less suited than Raman spectroscopy to observe the surface-based reactions that occur to UF 4 when exposed to humid air. Considering the importance of UF 4 in the production of nuclear fuel and weapons, the results presented herein are widely applicable to numerous nuclear science fields where uranium detection and speciation in humid environments is of value, including nuclear nonproliferation and nuclear forensics.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2013

Large amplitude inertial compressional Alfvénic shock and solitary waves, and acceleration of ions in magnetohydrodynamic plasmas

Large amplitude inertial compressional Alfvénic shock and solitary waves in magnetohydrodynamic plasmas are investigated. Dispersive effect caused by non-ideal electron inertia currents perpendicular to the ambient magnetic field can balance the nonlinear steepening of waves leading to the formation of a soliton. A Sagdeev-potential formalism is employed to derive an energy-balance like equation. The range of allowed values of the soliton speed, M (Mach number), plasma β (ratio of the plasma thermal pressure to the pressure in the confining magnetic field), and electron inertia, wherein solitary waves may exist, are determined. Depth of the potential increases with increasing the Mach number and plasma β, however decreases with the increasing electron inertia. The height of soliton increases with increasing in Mach number and decreases with plasma β. And with increasing electron inertial length, the width of soliton increases. The electron-ion collisional dissipation results a dissipative inertial compressional Alfvén wave, which can produce a shock like structure and can efficiently accelerate ions to the order of the local Alfvén velocity. The shock height increases with the increasing collision frequency, but shock height decreases with increasing plasma β.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2013

Electron beam driven lower hybrid waves in a dusty plasma

An electron beam propagating through a magnetized dusty plasma drives electrostatic lower hybrid waves to instability via Cerenkov interaction. A dispersion relation and the growth rate of the instability for this process have been derived taking into account the dust charge fluctuations. The frequency and the growth rate of the unstable wave increase with the relative density of negatively charged dust grains. Moreover, the growth rate of the instability increases with beam density and scales as the one-third power of the beam density. In addition, the dependence of the growth rate on the beam velocity is also discussed.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2013

Compressional Alfvénic rogue and solitary waves in magnetohydrodynamic plasmas

Generation of compressional Alfvénic rogue and solitary waves in magnetohydrodynamic plasmas is investigated. Dispersive effect caused by non-ideal electron inertia currents perpendicular to the ambient magnetic field can balance the nonlinear steepening of waves leading to the formation of a soliton. The reductive perturbation method is used to obtain a Korteweg–de Vries (KdV) equation describing the evolution of the solitary wave. The height of a soliton is proportional to the soliton speed “U” and inversely proportional to plasma “β” (ratio of plasma thermal pressure to pressure of the confining magnetic field) and the width of soliton is proportional to the electron inertial length. KdV equation is used to study the nonlinear evolution of modulationally unstable compressional Alfvénic wavepackets via the nonlinear Schrödinger equation. The characteristics of rogue wave influenced by plasma “β” and the electron inertial length are described.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2013

Sagdeev potential approach for large amplitude compressional Alfvenic double layers in viscous plasmas

Sagdeev’s technique is used to study the large amplitude compressional Alfvenic double layers in a magnetohydrodynamic plasma taking into account the small plasma β and small values of kinematic viscosity. Dispersive effect raised by non-ideal electron inertia currents perpendicular to the ambient magnetic field. The range of allowed values of the soliton speed, M (Mach number), plasma β (ratio of the plasma thermal pressure to the pressure in the confining magnetic field), and viscosity coefficient, wherein double layer may exist, are determined. In the absence of collisions, viscous dissipation modifies the Sagdeev potential and results in large amplitude compressional Alfvenic double layers. The depth of Sagdeev potential increases with the increasing Mach number and plasma β, however, decreases with the increasing viscosity. The double layer structure increases with the increasing plasma β, but decreases with increasing viscous dissipation μ(tilde sign)

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2014

Growth and characterization of nonpolar, heavily Mn-substituted ZnO films

Eight percent of Mn was successfully diluted into nonpolar ZnO films deposited by pulsed laser deposition on single crystal (100) SrTiO{sub 3} substrates. X-ray diffraction patterns and energy-dispersive X-ray spectroscopy confirmed high crystallinity of the films and excluded unintentional magnetic doping. A unique surface domain structure was observed by scanning electron microscope and atomic force microscope, which might play a vital role to strain release induced by lattice mismatch between nonpolar (11–20) ZnO film and (100) SrTiO{sub 3} substrate. In addition, the films showed strong ferromagnetism with a large coercivity H{sub C} ∼ 180 Oe at room temperature. The large magnetic moment is ascribed to carrier-mediated exchange interaction between the Mn ions, where the majority of the carriers are oxygen vacancies.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2015

Study on structural, optical properties of solvothermally synthesized Ni doped CdS nanorods

Undoped and alkali metal i.e Ni doped CdS nanorods (Cd{sub x}Ni{sub 1-x}S) with (x = 0.0, 0.3,) has been synthesized by using a convenient solvothermal technique. In order to confirm the structure of the synthesized nanorods X-ray diffraction (XRD) has been done which reveals the formation of hexagonal phase of the dilute magnetic semiconducting nanorods having size of undoped 27.79nm and doped 17.49nm. Energy dispersive X-ray analysis depicts the presence of elements Cd, Ni and S in their stoichiometric ratio. Optical behavior of undoped and doped nanorods has been investigated. UV-visible spectra show the blue shift in the band gap, as compared to the bulk CdS which may be due the quantum confinement occurs in the nanostructures. Morphological analysis has been done with the help of Transmission electron microscope which confirms the polycrystalline nature of the synthesized nanorods.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2015

Kinetic Alfven solitary waves in a magnetized plasma with superthermal electrons

A study of the ion Larmor radius effects on the solitary kinetic Alfven waves (SKAWs) in a magnetized plasma with superthermal electrons is presented by employing the kinetic theory. The linear dispersion relation of SKAW is shown to depend on the superthermal parameter κ, ion to electron temperature ratio, and the angle of wave propagation. Using the Sagdeev potential approach, the energy balance equation has been derived to study the dynamics of SKAWs. The effects of various plasma parameters are investigated for the propagation of SKAWs. It is shown that only compressive solitons can exist and in the Maxwellian limit our results are in good agreement with previous studies. Further, the characteristics of small amplitude SKAWs are investigated. Present study could be useful for the understanding of SKAWs in a low β plasma in astrophysical environment, where particle distributions are superthermal in nature.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2021

Particle emission with identification from an atmospheric pressure plasma liquid interface

A conspicuous emission phenomenon of luminous particles from the liquid anode surface of an atmospheric pressure DC glow discharge is reported. The emission has been shown to occur when the plasma forms a pattern on the surface of the liquid electrolyte. Here, the spatial-temporal evolutions of the trajectories of emitted particles were studied using a high-speed imaging system. Particles were sampled in flight using a witness plate for analysis. Critical particle characteristics were examined using electron microscope technologies. The morphology of the resulting splats and compositions suggest that they are molten droplets with a great deal of structure, including evidence of nanoprecipitation. A theoretical model was employed to estimate the particle size from the measured splats, which provides a radius range within a hundred micrometers. This experiment leads to the postulation of a mechanism in which particle emission at the plasma liquid interface is likely driven by the Taylor cone effect.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2014

Optical/near-infrared polarization survey of Sh 2-29: Magnetic fields, dense cloud fragmentations, and anomalous dust grain sizes

Sh 2-29 is a conspicuous star-forming region marked by the presence of massive embedded stars as well as several notable interstellar structures. In this research, our goals were to determine the role of magnetic fields and to study the size distribution of interstellar dust particles within this turbulent environment. We have used a set of optical and near-infrared polarimetric data obtained at OPD/LNA (Brazil) and CTIO (Chile), correlated with extinction maps, Two Micron All Sky Survey data, and images from the Digitized Sky Survey and Spitzer. The region's most striking feature is a swept out interstellar cavity whose polarimetric maps indicate that magnetic field lines were dragged outward, piling up along its borders. This led to a higher magnetic strength value (≈400 μG) and an abrupt increase in polarization degree, probably due to an enhancement in alignment efficiency. Furthermore, dense cloud fragmentations with peak A{sub V} between 20 and 37 mag were probably triggered by its expansion. The presence of 24 μm point-like sources indicates possible newborn stars inside this dense environment. A statistical analysis of the angular dispersion function revealed areas where field lines are aligned in a well-ordered pattern, seemingly due to compression effects from the H II region expansion. Finally, Serkowski function fits were used to study the ratio of the total-to-selective extinction, revealing a dual population of anomalous grain particle sizes. This trend suggests that both effects of coagulation and fragmentation of interstellar grains are present in the region.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2019

Tuning Edge Localized Spin Waves in Magnetic Microstripes by Proximate Magnetic Structures.

The propagation of edge localized spin waves (E-SWs) in yttrium iron garnet (YIG; Y3Fe5O12) microstripes with and without magnetic microstructures in close proximity is investigated by micromagnetic simulations. A splitting of the dispersion curve with the presence of permalloy (Py; Ni81Fe19) stripe is observed. The results show that E-SWs on the two edges of YIG stripe have different wavelengths, group velocities, and decay lengths at the same frequencies. The role of the Py stripe was found to be the source of the inhomogeneous static dipolar field without dynamic coupling with YIG. This work opens new perspectives for the design of innovative spin wave interference-based logic devices.

Zhang, Zhizhi↗
DOE OSTI2022

Capturing the ground state of uranium dioxide from first principles: Crystal distortion, magnetic structure, and phonons

Uranium dioxide (UO 2 ) remains a formidable challenge for first-principles approaches due to the complex interplay among spin-orbit coupling, Mott physics, magnetic ordering, and crystal distortions. Here we use DFT+U to explore UO 2 at zero temperature, incorporating all the aforementioned phenomena. The technical challenge is to navigate the many metastable electronic states produced by DFT+U, which is accomplished using f-orbital occupation matrix control to search for the ground state. We restrict our search to the high-symmetry ferromagnetic phase, including spin-orbit coupling, which produces a previously unreported occupation matrix. This newfound occupation matrix is then used as an initialization to explore the broken symmetry phases. We find the oxygen cage distortion of the 3k antiferromagnetic state to be in excellent agreement with experiments, and both the spin-orbit coupling and the Hubbard U are critical ingredients. Further, we demonstrate that only select phonon modes have a strong dependence on the Hubbard U, whereas magnetic ordering has only a small influence overall. We perform measurements of the phonon dispersion curves using inelastic neutron scattering, and our calculations show good agreement when using reasonable values of U. The quantitative success of DFT+U warrants exploration of thermal transport and other observables within this level of theory.

36 MATERIALS SCIENCE↗