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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 955 records · Page 53
All sourcesNASA NTRSDOE OSTI
NASA NTRS1987

Langmuir probe surveys of an arcjet exhaust

Electrostatic (Langmuir) probes of both spherical and cylindrical geometry have been used to obtain electron number density and temperature in the exhaust of a laboratory arcjet. The arcjet thruster operated on nitrogen and hydrogen mixtures to simulate fully decomposed hydrazine in a vacuum environment with background pressures less than 0.05 Pa. The exhaust appears to be only slightly ionized (less than 1 percent) with local plasma potentials near facility ground. The current-voltage characteristics of the probes indicate a Maxwellian temperature distribution. Plume data are presented as a function of arcjet operating conditions and also position in the exhaust.

Zana, Lynnette M.↗
DOE OSTI2023

Fiber-Optic Raman Probe for On-line EAF Slag Analysis

Here, in Electric Arc Furnace (EAF) steelmaking, the push for improved efficiency requires accurate analysis of the chemical composition of its slag system to control slag foaming, provide refractory protection, and maintain high furnace iron yield. Therefore, the ability to obtain real-time slag chemistry data would provide a useful tool to improve the control and efficiency of the process. The work reported here aims to assess the structure and chemistry of EAF slags at high temperatures using a portable fiber-optic Raman probe. As a result, the ability to relate Raman spectra peaks to chemistry and structure is demonstrated in experimental result with EAF slags at 1550°C.

47 OTHER INSTRUMENTATION↗
DOE OSTI2023

In situ saxs characterization of thermoresponsive behavior of a poly(ethylene glycol)-graft-(poly(vinyl caprolactam)-co-poly(vinyl acetate)) amphiphilic graft copolymer

In this work, we report the thermoresponsive assembly and rheology of an amphiphilic thermosensitive graft copolymer, poly(ethylene glycol)-graft-(poly(vinyl caprolactam)-co-poly(vinyl acetate)) (commercial name Soluplus ® ), which has been investigated for potential biomedical applications. It has received attention due to is ability to solubilize hydrophobic drugs and for its thickening behavior close to body temperature. Through use of the synchrotron at Brookhaven National Lab, and collaboration with the department of energy, the nanoscale structure and properties can be probed in greater detail. Soluplus ® undergoes two structural changes as temperature is increased; the first, a concentration independent change where samples become turbid at 32 °C. Increasing the temperature further causes the formation of physically associated hydrogels. This sol-gel transition is concentration dependent and occurs at 32 °C for 40 wt% samples, and increases to 42 °C for 10 wt% samples. From variable temperature SAXS characterization micelles of 20–25 nm in radius can be seen and maintain their size and packing below 32 °C. A gradual increase in the aggregation of micelles corresponding to a thickening of the material is also observed. Close to and above the gelation temperature, micelles collapse and form a physically associated 3D network. A model is proposed to explain these physical effects, where the poly(vinyl caprolactam) group transitions from the hydrophilic corona at room temperature to the hydrophobic core as temperature is increased.

36 MATERIALS SCIENCE↗
NASA NTRS1993

Kinetics of the Reaction C2H + O2 from 193 to 350 K Using Laser Flash Kinetic Infrared Absorption Spectroscopy

Rate coefficients for the reaction C2H + O2 are measured from 193 to 350 K by using transient absorption spectroscopy with an infrared color center laser. Ethynyl radicals are produced by pulsed laser photolysis of C2H2 in a temperature variable flow cell and a tunable color center laser probes the transient removal Of C2H ((bar-X(sup 2))Sigma(+))(0,0,0)) in absorption. The rate coefficient has a slight negative temperature dependence over the range 193-350 K which can be expressed as k(O2) = (1.5 +/- 0.3) x 10(exp -11) exp((230 +/- 36)/T) Cu cm/(Molecule.s). The lack of a pressure dependence under our experimental conditions strongly suggests that the HCCOO* complex is short lived with respect to encountering a collision and rapidly dissociates to products without competition from collisional stabilization to HCCOO or collisionally induced dissociation to reactants.

Opansky, Brian J.↗
DOE OSTI2024

Site requirements for inhibition-free CO oxidation over silica-supported bimetallic PdCu alloys

Pd catalysts are highly active for CO oxidation but suffer from inhibition by NO at low temperatures (<150 °C). We posit that incorporation of Cu into the Pd catalyst will improve low-temperature CO oxidation activity and reduce inhibition from competitive adsorbers. To probe this hypothesis, a series of PdCu alloys with different Pd : Cu ratios were synthesized and tested in the temperature-programmed oxidation of CO in the presence and absence of NO. Incorporation of small amounts of Cu into Pd improves the reactivity, as well as the resistance to NO inhibition. Beyond this, Cu incorporation into the Pd has a detrimental effect on the activity for CO oxidation. Based on combined infrared and X-ray absorption spectroscopy studies, here we show that high activity and resistance to inhibition requires alloying of Pd and Cu and the formation of a diverse surface, while surface segregation of Cu results in poor activity and inhibition.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
NASA NTRS1988

An Experimental Investigation of an Arcjet Thruster Exhaust Using Langmuir Probes

Electrostatic (Langmuir) probes of both spherical and cylindrical geometry have been used to obtain electron number density and temperature in the exhaust of a laboratory arcjet. The arcjet thruster operated on nitrogen and hydrogen mixtures to simulate fully decomposed hydrazine in a vacuum environment with background pressures less than 5 x 10 to the -2 Pa. The exhaust appears to be only slightly ionized (less than 1 percent) with local plasma potentials near facility ground. The current-voltage characteristics of the probes indicate a Maxwellian temperature distribution. Plume data are presented as a function of arcjet operating condition and also position in the exhaust.

Carney, Lynnette M.↗
DOE OSTI2022

Temperature Mapping of Stacked Silicon Dies from X-Ray-Diffraction Intensities

Increasing power densities in integrated circuits have led to an increased prevalence of thermal hotspots in integrated circuits. Tracking these thermal hotspots is imperative to prevent circuit failures. In three- dimensional (3D) integrated circuits, conventional surface techniques like infrared thermometry are unable to measure the 3D temperature distribution, and optical and magnetic resonance techniques are difficult to apply due to the presence of metals and large current densities. X-rays offer a high penetration depth and can be used to probe 3D structures. We report a method utilizing the temperature dependence of x-ray-diffraction intensity via the Debye-Waller factor to simultaneously map the temperature of individual silicon dies in a stack. Here, utilizing beamline 1-ID-E at the Advanced Photon Source (Argonne), we demonstrate, for each individual silicon die, a temperature resolution of 3 K, a spatial resolution of 100 × 400 μm 2 , and a temporal resolution of 20 s. Utilizing a sufficiently high-intensity laboratory source, e.g., from a liquid-anode source, this method can be scaled down to laboratories for noninvasive temperature mapping of 3D integrated circuits.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
NASA NTRS1992

Measurements of density, temperature, and their fluctuations in turbulent supersonic flow using UV laser spectroscopy

Nonintrusive measurements of density, temperature, and their turbulent fluctuation levels were obtained in the boundary layer of an unseeded, Mach 2 wind tunnel flow. The spectroscopic technique that was used to make the measurements is based on the combination of laser-induced oxygen fluorescence and Raman scattering by oxygen and nitrogen from the same laser pulse. Results from this demonstration experiment are compared with previous measurements obtained in the same facility using conventional probes and an earlier spectroscopic technique. Densities and temperatures measured with the current technique agree with the previous surveys to within 3 percent and 2 percent, respectively. The fluctuation amplitudes for both variables agree with the measurements obtained using the earlier spectroscopic technique and show evidence of an unsteady, weak shock wave that perturbs the boundary layer.

Fletcher, Douglas G.↗
DOE OSTI2023

Probing the Electronic and Opto-Electronic Properties of Multilayer MoS 2 Field-Effect Transistors at Low Temperatures

Transition metal dichalcogenides (TMDs)-based field-effect transistors (FETs) are being investigated vigorously for their promising applications in optoelectronics. Despite the high optical response reported in the literature, most of them are studied at room temperature. To extend the application of these materials in a photodetector, particularly at a low temperature, detailed understanding of the photo response behavior of these materials at low temperatures is crucial. Here we present a systematic investigation of temperature-dependent electronic and optoelectronic properties of few-layers MoS 2 FETs, synthesized using the mechanical exfoliation of bulk MoS 2 crystal, on the Si/SiO 2 substrate. Our MoS 2 FET show a room-temperature field-effect mobility μ FE ~40 cm 2 ·V -1 ·s -1 , which increases with decreasing temperature, stabilizing at 80 cm 2 ·V -1 ·s -1 below 100 K. The temperature-dependent (50 K < T < 300 K) photoconductivity measurements were investigated using a continuous laser source λ = 658 nm (E = 1.88 eV) over a broad range of effective illuminating laser intensity, P eff (0.02 μW < P eff < 0.6 μW). Photoconductivity measurements indicate a fractional power dependence of the steady-state photocurrent. The room-temperature photoresponsivity (R) obtained in these samples was found to be ~2 AW -1 , and it increases as a function of decreasing temperature, reaching a maximum at T = 75 K. The optoelectronic properties of MoS 2 at a low temperature give an insight into photocurrent generation mechanisms, which will help in altering/improving the performance of TMD-based devices for various applications.

2D materials↗
NASA NTRS1973

A cooled-gas pyrometer for use in hypersonic engine testing

A cooled-gas pyrometer designed for application in a hypersonic research engine program was fabricated and tested. Design and operational considerations and calibration data are presented. The probe was tested in a rocket-engine exhaust stream operating at Mach 2 and 2300 K. Test temperature measurements agreed to within 2 percent with a radiation shielded thermocouple probe.

Glawe, G. E.↗
DOE OSTI2021

Study of detached plasma profile in the divertor simulation experimental module of tandem mirror GAMMA 10/PDX

A divertor simulation experimental module (D-module) in the tandem mirror GAMMA 10/PDX was used for the study of plasma detachment. In previous studies, it was difficult to measure far-upstream plasma parameters in the D-module, and only electrostatic probes on the target plate were used to perform electron temperature and density measurements. Furthermore, to study the detached plasma structure, a Thomson scattering (TS) system and a microwave interferometer system have been installed to measure the inside plasma parameters of the D-module, and a movable electrostatic probe has been placed at the inlet of the D-module to measure the inlet plasma density and temperature. The TS system in the central cell observed the electron temperature and density of the core plasma simultaneously. These measurements revealed the entire density and temperature structure from the core plasma to the divertor plate. The line average electron density measured by the microwave interferometer showed a rollover behavior during detachment. The results indicated that the ionization region was located around the center of the D-module, and it appears to move upstream along the axis.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
NASA NTRS1971

Frequency response studies for a wedge probe in viscoelastic fluids.

Investigation of a hot-film wedge probe in viscoelastic fluids by imposing on the probe a sinusoidal vibration of known amplitude and frequency. Root-mean-square (rms) velocities calculated from the displacement of the probe are compared to rms velocities obtained with a constant temperature anemometer. The tests were performed under turbulent flow conditions and also at flow rates where viscoelastic effects, i.e., decrease of heat transfer rates from the probe to the fluid and drag reduction, were observed. The experimental technique was established by measuring the response of the probe in mineral oil.

Rodriguez, J. M.↗
NASA NTRS1982

A hot-film static-pressure probe

The procedure described involves calibrating the probe in the gas of interest over the range of temperatures and pressures anticipated in the wind-tunnel tests and then applying the calibration to reduce the data from those tests. Pressure readings from two probes, one having two hot-film sensors and an internal sonic orifice and the other connected to a conventional pressure gage, are recorded for several Reynolds numbers and compared. The conventional static-pressure probe with a pair of hot-film sensors and an interior sonic orifice is shown to provide the means of surveying flowfields in hypersonic flow at a rapid rate and with an accuracy of better than + or - 10%.

Ashby, G. C., Jr.↗
NASA NTRS1979

Calorimeter probes for measuring high thermal flux

The paper describes expendable, slug-type calorimeter probes developed for measuring high heat-flux levels of 10-30 kW/sq cm in electric-arc jet facilities. The probes are constructed with thin tungsten caps mounted on Teflon bodies; the temperature of the back surface of the tungsten cap is measured, and its rate of change gives the steady-state, absorbed heat flux as the calorimeter probe heats to destruction when inserted into the arc jet. It is concluded that the simple construction of these probes allows them to be expendable and heated to destruction to obtain a measurable temperature slope at high heating rates.

Russell, L. D.↗
NASA NTRS1993

Laboratory studies of low temperature rate coefficients: The atmospheric chemistry of the outer planets

The objectives are to measure laboratory rate coefficients for key reactions of hydrocarbon molecules and radicals at low temperatures, which are relevant to the atmospheric photochemistry of Saturn, Jupiter, and Titan. Upcoming NASA planetary missions, such as Cassini, will probe the atmosphere of Titan in more detail, offering an excellent opportunity to test kinetic models and to establish fiducial standards for using kinetic models to interpret various parameters of the outer planets. Accurate low temperature kinetic data, which are presently lacking, may require crucial revisions to the rates of formation and destruction and are of utmost importance to the success of these efforts. In this program, several key reactions of ethynyl radicals (C2H) with acetylene (C2H2), methane (CH4), and oxygen (O2), down to temperatures of 170 K were successfully investigated. The experimental apparatus developed in our laboratory for measuring reaction kinetics at low temperatures consists of a laser photolysis/infrared probe laser setup. The rate measurements are carried out as a function of (low) temperature with a transverse flow cell designed specifically for these studies. A 193 nm argon fluoride pulsed excimer laser is used to photolyze a suitable precursor molecule, such as acetylene to produce C2H, and a high resolution, tunable infrared F-center laser (2.3-3.35 mu m) probes the transient concentrations of the radical species directly in absorption to extract the kinetic rate coefficients.

Leone, Stephen R.↗
NASA NTRSDate not supplied

Entry, Descent, and Landing Analysis of Low Mass Martian Probe for Surface Climate Network

Aeolus is a mission to provide the first direct measurements of Martian atmospheric wind speeds and correlate them with thermal and compositional data to bring together a complete systematic description for the global energy balance and climate cycles of Mars. Objective A of the Mars Exploration Program Analysis Group (MEPAG) Goal II cites a Science Investigation Area to develop a network of surface landers to provide global, diurnal and synoptic coverage of the near-surface environment to characterize present Mars climate [1]. Aeolus will characterize the present Martian global climate system via an orbiter element and a novel surface network element. A series of low mass, low power probes will be distributed across the Martian surface and measure pressure, sky opacity, temperature, wind speed, water vapor and other trace gases. Low mass and power electrical systems designed to operate in extreme cold and daily thermal cycling for one Martian year could facilitate lower cost, Class-D science probes. Aeolus is targeting a total per-probe mass of <5 kg. Recent advances in nanofabrication of chip-scale sensors that are highly robust to temperature and shock, combined with a novel packaging concept (the deployable sensor probe [2]) originally developed by the Aerospace Corp., for the first time enables a Mars surface climate sensor network. These probes are folded flat during transit to Mars and automatically deploy into the final reentry configuration once released from the orbiter. The capability to fold for stowage significantly increases the probe quantity carried by the orbiter.

EDL↗
NASA NTRS2003

An Ultrasonic Sampler and Sensor Platform for In-Situ Astrobiological Exploration

The search for existing or past life in the Universe is one of the most important objectives of NASA's mission. In support of this objective, ultrasonic based mechanisms are currently being developed at JPL to allow probing and sampling rocks as well as perform as a sensor platform for in-situ astrobiological analysis. The technology is based on the novel Ultrasonic/Sonic Driller/Corer (USDC), which requires low axial force, thereby overcoming one of the major limitations of planetary sampling in low gravity using conventional drills. The USDC was demonstrated to: 1) drill ice and various rocks including granite, diorite, basalt and limestone, 2) not require bit sharpening, and 3) operate at high and low temperatures. The capabilities that are being investigated including probing the ground to select sampling sites, collecting various forms of samples, and hosting sensors for measuring chemical/physical properties. A series of modifications of the USDC basic configuration were implemented leading an ultrasonic abrasion tool (URAT), Ultrasonic Gopher for deep Drilling, and the lab-on-a-drill.

robotics↗