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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 973 records · Page 54
All sourcesNASA NTRSDOE OSTI
DOE OSTI2023

Kinetic study of Ni-M/CNT catalyst in methane decomposition under microwave irradiation

Methane catalytic decomposition has been studied with catalysts that can attenuate the energy of electromagnetic waves to heat and drive the reaction. Herein, we report, for the first time, a comprehensive kinetic study of Ni-M (M=Pd, Cu, or Fe)-CNT catalysts under microwave irradiation. These binary metal alloy nanoparticles have been synthesized on multiwalled carbon nanotube support with solvothermal process. These catalysts showed incredible performance for both absorbing microwave energy and catalyzing the reaction to form carbon nanotubes and hydrogen. Ni-M-CNT has a reaction order of 0.74. 10Ni-1 Pd-CNT, 10Ni-1Cu-CNT, and 10Ni-1Fe-CNT have activation energies at 87, 75, and 69 kJ/mol. The investigation was carried out in a differential reactor. The results indicated that 10Ni-1Fe-CNT had the lowest activation energy due to the increase in microwave susceptibility. Here, this work pioneered the microwave catalytic methane decomposition field as well as paving the way for future electrification of CO x -free hydrogen production.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2014

A block-tridiagonal solver with two-level parallelization for finite element-spectral codes

Two-level parallelization is introduced to solve a massive block-tridiagonal matrix system. One-level is used for distributing blocks whose size is as large as the number of block rows due to the spectral basis, and the other level is used for parallelizing in the block row dimension. The reason for the added parallelization dimension is to retard the saturation of the scaling due to communication overhead and inefficiencies in the single-level parallelization only distributing blocks. As a technique for parallelizing the tridiagonal matrix, the combined method of “Partitioned Thomas method” and “Cyclic Odd–Even Reduction” is implemented in an MPI-Fortran90 based finite element-spectral code (TORIC) that calculates the propagation of electromagnetic waves in a tokamak. The two-level parallel solver using thousands of processors shows more than 5 times improved computation speed with the optimized processor grid compared to the single-level parallel solver under the same conditions. Three-dimensional RF field reconstructions in a tokamak are reflected as examples of the physics simulations that have been enabled by this algorithmic advance.

97 MATHEMATICS AND COMPUTING↗
DOE OSTI2023

Model predictive current profile control in tokamaks by exploiting spatially moving electron cyclotron current drives

The plasma control systems in next-generation tokamaks like ITER will balance competing control objectives to achieve the desired level of performance in advanced scenarios while preventing magnetohydrodynamic instabilities and disruptions. During normal tokamak operation, the points of incidence of the electromagnetic waves generated by the electron cyclotron heating and current drives (EC H&CDs) are usually fixed in space. However, the points of incidence can be modified in real-time by changing the angles of the mirrors that reflect the EC H&CD waves. Altering the points of incidence, in turn, varies the ability of the plasma control system to regulate a plasma property. For instance, changing the EC H&CD wave incidence location may place the power demands necessary to achieve a particular plasma target within saturation limits. Therefore, using the EC H&CD deposition location, which is related to the EC H&CD mirror angle, as a supplementary controllable variable may facilitate access to a given target scenario. However, active scenario-control algorithms have not been designed so far to fully exploit this capability in real time. In this work, a model predictive controller that can handle actuation locations as control inputs is developed. In particular, the controller is designed to regulate both the auxiliary powers and the EC H&CD deposition locations in a pre-defined optimal sense to achieve the control objective of attaining and sustaining a target current profile. Further, the proposed controller is tested for a DIII-D tokamak scenario in nonlinear simulations using the Control Oriented Transport SIMulator (COTSIM).

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2025

Multi-frequency progressive refinement for learned inverse scattering

Interpreting scattered acoustic and electromagnetic wave patterns is a computational task that enables remote imaging in a number of important applications, including medical imaging, geophysical exploration, sonar and radar detection, and nondestructive testing of materials. However, accurately and stably recovering an inhomogeneous medium from far-field scattered wave measurements is a computationally difficult problem, due to the nonlinear and non-local nature of the forward scattering process. We design a neural network, called Multi-Frequency Inverse Scattering Network (MFISNet), and a training method to approximate the inverse map from far-field scattered wave measurements at multiple frequencies. We consider three variants of MFISNet, with the strongest performing variant inspired by the recursive linearization method — a commonly used technique for stably inverting scattered wavefield data — that progressively refines the estimate with higher frequency content. MFISNet outperforms past methods in regimes with high-contrast, heterogeneous large objects, and inhomogeneous unknown backgrounds.

97 MATHEMATICS AND COMPUTING↗
DOE OSTI2016

Single-handed helical carbonaceous nanotubes prepared using a pair of cationic low molecular weight gelators

Highlights: • 3-aminophenol-formaldeyde resins were prepared through a templating method. • A pair of cationic gelators have been used as the templates. • Single-handed helical carbonaceous nanotubes were obtained after carbonization. • The carbonaceous nanotubes showed optical activity. - Abstract: We design a facile route to obtain enantiopure carbonaceous nanostructures, which have potential application as chiral sensors, electromagnetic wave absorbers, and asymmetric catalysts. A pair of cationic low molecular weight gelators was synthesized, which were able to self-assemble into twisted nanoribbons in ethanol at a concentration of 20 g L{sup −1} at 25 °C. Single-handed helical 3-aminophenol-formaldehyde resin nanotubes with optical activity were prepared using the self-assembly of the low molecular weight gelators as templates. After carbonization, single-handed helical carbonaceous nanotubes were obtained and characterized using circular dichroism, wide-angle X-ray diffraction, field-emission scanning electron microscopy, transmission electron microscopy, and Raman spectroscopy. The results indicate that the walls of the nanotubes are amorphous carbon. Moreover, the left- and right-handed helical nanotubes exhibit opposite optical activity.

36 MATERIALS SCIENCE↗
DOE OSTI2018

RGO/BaFe12O19/Fe3O4 nanocomposite as microwave absorbent with lamellar structures and improved polarization interfaces

Highlights: • RGO/BaFe{sub 12}O{sub 19}/Fe{sub 3}O{sub 4} nanocomposite are prepared via a two-step solvothermal method. • The maximum reflection loss can reach −46.04 dB, and the effective absorption bandwidth under −10 dB is 5.68 GHz. • Interfacial polarization as one of the mechanism for the enhanced absorption properties was detailedly analyzed. - Abstract: In this paper, we designed and prepared a composite of BaFe{sub 12}O{sub 19} (BFO) flakes, two-dimensional graphene and Fe{sub 3}O{sub 4} nanoparticles using a two-step solvothermal method. The combination of BFO flakes and two-dimensional graphene could effectively enhance the heterointerface and is believed to be favorable to enhance the interface polarization. The introduction of inverse spinel Fe{sub 3}O{sub 4} as the third phase could increase the saturated magnetization. The phase structure, morphology, magnetic properties and electromagnetic wave absorption performance of the as-prepared samples were characterized. Due to the enhanced interfacial polarization between the BaFe{sub 12}O{sub 19} flakes and graphene, the composite of RGO/BaFe{sub 12}O{sub 19}/Fe{sub 3}O{sub 4} exhibits excellent microwave absorption properties. The maximum reflection loss can reach -46.04 dB at 15.6 GHz with a thickness of 1.8 mm, and the effective absorption bandwidth reaches 5.68 GHz (from 11.60 GHz to 17.28 GHz). It is believed that the RGO/BaFe{sub 12}O{sub 19}/Fe{sub 3}O{sub 4} composites can find potential application in the field of microwave absorption due to their excellent absorption properties.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2022

Novel fractal-textured solar absorber surfaces for concentrated solar power

The solar absorptance of a thermal receiver surface significantly affects the photothermal conversion efficiency of concentrated solar power (CSP) plants. The development of low-cost Gen3 CSP systems calls for increasing the solar absorptance of the thermal receivers at operating temperatures above 750 °C. This study presents an innovative approach to the fractal, multiscale texturing of absorber surfaces to significantly enhance solar energy absorption for Gen3 CSP applications. The absorber surface is described in terms of its fractal parameters that are uniquely determined from surface profile measurements. The interaction of solar radiation with the fractal surface is numerically simulated by solving the governing Maxwell’s equations for electromagnetic wave propagation to investigate the effect of texturing on the absorptance of the surfaces. It is shown that absorption of the solar spectrum increases with an increase in the fractal dimension and the multiscale asperity height of the surface texturing. Here, the theoretical model is demonstrated to be in close agreement with experimental measurements of spectral absorptance of electrodeposited copper (Cu), copper mono-oxide (CuO), and copper-manganese oxide (CuMnO) surfaces that are textured to produce a range of fractal parameters by tailoring the deposition parameters. Fractal surface texturing is shown to reduce reflectance by over one order of magnitude, yielding an absorptance of greater than 0.985 for CuMnO. For the first time, the study presents a significant effective means of increasing solar absorptance and a fundamental theoretical description of the underlying physics.

14 SOLAR ENERGY↗
DOE OSTI2021

Multifunctional Metal–Oxide Nanocomposite Thin Film with Plasmonic Au Nanopillars Embedded in Magnetic La 0.67 Sr 0.33 MnO 3 Matrix

Searching for multifunctional materials with tunable magnetic and optical properties has been a critical task toward the implementation of future integrated optical devices. Vertically aligned nanocomposite (VAN) thin films provide a unique platform for multifunctional material designs. In this work, a new metal–oxide VAN has been designed with plasmonic Au nanopillars embedded in a ferromagnetic La 0.67 Sr 0.33 MnO 3 (LSMO) matrix. Such Au–LSMO nanocomposite presents intriguing plasmon resonance in the visible range and magnetic anisotropy property, which are functionalized by the Au and LSMO phase, respectively. Furthermore, the vertically aligned nanostructure of metal and dielectric oxide results in the hyperbolic property for near-field electromagnetic wave manipulation. Such optical and magnetic response could be further tailored by tuning the composition of Au and LSMO phases.

36 MATERIALS SCIENCE↗
DOE OSTI2023

More Than 30 000-fold Field Enhancement of Terahertz Nanoresonators Enabled by Rapid Inverse Design

The rapid development of 6G communications using terahertz (THz) electromagnetic waves has created a demand for highly sensitive THz nanoresonators capable of detecting these waves. Among the potential candidates, THz nanogap loop arrays show promising characteristics but require significant computational resources for accurate simulation. This requirement arises because their unit cells are 10 times smaller than millimeter wavelengths, with nanogap regions that are 1 000 000 times smaller. To address this challenge, we propose a rapid inverse design method using physics-informed machine learning, employing double deep Q-learning with an analytical model of the THz nanogap loop array. In ~39 h on a middle-level personal computer, our approach identifies the optimal structure through 200 000 iterations, achieving an experimental electric field enhancement of 32 000 at 0.2 THz, 300% stronger than prior results. In conclusion, our analytical model-based approach significantly reduces the amount of computational resources required, offering a practical alternative to numerical simulation-based inverse design for THz nanodevices.

21 terahertz time-domain spectroscopy↗
DOE OSTI2016

Profiling Photoinduced Carrier Generation in Semiconductor Microwire Arrays via Photoelectrochemical Metal Deposition

Au was photoelectrochemically deposited onto cylindrical or tapered p-Si microwires on Si substrates to profile the photoinduced charge-carrier generation in individual wires in a photoactive semiconductor wire array. Similar experiments were repeated for otherwise identical Si microwires doped to be n-type. The metal plating profile was conformal for n-type wires, but for p-type wires was a function of distance from the substrate and was dependent on the illumination wavelength. Spatially resolved charge-carrier generation profiles were computed using full-wave electromagnetic simulations, and the localization of the deposition at the p-type wire surfaces observed experimentally correlated well with the regions of enhanced calculated carrier generation in the volumes of the microwires. Finally, this technique could potentially be extended to determine the spatially resolved carrier generation profiles in a variety of mesostructured, photoactive semiconductors.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2017

Hot-Carrier-Mediated Photon Upconversion in Metal-Decorated Quantum Wells

Manipulating the frequency of electromagnetic waves forms the core of many modern technologies, ranging from imaging and spectroscopy to radio and optical communication. The process of converting photons from higher to lower energy is easily accomplished and technologically widespread. However, upconversion, which is the process of converting lower-energy photons into higher-energy photons, is still a growing field of study with nascent applications and burgeoning interest. Here, we experimentally demonstrate a new photon upconversion technique mediated by hot carriers in plasmonic nanostructures. Hot holes and hot electrons generated via plasmon decay in illuminated metal nanoparticles are injected into an adjacent semiconductor quantum well where they radiatively recombine to emit higher-energy photons. Using GaN/InGaN quantum wells decorated with gold and silver nanoparticles, we show photon upconversion from 2.4 to 2.8 eV. The process scales linearly with illumination power and enables both geometry- and polarization-based tunability. The conversion of plasmonic losses into upconverted optical emission has the potential to impact bioimaging, on-chip wavelength conversion, and high-efficiency photovoltaics.

14 SOLAR ENERGY↗
DOE OSTI2018

Low-Loss Near-Infrared Hyperbolic Metamaterials with Epitaxial ITO-In 2 O 3 Multilayers

Artificial metamaterials with hyperbolic dispersions exhibit unusual optical properties not found in Nature. Such hyperbolic metamaterials (HMMs) permit the access to and control of electromagnetic waves with large wave vectors. An important criterion for multilayer-based HMMs is whether the thickness of each individual layer can be far below the operating wavelength while still maintaining the material and interfacial quality. Here in this paper, we report heteroepitaxial growth of HMMs composed of multilayers of ultrathin indium tin oxide (ITO) and indium oxide (In 2 O 3 ) films. In conclusion, the disparate metallic and dielectric properties of the individual building blocks, in conjunction with the good carrier mobility and film morphology enable a low-loss infrared HMM platform on which we demonstrate ultrafast optical switching and the enhancement of the radiative decay rate of PbS quantum dots in the telecommunication wavelength regime.

36 MATERIALS SCIENCE↗
DOE OSTI2014

Directed liquid phase assembly of highly ordered metallic nanoparticle arrays

Directed assembly of nanomaterials is a promising route for the synthesis of advanced materials and devices. We demonstrate the directed-assembly of highly ordered two-dimensional arrays of hierarchical nanostructures with tunable size, spacing and composition. The directed assembly is achieved on lithographically patterned metal films that are subsequently pulse-laser melted; during the brief liquid lifetime, the pattened nanostructures assemble into highly ordered primary and secondary nanoparticles, with sizes below that which was originally patterned. Complementary fluid-dynamics simulations emulate the resultant patterns and show how the competition of capillary forces and liquid metal–solid substrate interaction potential drives the directed assembly. Lastly, as an example of the enhanced functionality, a full-wave electromagnetic analysis has been performed to identify the nature of the supported plasmonic resonances.

77 NANOSCIENCE AND NANOTECHNOLOGY↗
DOE OSTI2018

What Causes Radiation Belt Enhancements: A Survey of the Van Allen Probes Era

We survey radiation belt enhancement events during the Van Allen Probes era to determine what mechanism is the dominant cause of enhancements and where it is most effective. Two primary mechanisms have been proposed: (1) betatron/Fermi acceleration due to the Earthward radial transport of electrons, which produces monotonic gradients in phase space density (PSD), and (2) “local acceleration” due to gyro/Landau resonant interaction with electromagnetic waves, which produces radially localized growing peaks in PSD. Here, to differentiate between these processes, we examine radial profiles of PSD in adiabatic coordinates using data from the Van Allen Probes and Time History of Events and Macroscale Interactions during Substorms satellites for 80 outer belt enhancement events from October 2012 to April 2017. Here, this study shows that local acceleration is the dominant acceleration mechanism for MeV electrons in the outer belt, with 87% of the enhancement events exhibiting growing peaks. The strong correlation of the location of these with geomagnetic activity further supports this conclusion.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2018

Observational Evidence of Magnetic Reconnection in the Terrestrial Bow Shock Transition Region

Here, we report evidence of magnetic reconnection in the transition region of the Earth's bow shock when the angle between the shock normal and the immediate upstream magnetic field is 65°. An ion-skin-depth-scale current sheet exhibits the Hall current and field pattern, electron outflow jet, and enhanced energy conversion rate through the nonideal electric field, all consistent with a reconnection diffusion region close to the X-line. In the diffusion region, electrons are modulated by electromagnetic waves. An ion exhaust with energized field-aligned ions and electron parallel heating are observed in the same shock transition region. The energized ions are more separated from the inflowing ions in velocity above the current sheet than below, possibly due to the shear flow between the two inflow regions. The observation suggests that magnetic reconnection may contribute to shock energy dissipation.

58 GEOSCIENCES↗
DOE OSTI2018

Plasma Anisotropies and Currents in the Near-Earth Plasma Sheet and Inner Magnetosphere

The region occupying radial distances of ~3–9 Earth radii (R E ) in the nightside includes the near-Earth plasma sheet with stretched magnetic field lines and the inner magnetosphere with strong dipolar magnetic field. In this region, the plasma flow energy, which was injected into the inner magnetosphere from the magnetotail, is converted to particle heating and electromagnetic wave generation. These important processes are controlled by plasma anisotropies, which are the focus here. Using measurements of Time History of Events and Macroscale Interactions during Substorms and Van Allen Probes in this transition region we obtain radial profiles of ion and electron temperatures and anisotropies for various geomagnetic activity levels. Ion and electron anisotropies vary with the geomagnetic activity in opposite directions. Parallel anisotropic ions are observed together with transversely anisotropic electrons, whereas the change of ion anisotropy from parallel to transverse (with increasing K p ) is accompanied by the electron anisotropy changing from transverse to parallel. Finally, based on plasma anisotropy observations, we estimate that the anisotropy-related currents (curvature currents) are about 10–20% of the diamagnetic currents.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2020

Solitary Magnetic Structures at Quasi–Parallel Collisionless Shocks: Formation

Solitary magnetic structures known as SLAMS (short large-amplitude magnetic structures) have been considered as essential elements of collisionless shocks with quasi-parallel geometries. Yet the physics underlying their formation remains an open question. In this paper, we use measurements from the magnetospheric multiscale mission combined with fully kinetic simulations to study the formation of SLAMS. We find that gyro-resonance between solar wind ions and right-hand circularly polarized electromagnetic waves results in magnetic field amplification. Gyro-trapping by the growing magnetic field builds up the plasma density that further enhances the current and field. The solitary nature of SLAMS stems from a beat-like magnetic field envelope where the maximum sets the initial location for nonlinear growth. Our results present a conceptual advance on SLAMS, and may shed new light on the open question of magnetic field amplification at astrophysical shocks.

58 GEOSCIENCES↗
DOE OSTI2022

Solitary Magnetic Structures Developed From Gyro-Resonance With Solar Wind Ions at Mars and Earth

We investigate solitary magnetic structures in the foreshock of Mars and Earth. The structures exhibit pulse-like magnetic field and density enhancements along with plasma heating and local solar wind (SW) ion reflection. The structures at Mars resemble the foreshock structures developed from ultra-low-frequency electromagnetic waves gyro-resonant with SW ions at Earth, and propagate toward the magnetosphere. We perform fully kinetic simulations to reproduce the solitary structures and the nonlinear evolution of ion distribution functions, illustrating their resonance with SW ions. The structures present self-induced foreshock turbulence that can have space weather effects. Our results advance the fundamental understanding of how SW interacts with planetary magnetospheres, and have potential impact on the current picture of planet-origin ion escape.

79 ASTRONOMY AND ASTROPHYSICS↗