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At least 955 records · Page 53

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DOE OSTI2023

Molecular beam epitaxy and crystal structure of majority a -plane-oriented and substrate-strained Mn 3 Sn thin films grown directly on sapphire (0001)

The Kagome antiferromagnet Mn 3 Sn has garnered much attention due to the presence of exciting properties such as anomalous Hall and Nernst effects. This paper discusses the synthesis of crystalline Mn 3 Sn thin films, prepared on Al 2 O 3 (0001) substrates at 453 ± 5°C using molecular beam epitaxy. The growth is monitored in situ using reflection high energy electron diffraction and measured ex situ using x-ray diffraction, Rutherford back-scattering, and cross-sectional scanning transmission electron microscopy. Our analysis shows the in-plane lattice constants of a 1,M = 4.117 ± 0.027 Å and a 2,M = 4.943 ± 0.033 Å, which is a very unexpected result when compared to the bulk a-plane Mn 3 Sn. This indicates a strain in the film and makes it challenging to provide a straightforward explanation. In an effort to explain our results, we discuss two possible orientation relationships between the Mn 3 Sn films and the sapphire substrates. Samples prepared under these conditions appear to have smooth surfaces locally, but overall the film has a 3D island morphology. First-principles calculations provide atomic models of the Mn 3 Sn (112¯0) lattice on Al 2 O 3 (0001) high symmetry sites, indicating that the L3-R90° is the most stable configuration. A detailed discussion of the experimental data and theoretical results, as well as strain effects, is provided.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

DOE OSTI2021

Investigations into Spin- and Unpolarized Secondary Electron-Induced Reactions in Self-Assembled Monolayers of Cysteine

Cysteine is the simplest thiolated, chiral amino acid and is often used as the anchor for studies of self-assembled monolayers (SAMs) of complex biomolecules such as peptides. Understanding the interaction of SAMs of cysteine with low-energy secondary electrons (SEs) produced by X-rays can further our understanding of radiation damage in biomolecules. In particular, if the electrons are polarized, chiral-selective chemistry could have bearing on the origin of homochirality in nature. In the present paper, we use synchrotron radiation-based X-ray photoelectron spectroscopy to determine the changes that occur in the bonding of self-assembled layers of cysteine on gold as a result of soft X-ray irradiation. To investigate the possibility of chiral selectivity resulting from the interaction of low-energy, spin-polarized SEs (SPSEs), measurements were conducted on cysteine adsorbed on a 3 nm-thick gold layer deposited on a CoPt thin-film multilayer with perpendicular magnetic anisotropy. Time-dependent measurements of the C 1s, N 1s, O 1s, S 2p, and Au 4f core levels are used to follow the changes in surface chemistry and determine reaction cross-sections as a function of SE exposure. Analysis of the data results in cross-sections in the range of 5-7 Mb and suggests possible reaction pathways. Changing the magnetization direction of the CoPt multilayer produces SPSEs with opposite polarity. Some evidence of spin-dependent reactions is indicated but is inconclusive. Possible reasons for the discrepancy are posited.

38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEA↗

NASA NTRS1971

Development of a collapsible reinforced cylindrical space observation window

Existing material technology was applied to the development of a collapsible transparent window suitable for manned spacecraft structures. The effort reported encompasses the evaluation of flame retardants intended for use in the window matrix polymer, evaluation of reinforcement angle which would allow for a twisting pantographing motion as the cylindrical window is mechanically collapsed upon itself, and evaluation of several reinforcement embedment methods. A fabrication technique was developed to produce a reinforced cylindrical space window of 45.7 cm diameter and 61.0 cm length. The basic technique involved the application of a clear film on a male-section mold; winding axial and girth reinforcements and vacuum casting the outer layer. The high-strength transparent window composite consisted of a polyether urethane matrix reinforced with an orthogonal pattern of black-coated carbon steel wire cable. A thin film of RTV silicone rubber was applied to both surfaces of the urethane. The flexibility, retraction system, and installation system are described.

Khan, A. Q.↗

NASA NTRS1975

Inviscid interpenetration of two streams with unequal total pressures

A theory is proposed for analyzing the inviscid interpretation of two streams in the case when the difference in total pressure between the streams is relatively small. A stream is considered which discharges from a nozzle or reservoir into a partially moving and partially stationary environment in such a way that the flows leave the solid boundaries in a tangential direction where the two streams first interact. The problem is solved by expanding in a small parameter related to the difference in total pressure between the streams, the zeroth-order solution is obtained by classical methods, and a technique similar to that employed in thin-airfoil theory is used to transfer the first-order boundary conditions to the zeroth-order boundary. A procedure is developed to transform the problem into one that can be solved by standard techniques of the theory of sectionally analytic functions. Solutions are obtained for flows with and without free streamlines, and the general theory is applied to several specific flow configurations.

Goldstein, M. E.↗

NASA NTRS1985

Numerical methods for analyzing electromagnetic scattering

Attenuation properties of the normal modes in an overmoded waveguide coated with a lossy material were analyzed. It is found that the low-order modes, can be significantly attenuated even with a thin layer of coating if the coating material is not too lossy. A thinner layer of coating is required for large attenuation of the low-order modes if the coating material is magnetic rather than dielectric. The Radar Cross Section (RCS) from an uncoated circular guide terminated by a perfect electric conductor was calculated and compared with available experimental data. It is confirmed that the interior irradiation contributes to the RCS. The equivalent-current method based on the geometrical theory of diffraction (GTD) was chosen for the calculation of the contribution from the rim diffraction. The RCS reduction from a coated circular guide terminated by a PEC are planned schemes for the experiments are included. The waveguide coated with a lossy magnetic material is suggested as a substitute for the corrugated waveguide.

Lee, S. W.↗

NASA NTRS1987

Research sensors

The program described covers development of sensors and sensing techniques for research applications on aeropropulsion systems. In general, the sensors are used in-situ to measure the environment at a given location within a turbine engine, or to measure the response of an engine component to the imposed environment. Locations of concern are generally in the gas path and, for the most part, are within the hot section. Specific parameters of concern are dynamic gas temperature, heat flux, airfoil surface temperature, and strain on airfoils and combustor liners. In order to minimize the intrusiveness of surface-mounted sensors, a considerable effort was expended to develop thin-film sensors for surface temperature, strain, and heat flux measurements. Most of the work described is sufficiently advanced that sensors were used and useful data were obtained. The notable exception is the work to develop a high-temperature static strain measuring capability; this work is still in progress.

Englund, David R.↗

NASA NTRS1989

Nuclear fragmentation studies for microelectronic application

A formalism for target fragment transport is presented with application to energy loss spectra in thin silicon devices. Predicted results are compared to experiments with the surface barrier detectors of McNulty et al. The intranuclear cascade nuclear reaction model does not predict the McNulty experimental data for the highest energy events. A semiempirical nuclear cross section gives an adequate explanation of McNulty's experiments. Application of the formalism to specific electronic devices is discussed.

Ngo, Duc M.↗

NASA NTRS1991

Tiltrotor research aircraft composite blade repairs: Lessons learned

The XV-15, N703NA Tiltrotor Research Aircraft located at the NASA Ames Research Center, Moffett Field, California, currently uses a set of composite rotor blades of complex shape known as the advanced technology blades (ATBs). The main structural element of the blades is a D-spar constructed of unidirectional, angled fiberglass/graphite, with the aft fairing portion of the blades constructed of a fiberglass cross-ply skin bonded to a Nomex honeycomb core. The blade tip is a removable laminate shell that fits over the outboard section of the spar structure, which contains a cavity to retain balance weights. Two types of tip shells are used for research. One is highly twisted (more than a conventional helicopter blade) and has a hollow core constructed of a thin Nomex-honeycomb-and-fiberglass-skin sandwich; the other is untwisted with a solid Nomex honeycomb core and a fiberglass cross-ply skin. During initial flight testing of the blades, a number of problems in the composite structure were encountered. These problems included debonding between the fiberglass skin and the honeycomb core, failure of the honeycomb core, failures in fiberglass splices, cracks in fiberglass blocks, misalignment of mated composite parts, and failures of retention of metal fasteners. Substantial time was spent in identifying and repairing these problems. Discussed here are the types of problems encountered, the inspection procedures used to identify each problem, the repairs performed on the damaged or flawed areas, the level of criticality of the problems, and the monitoring of repaired areas. It is hoped that this discussion will help designers, analysts, and experimenters in the future as the use of composites becomes more prevalent.

Espinosa, Paul S.↗

NASA NTRS1992

Tiltrotor Research Aircraft composite blade repairs - Lessons learned

Espinosa, Paul S.↗

NASA NTRS1994

Head-on parallel blade-vortex interaction

An experimental and computational study was carried out to investigate the parallel head-on blade-vortex interaction (BVI) and its noise generation mechanism. A shock tube, with an enlarged test section, was used to generate a compressible starting vortex which interacted with a target airfoil. The dual-pulsed holographic interferometry (DPHI) technique and airfoil surface pressure measurements were employed to obtain quantitative flow data during the BVI. A thin-layer Navier-Stokes code (BV12D), with a high-order upwind-biased scheme and a multizonal grid, was also used to simulate numerically the phenomena occurring in the head-on BVI. The detailed structure of a convecting vortex was studied through independent measurements of density and pressure distributions across the vortex center. Results indicate that, in a strong head-on BVI, the opposite pressure peaks are generated on both sides of the leading edge as the vortex approaches. Then, as soon as the vortex passes by the leading edge, the high-pressure peak suddenly moves toward the low-peak-reducing in magnitude as it moves--simultaneously giving rise to the initial sound wave. In both experiment and computation, it is shown that the viscous effect plays a significant role in head-on BVIs.

Lee, Soogab↗

NASA NTRS2005

Quantifying the Material Processing Conditions for an Optimized FSW Process

In friction stir welding (FSW), a rotating threaded pin tool is inserted into a weld seam and literally stirs the edgs of the seam together. This environmentally friendly, solid-state technique has been successfully used in the joining of materials that are difficult to fusion weld. To determine optimal processing parameters for producing a defect free weld, a better understanding of the resulting metal deformation flow path and velocity is required. In this study the metal flow fields are marked by the use of thin (0.001 in. tungsten) wires embedded in the weld seam at various locations. X-ray radiographs record the position and segmentation of the wire and are used to elucidate the flow field. Microstructures observed in a FSW cross-section in an aluminum alloy are related to their respective strain-strain rate-temperature histones along their respective flow trajectories. Two kinds of trajectories, each subjecting the weld metal to a distinct thermomechanical process and imparting a distinct microstructure, can be differentiated within the weld structure.

Schneider, Judy↗

DOE OSTI2023

Probing Fundamental Mechanisms of Plastic Deformation with High Energy X-rays (Final Progress Report)

Overall, substantial progress was made on developing BCDI techniques in the direction of imaging defects in multi-crystal samples. Section 2.1 describes a new method to reconstruct the 3D atomic displacement field within a grain from multiple coherently resolved diffraction peaks. The key development is the ability to recover a best fit to the grain shape at the same time as the internal displacement (strain) variation with no prior knowledge of the microstructure. This is complemented by the development of a method, Sec. 2.2, to separate out sets of Laue reflections that belong to a single grain (and thus be able to index its orientation) in the commonly encountered situation in which the beam illuminates several grains in a given location. This is essential for enabling collection of coherent diffraction data (at APS 34-ID-C) from neighboring grains. All experiments depend on the quality of samples used. Although good progress has been made with thin film samples, we are working with a broader range of geometries. A new sample design uses a high-Z metal (e.g., Pt) deposited in a sub-micron trench in a low-Z metal (e.g., Al) so that the grain size is prevented from exceeding the current limit for BCDI. We also report in section 3.1 on successfully applying NF-HEDM to a fine-grain Mg sample that would normally be considered out of scope for the method. This represents progress towards being able to map out polycrystalline samples in 3D before performing BCDI on individual grains. We further report in section 3.2 on preliminary NF-HEDM characterization of a sample of UO2 that has sub-micron grains; the data imply the capability of mapping fine-grain polycrystals at 1-ID-E, again for the purposes of BCDI in the bulk. Lastly, our plan is to load grains in polycrystalline samples by inducing thermal stress. We also report the experimental measurements of the Ti- 6Al-4V alloy obtained at the European Synchrotron Radiation Facility (ESRF), which had been indexed and mapped via HEDM at APS in section 9. As discussed below, however, technique development pre-occupied the team throughout the project which meant that we did not make any significant progress towards answering the original hypotheses as stated in the proposal. In summary, we assert that we have made good progress in methods and samples and future work taking advantage of this progress is likely to obtain and analyze BCDI data from multiple adjacent grains in 3D polycrystals. Obtaining such data depends on re-gaining access to the Advanced Photon Source, which is anticipated in late summer or the Fall. In all cases, work has involved close collaboration with faculty, staff, postdocs and students from Brigham Young University (BYU), the Los Alamos National Laboratory and APS beamlines 1-ID and 34-ID.

36 MATERIALS SCIENCE↗

DOE OSTI2026

Precise 2D electric field density simulations for superconducting quantum devices

Dielectric loss due to two-level systems is a limiting factor for superconducting qubit relaxation times. These losses arise mostly from nanometer-scale interfacial defect regions in superconducting devices with planar dimensions of microns to millimeters, thus making it resource intensive to accurately simulate the electric field density in these regions with traditional electromagnetic solvers. In this work, we demonstrate a fast boundary integral equation solver that allows precise simulation of electric field density in these thin regions, showing a speedup of around two orders of magnitude over traditional solvers, with relative errors around $10^{-7}$ for a ten-minute solution runtime. By computing participation ratios through Green's first identity without squaring the electric field, our approach is less susceptible to the field singularities near conductor corners. We apply this solver to a basic untrenched coplanar waveguide cross-section, showing that the common assumption of participation ratio linearity with dielectric constant holds well for some interfaces and not others; in particular, while the metal-air (MA) top and corner follow this linear relationship strongly, the MA sidewall does not. We then compare isotropic and anisotropic etching, showing that the MA sidewall and the metal-air-substrate triple junction are the most strongly affected. We are currently leveraging this solver to explore geometries that will uniquely isolate the participation ratios of the different dielectrics. Finally, we are working to combine this solver framework with a full 3D microwave solver to accurately calculate participation ratios for the thin dielectrics that are known sources of loss in superconducting qubits.

Gimbutas, Z. [NIST, Boulder] (ORCID:00000003320982↗

NASA NTRS1987

CSCM methodology for slot injection cooled cavity flow design in a high enthalpic stream

The CSCM method for the compressible Navier-Stokes equations is applied to study design factors in a slot injection cooled cavity flow in the side of a 2-D wedge body in a high enthalpy free stream. The flow geometry is being designed and will be tested in an arc jet tunnel at NASA-Ames Research Center. Objectives of the design are to provide adequate thermal protection for and minimize aero-optical distortion in the path above a window located in the bottom of the cavity. Among design issues, are the geometry of and flow conditions in the expanding section of the supersonic slot injection nozzle. Here, for straight walled nozzles, two geometries are considered for the upper nozzle lip between the hot, high speed outer flow and the colder, denser cooling flow. The two lip geometries - thick, square and thin, wedge - as the result of associated widely differing base/wake flows also exhibit different and interesting viscous-inviscid flow structures near the ramp termination to the cavity. For the thin lip case, the consequences on flow quality of off design nozzle conditions relative to matching pressure with the outer flow are explored.

Bardina, Jorge↗

NASA NTRS1986

Precision cast vs. wrought superalloys

While cast polycrystalline superalloys recommend themselves in virtue of better 'buy-to-fly' ratios and higher strengthening gamma-prime volume fractions than those of wrought superalloys, the expansion of their use into such critical superalloy applications as gas turbine hot section components has been slowed by insufficient casting process opportunities for microstructural control. Attention is presently drawn, however, to casting process developments facilitating the production of defect-tolerant superalloy castings having improved fracture reliability. Integrally bladed turbine wheel and thin-walled turbine exhaust case near-net-shape castings have been produced by these means.

Tien, J. K.↗

NASA NTRS1991

Evaluation of a three-dimensional Navier-Stokes solver for transonic flow over a low-aspect-ratio wing mounted in a wind tunnel

A three dimensional Navier-Stokes solver is evaluated for transonic flow over a thin, swept, low-aspect ratio wing. The computational study was undertaken in support of a wind tunnel experimental program. The computational results are compared to experimental surface pressure data obtained in a cryogenic wind tunnel with an adaptive wall test section. The results show favorable agreement over a wide range of conditions, further the numerical results provide additional data of the complex three-dimensional flow field. Differences in the predictions and experiment suggest a need to conduct further experiments to evaluate the adaptive wall testing technique, and to model the tunnel sidewall boundary layer in the computations.

Milholen, William E., II↗

NASA NTRS1994

Footprints of storms on the sea: A view from spaceborne synthetic aperture radar

Synthetic aperture radar (SAR) on board Seasat observed images of stormlike echoes on the sea in 1978. The core of these images is usually an echo-free hole which is attributed to the damping of the short (30-cm) radar detectable gravity waves by the intense rain in the storm core. Although 'the beating down of waves by rain' is consistent with observations by seafarers and with the first scientific explanation of the phenomenon by Reynolds (1875), neither theory nor experiment has provided definitive support. One experiment appears to provide the key; it shows that the kenetic energy of the rain produces sufficient turbulence in a thin fresh water layer to damp 30-cm waves in 10-20 s, thus producing the echo-free hole. A sequence of positive feedbacks then serves to damp the longer waves. The angular dependence of the sea surface echo cross sections seen by Seasat SAR outside the echo-free hole indicates winds diverging from the downdraft induced by the intense rain core. The wind-generated waves and associated echoes extend out to a sharply defined gust front. The sea surface footprint thus mimics the features of a storm microburst. The variations in surface radar cross section due to a combination of rain and wind effects impacts spaceborne measurements of surface winds by scatterometry and rainfall measurements by radar. Portions of this synthesis remain speculative but serve as hypotheses for further research.

Atlas, David↗

NASA NTRS1998

Design Considerations for Lightweight Space Radiators Based on Fabrication and Test Experience with a Carbon-Carbon Composite Prototype Heat Pipe

This report discusses the design implications for spacecraft radiators made possible by the successful fabrication and Proof-of-concept testing of a graphite-fiber-carbon-matrix composite (i.e., carbon-carbon (C-C)) heat pipe. The proto-type heat pipe, or space radiator element, consists of a C-C composite shell with integrally woven fins. It has a thin-walled furnace-brazed metallic (Nb-1%Zr) liner with end caps for containment of the potassium working fluid. A short extension of this liner, at increased wall thickness beyond the C-C shell, forms the heat pipe evaporator section which is in thermal contact with the radiator fluid that needs to be cooled. From geometric and thermal transport properties of the C-C composite heat pipe tested, a specific radiator mass of 1.45 kg/m2 can be derived. This is less than one-fourth the specific mass of present day satellite radiators. The report also discusses the advantage of segmented space radiator designs utilizing heat pipe elements, or segments, in their survivability to micro-meteoroid damage. This survivability is further raised by the use of condenser sections with attached fins, which also improve the radiation heat transfer rate. Since the problem of heat radiation from a fin does not lend itself to a closed analytical solution, a derivation of the governing differential equation and boundary conditions is given in appendix A, along with solutions for rectangular and parabolic fin profile geometries obtained by use of a finite difference computer code written by the author.

Juhasz, Albert J.↗