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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 973 records · Page 54
All sourcesNASA NTRSDOE OSTI
DOE OSTI2015

Evaluation of microstructure anisotropy on room and medium temperature ECAP deformed F138 steel

The microstructure developed during severe plastic deformation results in improved mechanical properties because of the decrease in domain sizes and accumulation of defects, mainly dislocation arrays. The characteristic deformation stages observed in low stacking fault energy (SFE) face centered cubic (FCC) materials are highly influenced by the development of the primary and secondary twinning that compete with dislocation glide. In this paper, a low SFE F138 stainless steel is deformed by equal channel angular pressing (ECAP) up to 4 passes at room temperature (RT) and at 300 °C to compare the grain refinement and twin boundary development with increasing deformation. Tensile tests were performed to determine the deformation stages reached by the material before and after ECAP deformation, and the resulting microstructure was observed by TEM. X-ray diffraction and EBSD, average technique the first and local the second one, were used to quantify the microstructural changes, allowing the determination of diffraction domain sizes, dislocation and stacking fault densities and misorientation indices, which lead to a complete analysis of the deformation introduced in the material, with comparative correlations between various microstructural parameters. - Highlights: • The microstructure of ECAP pressed F138 steel was studied using TEM, EBSD and XRD. • Increasing deformation reduced domain sizes and increased dislocation densities. • Dislocation array compactness and misorientation increased with higher deformation. • Largest dislocation densities, mostly screw, match with simultaneous activation of twins. • Several correlations among microstructural features and parameters have been disclosed.

36 MATERIALS SCIENCE↗
DOE OSTI2018

Cold rolling texture evolution of TiB2 particle reinforced Al-based composites by Neutron Diffraction and EBSD analysis

Highlights: • Texture development of in-situ TiB{sub 2} particle reinforced Al matrix composites after cold rolling were characterized. • The sum of rolling texture volume fractions has been significantly reduced by the weak texture in particle deformation zone. • Recrystallization nuclei with the Cube and Rotated-Cube orientations were observed in the particle deformation zones. • Small TiB{sub 2} particles within Al grains kept the parallel relationship with surrounding matrix during the deformation. - Abstract: Texture development of particle-reinforced metal matrix materials (P-MMCs) has not been understood well, especially the effects of second-phase particles during the deformation. In this work, we have investigated the texture evolution of TiB{sub 2}/Al composites during cold rolling by Neutron Diffraction and EBSD analysis. Two forms of TiB{sub 2} particles influenced the texture evolution in different ways. The particle-clusters aggregated along grain boundaries led to a reduction of texture volume fraction; recrystallization nuclei with weak texture appeared around these particle-clusters. Small non-shearable TiB{sub 2} particles dispersed inside Al matrix contributed to strong Copper texture component at high strains; the individual particles rotated together with Al matrix during the deformation. These revealed effects of particles on the texture development in TiB{sub 2}/Al composites provide a reference for the texture control of P-MMCs.

36 MATERIALS SCIENCE↗
DOE OSTI2017

Influence of surface morphology and UFG on damping and mechanical properties of composite reinforced with spinel MgAl{sub 2}O{sub 4}-SiC core-shell microcomposites

Interface between ceramic particulate and matrix is known to control the response of the materials and functionality of the composite. Among numerous physical properties, grain structure of the materials has also played a significant role in defining the behaviour of metal matrix composites. Usually, silicon carbide (SiC) particles show poor interfacial wettability in aluminium melt. Herein, we were successfully synthesized magnesium oxide (MgO) and nanocrystalline magnesium aluminate (MgAl{sub 2}O{sub 4}) spinel coated silicon carbide (SiC) core-shell micro-composites through sol-gel technique to improve the wettability of dispersoids. Core-shell structures of submicron size were thoroughly investigated by various characterization techniques. Further, aluminium matrix composites incorporated with pristine SiC, MgO grafted SiC and MgAl{sub 2}O{sub 4} grafted SiC particles were fabricated by stir casting technique, respectively. Additionally, as-cast composites were processed via friction stir processing (FSP) technique to observe the influence of grain refinement on mechanical and damping properties. Electron back scattered diffraction (EBSD), Field emission scanning electron microscopy (FE-SEM) and X-ray energy dispersion spectroscopy (EDX) analysis were conducted for investigating grain size refinement, adequate dispersion, stability and de-agglomeration of encapsulated SiC particles in aluminium matrix. The mechanical as well as thermal cyclic (from − 100 to 400 °C) damping performance of the as-cast and friction stir processed composites were studied, respectively. Finally, the enhanced properties were attributable to reduced agglomeration, stabilization and proper dispersion of the tailored SiC particles Al matrix. - Highlights: •Synthesizing a novel coating layer of MgO and MgAl{sub 2}O{sub 4} spinel onto SiC particles •Significant improvement in UTS and hardness by reinforcing tailored SiC in Al •Significant grain refinements were obtained through FSP •SiC/MgAl{sub 2}O{sub 4}/Al exhibits ~ 61% higher storage modulus as compare to pure Al after FSP.

36 MATERIALS SCIENCE↗
DOE OSTI2014

Dynamic recrystallization behavior of an as-cast TiAl alloy during hot compression

High temperature compressive deformation behaviors of as-cast Ti–43Al–4Nb–1.4W–0.6B alloy were investigated at temperatures ranging from 1050 °C to 1200 °C, and strain rates from 0.001 s{sup −1} to 1 s{sup −1}. Electron back scattered diffraction technique, scanning electron microscopy and transmission electron microscopy were employed to investigate the microstructural evolutions and nucleation mechanisms of the dynamic recrystallization. The results indicated that the true stress–true strain curves show a dynamic flow softening behavior. The dependence of the peak stress on the deformation temperature and the strain rate can well be expressed by a hyperbolic-sine type equation. The activation energy decreases with increasing the strain. The size of the dynamically recrystallized β grains decreases with increasing the value of the Zener–Hollomon parameter (Z). When the flow stress reaches a steady state, the size of β grains almost remains constant with increasing the deformation strain. The continuous dynamic recrystallization plays a dominant role in the deformation. In order to characterize the evolution of dynamic recrystallization volume fraction, the dynamic recrystallization kinetics was studied by Avrami-type equation. Besides, the role of β phase and the softening mechanism during the hot deformation was also discussed in details. - Highlights: • The size of DRXed β grains decreases with increasing the value of the Z. • The CDRX plays a dominant role in the deformation. • The broken TiB{sub 2} particles can promote the nucleation of DRX.

36 MATERIALS SCIENCE↗
DOE OSTI2016

Evolution of mechanical properties of ultrafine grained 1050 alloy annealing with electric current

The tensile properties and microstructures of 1050 aluminum alloy prepared by equal channel angular pressing at cryogenic temperature (cryoECAP) after electric current annealing at 90–210 °C for 3 h were investigated by tensile test, electron back scattering diffraction (EBSD) and transmission electron microscopy (TEM). An unexpected annealing-induced strengthening phenomenon occurs at 90–210 °C, due to a significant decrease in the density of mobile dislocations after annealing, and thus a higher yield stress is required to nucleate alternative dislocation sources during tensile test. The electric current can enhance the motion of dislocations, lead to a lower dislocation density at 90–150 °C, and thus shift the peak annealing temperature from 150 °C to 120 °C. Moreover, the electric current can promote the migration of grain boundaries at 150–210 °C, result in a larger grain size at 150 °C and 210 °C, and thus causes a lower yield stress. The sample annealed with electric current has a lower uniform elongation at 90–120 °C, and the deviation in the uniform elongation between samples annealed without and with electric current becomes smaller at 150–210 °C. - Highlights: • An unexpected annealing-induced strengthening phenomenon occurs at 90–210 °C. • The d. c. current can enhance the motion of dislocations at 90–150 °C, and thus shift the peak annealing temperature from 150 °C to 120 °C. • The d. c. current can promote the grain growth at 150–210 °C, and thus cause a lower yield stress. • The DC annealed sample has a lower uniform elongation at 90–120 °C.

36 MATERIALS SCIENCE↗
DOE OSTI2018

iCHORD-SI combination as an alternative to EDS-EBSD coupling for the characterization of γ-γ′ nickel-based superalloy microstructures

Highlights: • A new method to get orientation maps discriminating the gamma and gamma’ phases of Ni superalloys is described. • The method combines the iCHORD technique with secondary ion imaging. • The new method resolves precipitates down to 150 nm within a reasonable acquisition time. - Abstract: Because they exhibit very similar diffraction patterns, the γ and γ′ phases of nickel-based superalloys cannot be distinguished by the conventional EBSD technique alone. This paper presents an original method which discriminates those phases on an orientation map by exploiting their chemical differences. Performed with a Focused Ion Beam (FIB) microscope, the method is the combination of the ion CHanneling ORientation Determination technique (iCHORD) – recently developed by Langlois et al. [1] – with the chemical information obtained from Secondary Ion (SI) images. The performances of the method are compared to the EDS-EBSD coupling which also discriminates phases based on their chemical compositions. Applied filters, angular resolution, spatial resolution of the phase discrimination and acquisition time are discussed. It results that the iCHORD–SI combination offers an orientation map with an angular resolution slightly decreased compared to that of the EBSD technique, but with a good phase resolution (down to 150 nm) and within a reasonable acquisition time. Thus, the iCHORD–SI combination appears to be an interesting method for the crystallographic systems where phases are difficult to discriminate by the EBSD technique alone but present a significant chemical contrast.

36 MATERIALS SCIENCE↗
DOE OSTI2018

Austenitic Reversion of Cryo-rolled Ti-Stabilized Austenitic Stainless Steel: High-Resolution EBSD Investigation

In this study, AISI 321 austenitic stainless steel (ASS) was cryo-rolled and subsequently annealed at 650 and 800 °C to reverse BCC α′-martensite to FCC γ-austenite. The texture evolution associated with the reversion at the selected temperatures was investigated using high-resolution EBSD. After the reversion, TiC precipitates were observed to be more stable in 650 °C-annealed specimens than those reversed at 800 °C. {110} texture was mainly developed in specimens subjected to both annealing temperatures. However, specimens reversed at 650 °C have stronger texture than those annealed at 800 °C, even at the higher annealing time. The strong intensity of {110} texture component is attributed to the ability of AISI 321 ASS to memorize the crystallographic orientation of the deformed austenite, a phenomenon termed texture memory. The development of weaker texture in 800 °C-annealed specimens is attributed to the residual strain relief in grains, dissolution of grain boundary precipitates, and an increase in atomic migration along the grain boundaries. Based on the observed features of the reversed austenite grains and estimation from an existing model, it is suspected that the austenite reversion at 650 and 800 °C undergone diffusional and martensitic shear reversion, respectively.

36 MATERIALS SCIENCE↗
DOE OSTI2023

Sputter-Deposited Mo Thin Films: Multimodal Characterization of Structure, Surface Morphology, Density, Residual Stress, Electrical Resistivity, and Mechanical Response

Multimodal datasets of materials are rich sources of information which can be leveraged for expedited discovery of process–structure–property relationships and for designing materials with targeted structures and/or properties. For this data descriptor article, we provide a multimodal dataset of magnetron sputter-deposited molybdenum (Mo) thin films, which are used in a variety of industries including high temperature coatings, photovoltaics, and microelectronics. In this dataset we explored a process space consisting of 27 unique combinations of sputter power and Ar deposition pressure. Here, the phase, structure, surface morphology, and composition of the Mo thin films were characterized by x-ray diffraction, scanning electron microscopy, atomic force microscopy, and Rutherford backscattering spectrometry. Physical properties—namely, thickness, film stress and sheet resistance—were also measured to provide additional film characteristics and behaviors. Additionally, nanoindentation was utilized to obtain mechanical load-displacement data. The entire dataset consists of 2072 measurements including scalar values (e.g., film stress values), 2D linescans (e.g., x-ray diffractograms), and 3D imagery (e.g., atomic force microscopy images). An additional 1889 quantities, including film hardness, modulus, electrical resistivity, density, and surface roughness, were derived from the experimental datasets using traditional methods. Minimal analysis and discussion of the results are provided in this data descriptor article to limit the authors’ preconceived interpretations of the data. Overall, the data modalities are consistent with previous reports of refractory metal thin films, ensuring that a high-quality dataset was generated. The entirety of this data is committed to a public repository in the Materials Data Facility.

36 MATERIALS SCIENCE↗
DOE OSTI2015

Calcium and zirconium as texture modifiers during rolling and annealing of magnesium–zinc alloys

Rolling experiments were carried out on a ternary Mg–Zn–Ca alloy and its modification with zirconium. Short time annealing of as-rolled sheets is used to reveal the microstructure and texture development. The texture of the as-rolled sheets can be characterised by basal pole figures with split peak towards the rolling direction (RD) and a broad transverse angular spread of basal planes towards the transverse direction (TD). During annealing the RD split peaks as well as orientations in the sheet plane vanish whereas the distribution of orientations tilted towards the TD remains. It is shown in EBSD measurements that during rolling bands of twin containing structures form. During subsequent annealing basal orientations close to the sheet plane vanish based on a grain nucleation and growth mechanism of recrystallisation. Orientations with tilt towards the TD remain in grains that do not undergo such a mechanism. The addition of Zr delays texture weakening. - Highlights: • Ca in Mg–Zn-alloys contributes to a significant texture weakening during rolling and annealing. • Grain nucleation and growth in structures consisting of twins explain a texture randomisation during annealing. • Grains with transverse tilt of basal planes preferentially do not undergo a grain nucleation and growth mechanism. • Zr delays the microstructure and texture development.

36 MATERIALS SCIENCE↗
DOE OSTI2016

A comparison of EBSD based strain indicators for the study of Fe-3Si steel subjected to cyclic loading

The current work aims at proposing an EBSD-based indicator for fatigue damage of a Fe-3Si steel. At the same time direct observation of dislocation structures is provided by electron channelling contrast imaging (ECCI). The investigation consisted in processing the EBSD data from patterns collected on specimen subjected to low cycle fatigue. It revealed two different regimes depending on the applied total strain variation which is explained by the identification of the dislocations structures and their evolution. At low strain variation, strain accommodation occurs by planar glide of dislocations uniformly distributed throughout the grains. No misorientation evolution is observed. At higher strain variation, the vein-channel structure is observed within the grain and the wall-channel structure in the vicinity of grain boundaries. The misorientation between these two dislocation structures is evaluated at about 0.7° which is detected by the EBSD analyses and explains the increase of the different misorientation based criteria. The EBSD study enables also the prediction of crack initiation mode. Finally, this study points out the limits of the EBSD technique as no misorientation evolution is detected at small strain variation. Indeed, the lattice distortion is too weak to be detected by conventional EBSD. - Highlights: • Microstructure investigation of the fatigue behaviour of an iron-silicon steel • Use of cECCI to investigate the fatigue dislocations structures • Characterisation of local plastic accommodation through EBSD misorientation criteria.

36 MATERIALS SCIENCE↗
DOE OSTI2017

A phase quantification method based on EBSD data for a continuously cooled microalloyed steel

Mechanical properties of steels depend on the phase constitutions of the final microstructures which can be related to the processing parameters. Therefore, accurate quantification of different phases is necessary to investigate the relationships between processing parameters, final microstructures and mechanical properties. Point counting on micrographs observed by optical or scanning electron microscopy is widely used as a phase quantification method, and different phases are discriminated according to their morphological characteristics. However, it is difficult to differentiate some of the phase constituents with similar morphology. Differently, for EBSD based phase quantification methods, besides morphological characteristics, other parameters derived from the orientation information can also be used for discrimination. In this research, a phase quantification method based on EBSD data in the unit of grains was proposed to identify and quantify the complex phase constitutions of a microalloyed steel subjected to accelerated coolings. Characteristics of polygonal ferrite/quasi-polygonal ferrite, acicular ferrite and bainitic ferrite on grain averaged misorientation angles, aspect ratios, high angle grain boundary fractions and grain sizes were analysed and used to develop the identification criteria for each phase. Comparing the results obtained by this EBSD based method and point counting, it was found that this EBSD based method can provide accurate and reliable phase quantification results for microstructures with relatively slow cooling rates. - Highlights: •A phase quantification method based on EBSD data in the unit of grains was proposed. •The critical grain area above which GAM angles are valid parameters was obtained. •Grain size and grain boundary misorientation were used to identify acicular ferrite. •High cooling rates deteriorate the accuracy of this EBSD based method.

36 MATERIALS SCIENCE↗
DOE OSTI2017

Effects of LPSO/α-Mg interfaces on dynamic recrystallization behavior of Mg96.5Gd2.5Zn1 alloy

Highlights: • The effects of LPSO/α-Mg interfaces on the dynamic recrystallization (DRX) behavior of Mg{sub 96.5}Gd{sub 2.5}Zn{sub 1} (at.%) alloy during indirect extrusion at 350 °C were investigated. • The LPSO/α-Mg interfaces in Mg{sub 96.5}Gd{sub 2.5}Zn{sub 1} alloy appeared as two groups, including the basal and non-basal LPSO/α-Mg interfaces, which have various effects on the DRX behavior of Mg{sub 96.5}Gd{sub 2.5}Zn{sub 1} alloy. • Compared with the basal LPSO/α-Mg interfaces, DRX grains are preferentially nucleated near the non-basal LPSO/α-Mg interfaces where there is higher V{sub GROD} and lower required energy E{sub s} for the DRX nucleation. - Abstract: Mg-Gd-Zn alloy, which contains a long period stacking ordered (LPSO) structure, has the potential to become a high-strength Mg alloy within the automotive and aerospace industries. Two types of LPSO/α-Mg interfaces in Mg{sub 96.5}Gd{sub 2.5}Zn{sub 1} (at.%) alloy were characterized, namely, basal and non-basal LPSO/α-Mg interfaces. The effects of LPSO/α-Mg interfaces on the dynamic recrystallization (DRX) behavior during indirect extrusion at 350 °C were investigated. The grain reference orientation deviation (GROD) value (V{sub GROD}), derived from EBSD, could qualitatively characterize the dislocation density within a grain and determine the presence of DRX grain nucleation. The results suggested that the areas around non-basal LPSO/α-Mg interfaces always have higher V{sub GROD} than do basal LPSO/α-Mg interfaces. In addition, the stored energy (E{sub s}) required for DRX nucleation on the non-basal LPSO/α-Mg interface is lower than that on the basal LPSO/α-Mg interface. This is a result of the flat, sharp basal LPSO/α-Mg interface compared to the faceted non-basal LPSO/α-Mg interface. Regardless of whether the LPSO structure/α-Mg matrix interface is coherent or not, non-basal LPSO/α-Mg interfaces are favorable nucleation sites for DRX grains due to the higher V{sub GROD} and lower required energy E{sub s}.

36 MATERIALS SCIENCE↗
DOE OSTI2018

Residual stresses distribution, correlated with bending tests, within explosively welded Ti gr. 2/A1050 bimetals

Highlights: • Ti gr.2/A1050 clad was slightly affected by the explosive welding since negative sign values of stress tensor were detected. • Upon bending higher negative compression stresses were detected in this area. • Twins morphology changed from parallel to cross-shaped arrangement as a consequence of bending. • The compressive twinning was the dominant system before and after three point bending. - Abstract: Synchrotron radiation and XRD{sup 2} method were used to investigate the residual stress distribution before and after three point bending tests within an explosively welded composite composed of two light metals, namely: Ti gr. 2 and A1050. The analysis has shown that the bimetal is slightly affected by the explosive welding process since negative sign values of stress tensor were detected only in the immediate vicinity of interface of Ti gr. 2 characterized by a width of about 0.25 mm. Upon bending higher negative compression stresses are detected in this area as the σ{sub 11} value changes from −500 MPa to −1200 MPa. Additionally, the analysis of microstructure has revealed significant changes in twins morphology with primary and conjugate twinning before and after bending, respectively. However, the compressive twinning was the dominant system in both cases. Bending has changed the initial bimodal texture developing more spread basal components towards the transverse direction. The sample surface has been also significantly affected as the presence of compressive residual stress (−500 MPa) after bending was measured.

36 MATERIALS SCIENCE↗
DOE OSTI2018

The relationship between low-temperature toughness and secondary crack in low-carbon bainitic weld metals

Highlights: • The crack propagation plane was identified with the decreasing possibility of {110}/{100}, {112} and {123}. • Crack path deviates at some middle-angle misorientation boundaries with high strain concentration. • The most effective barrier to arrest crack in Ni0 and Ni2 is the boundaries of inter-Bain in a CPP packet, while in Ni4 the boundaries of inter-CPP and intra-Bain packets impede crack propagation. - Abstract: This paper aims to reveal the relationship among low-temperature toughness, microstructure and secondary crack from both microstructural and crystallographic perspectives. Instrumented Charpy tests were carried out in the upper platform, transition temperature range, as well as at lower temperatures. Quantitative fractographic analysis, microstructural characterization and secondary crack observation were conducted on half of the impact specimen. Crystallographic features were identified in the secondary crack proximity, e.g. variant selection, orientation relationship, cleavage plane of the corresponding crack matrix. Some results in literature are confirmed. Nickel addition is beneficial to hindering crack propagation as a result of microstructure improvement. The most effective barrier for crack propagation is high-angle misorientation boundaries between Bain packets and the boundaries of ferrite matrix with the microstructure of granular bainite. Additionally, high-angle misorientation boundaries between closed-packed plane packets arrest cracks in the mixed microstructure of fine lath bainite and intricate acicular ferrite. Most preferred crack propagation planes are {110} and {100} in our low carbon bainitic weld metals, with the decreasing possibility of {112} and {123}.

36 MATERIALS SCIENCE↗
DOE OSTI2018

Advanced processing of EBSD data to distinguish the complex microstructure evolution of a Cu-Ni-Si alloy induced by fatigue

Highlights: • Microstructure investigation of the fatigue behaviour of a Cu-Ni-Si alloy • Use of ECCI and EBSD to investigate the microstructure evolution related to fatigue dislocations structures • Characterisation of local plastic accommodation through EBSD misorientation criteria - Abstract: The present work aims at identifying the evolution of the microstructure of a Cu-Ni-Si (Corson alloy) alloy after low cycle fatigue by means of advanced electron microscopy analysis techniques (SEM-ECCI, Orientation Imaging Microscopy by means of SEM-EBSD and TEM). Deep attention is paid on the material subjected to high cyclic strains where a transient cellular dislocation structure transformed into precipitate free bands. It is shown that the formation of dislocation cells leads to a high GROD and high GOSaera value and its standard deviation. However, the presence of precipitate free bands results in the low GOSarea level and its low standard deviation.

36 MATERIALS SCIENCE↗
DOE OSTI2018

Application of chord length distributions and principal component analysis for quantification and representation of diverse polycrystalline microstructures

Highlights: • Microstructure quantification based on directional chord length distribution and principal component analysis is presented • A boundary-based algorithm of calculations of chord length distributions is introduced • Utility of the quantification framework is shown in three case studies on synthetic, experimental, and simulation datasets • Angularly resolved chord length distribution captures essential details of grain size and shape in diverse microstructures • Low-dimensional representations of directional chord length distributions are obtained using principal component analysis - Abstract: Quantification of mesoscale microstructures of polycrystalline materials is important for a range of practical tasks of materials design and development. The current protocols of quantifying grain size and morphology often rely on microstructure metrics (e.g., mean grain diameter) that overlook important details of the mesostructure. In this work, we present a quantification framework based on directionally resolved chord length distribution and principal component analysis as a means of extracting additional information from 2-D microstructural maps. Towards this end, we first present in detail a method for calculating chord length distribution based on boundary segments available in modern digital datasets (e.g., from microscopy post-processing) and their low-rank representations by principal component analysis. The utility of the proposed framework for capturing grain size, morphology, and their anisotropy for efficient visualization, representation, and specification of polycrystalline microstructures is then demonstrated in case studies on datasets from synthetic generation, experiments (on Ni-base superalloys), and simulations (on steel during recrystallization).

36 MATERIALS SCIENCE↗
DOE OSTI2018

Free surface effects on the recrystallization of compressed, stable, Al-Mn single crystals

Highlights: • The free surface provokes high frequency nucleation. • The free surface and surface ‘quality’ do not modify the orientations of the recrystallized grains. • The misorientation relations across recrystallization front are similar for all sections of both orientations. The free surface effect on the grain crystallography and morphology during recrystallization has been studied in stable Goss {110}001 and brass {110}112 - oriented single crystals of Al-1%wt.Mn alloy. The samples were plane strain compressed up to a strain of about 0.5 to develop a homogeneous structure comprising two sets of symmetrical microbands and then lightly annealed. The variation of recrystallization after annealing was then analysed by optical microscopy and SEM/EBSD on different cross-sections. The results are discussed in terms of the misorientation angle and axis distributions. The free surface provokes high frequency nucleation leading to a small grain size compared to internal sections of the bulk sample. However, the free surface and surface ‘quality’ do not modify the orientations of the recrystallized grains, i.e. similar groups of recrystallized grain orientations were observed for all sections. This leads to a strong misorientation relation between deformed/recovered area orientations and the limited number of groups of recrystallized grain orientations, basically the same as those observed during bulk recrystallization of similar crystals.

36 MATERIALS SCIENCE↗
DOE OSTI2016

Investigation of orientation inhomogeneities in polycrystalline materials by means of FEG-SEM, FIB, EBSD and 3-D reconstruction

The efficiency of different techniques application for the investigation of orientation inhomogeneities in polycrystalline materials was studied using FEG SEM-FIB dual beam station equipped with EBSD. It is shown that for the visualization of pearlitic ferrite fragments it is more appropriate to acquire the images in secondary electrons induced by Ga ions. At the same time for the visualization of nano-sized particles it is more prospective to use images in forward scatter electrons in combination with IQ maps. It is established that pearlitic ferrite fragments are not flat. Complicated spatial configuration of orientation inhomogeneities in pearlitic ferrite is shown by means of 3-d reconstruction. The features of ferrites aggregation are revealed depending on pearlitic ferrite fragmentation criterion. The existence of long-range misorientations in the aggregation area of proeutectoid and pearlitic ferrites is shown.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗