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All sourcesNASA NTRSDOE OSTI
DOE OSTI2014

TU-F-BRE-01: A High Resolution Micro Fiber Scintillator Detector Optimized for SRS and SBRT in Vivo Real Time Treatment Verification

Purpose: We have built a high resolution real time scintillating fiber detector prototype to determine in real time the accuracy of stereotactic radiosurgery (SRS) and stereotactic body radiotherapy (SBRT) treatments when only a fraction of the planned dose was delivered. The motivation of this work is to enhance dose delivery accuracy and to achieve error free radiosurgery. Methods: A high density array of scintillating fibers and a high speed photo detectors array were integrated to implement a high resolution real time dosimeter that can sample with high resolution pulsed SRS and SBRT beams cross sections. The high efficiency of the developed system allows to read each linac pulse in real time and to compute the accumulated dose and dose errors when only a fraction of the beam was delivered. The fibers are highly packed in a substrate that is directly coupled to two 128 pixel arrays with a pitch matching the fiber spacing to achieve accurate spatial localization. The small cross section of the fiber array allows stacking multiple fiber arrays to measure independent angular profiles that are digitally processed in parallel for real time dosimetry. Results: We implemented a high density array detector prototype with a pitch of 0.5 mm, readout speed of 1.2 msec, and a response time of 0.5 usec. The fast reading speed has the capability to determining the dose in flattening free filter beams. The detector can be installed in transmission mode at the output port of a micro-MLC. Treatment deviations smaller than 3% are detected when less than 1/100 of the planned dose was delivered. Conclusions: We built a prototype of a high resolution fiber scintillator array detector for SRS and SBRT in vivo dosimetry. Results show that the developed detector has the potential to assure error free SRS and SBRT treatments.

60 APPLIED LIFE SCIENCES↗
DOE OSTI2013

MECHANICAL PROPERTIES AND MICROSTRUCTURAL CHARACTERIZATION OF A MULTILAYERED MULTIPASS FRICTION STIR WELD IN STEEL

Multilayered multipass friction stir welding (MM-FSW) makes it possible to use FSW to fabricate thick-section structures. In this work, MM-FSW was demonstrated on a high strength low alloy steel; ASTM A572 Grade 50. Three steel plates with thicknesses of 0.18", 0.18", 0.24" respectively were stacked and friction stir welded together to form a 0.6" thick welded structure. The welded plate was sectioned into rectangular bars transverse to the weld direction for tensile testing to evaluate mechanical properties. Digital image correlation (DIC) was employed to map the local strain fields during tensile testing. The initial failure was found to occur simultaneously at the bottom and middle layers away from the weld zone. The top layer failed last in the base metal. The failure locations were consistent among different samples tested. Also, Charpy V-notch impact tests were conducted for weld metal, heat affected zone, and the base metal at each layer as a function of temperature. The weld microstructures were characterized using optical and electron microscopy and micro-hardness mapping.

Lim, Yong Chae↗
DOE OSTI2025

High-resolution tunnelling spectroscopy of fractional quantum Hall states

Strong interactions between electrons in two-dimensional systems in the presence of a high magnetic field give rise to fractional quantum Hall states that host quasiparticles with a fractional charge and fractional exchange statistics. Here, in this work, we demonstrate high-resolution scanning tunnelling microscopy and spectroscopy of fractional quantum Hall states in ultra-clean Bernal-stacked bilayer graphene devices. Spectroscopy measurements show sharp excitations that have been predicted to emerge when electrons fractionalize into bound states of quasiparticles. We found energy gaps for candidate non-abelian fractional states that are larger by a factor of five than those in other related systems, for example, semiconductor heterostructures, and this suggests that bilayer graphene is an ideal platform for manipulating these quasiparticles and for creating topological quantum bits. We also found previously unobserved fractional states in our very clean graphene samples.

quantum Hall↗
DOE OSTI2013

AN EXPONENTIAL DECLINE AT THE BRIGHT END OF THE z = 6 GALAXY LUMINOSITY FUNCTION

We present the results of a search for the most luminous star-forming galaxies at redshifts z Almost-Equal-To 6 based on Canada-France-Hawaii Telescope Legacy Survey data. We identify a sample of 40 Lyman break galaxies (LBGs) brighter than magnitude z' = 25.3 across an area of almost 4 deg{sup 2}. Sensitive spectroscopic observations of seven galaxies provide redshifts for four, of which only two have moderate to strong Ly{alpha} emission lines. All four have clear continuum breaks in their spectra. Approximately half of the LBGs are spatially resolved in 0.7 arcsec seeing images, indicating larger sizes than lower luminosity galaxies discovered with the Hubble Space Telescope, possibly due to ongoing mergers. The stacked optical and infrared photometry is consistent with a galaxy model with stellar mass {approx}10{sup 10} M{sub Sun }. There is strong evidence for substantial dust reddening with a best-fit A{sub V} = 0.75 and A{sub V} > 0.48 at 2{sigma} confidence, in contrast to the typical dust-free galaxies of lower luminosity at this epoch. The spatial extent and spectral energy distribution suggest that the most luminous z Almost-Equal-To 6 galaxies are undergoing merger-induced starbursts. The luminosity function of z = 5.9 star-forming galaxies is derived. This agrees well with previous work and shows strong evidence for an exponential decline at the bright end, indicating that the feedback processes that govern the shape of the bright end are occurring effectively at this epoch.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2012

Comparison of luminescence properties of bilayer and multilayer InAs/GaAs quantum dots

Highlights: Black-Right-Pointing-Pointer We seek to compare the optical behavior of coupled bilayer and multilayer QDs. Black-Right-Pointing-Pointer The coupled InAs/GaAs QD stacks are grown by Stranski-Krastanow growth technique. Black-Right-Pointing-Pointer We comment on roles of vertical strain and electronic coupling along the stacks. -- Abstract: Coupled InAs/GaAs quantum dots have generated an interest for their longer emission wavelength and narrower line-width. However, a consensus has not been reached on the parameters of growth required to achieve a desired effect from coupling due to contradictory reports of shorter emission wavelengths. In this paper, we seek to compare the luminescence properties of bilayer quantum dots (BQDs) with those of multilayer quantum dots (MQDs), grown at a very low deposition rate, keeping all parameters constant. The BQD and MQD samples were grown by solid source MBE at a slow growth rate of 0.03 ML/s. A blueshift in the PL spectra for 11 layer coupled InAs/GaAs MQD heterostructure is observed compared to the BQDs for temperatures less than 180 K. This undesired blueshift is attributed to strain in the structure which overshadowed the usual redshift in emission wavelength in such structures due to electronic coupling. The variation in PL line-width with temperature in the MQD structure is found to be much lower than in the BQD. However the PL intensity of the MQDs fall at a faster rate with temperature compared to the BQD sample, due to strain generated non-radiative centers in the islands which favors in thermalization of carriers.

36 MATERIALS SCIENCE↗
DOE OSTI2016

Static and dynamic properties of vortex pairs in asymmetric nanomagnets

Stacked spin-vortex pairs in magnetic multilayered nanopillars, with vertical separation between the vortices small compared to the vortex core size and pure magnetostatic coupling, exhibit spin dynamics absent in individual vortices. This dynamics is nonlinear and is due to the strong direct core-core coupling in the system, dominating energetically for small-signal excitation. We observe and explain the appearance of spin resonance modes, forbidden within linear dynamics, and discuss how they depend on the magnetic and morphological asymmetries in the samples.

77 NANOSCIENCE AND NANOTECHNOLOGY↗
DOE OSTI2015

Precipitation in pores: A geochemical frontier

This article's purpose is to review some of the recent research in which geochemists have examined precipitation of solid phases in porous media, particularly in pores a few nanometers in diameter (nanopores). While this is a “review,” it is actually more forward-looking in that the list of things about this phenomenon that we do not know or cannot control at this time is likely longer than what we do know and can control. For example, there are three directly contradictory theories on how to predict how precipitation proceeds in a medium of varying pore size, as will be discussed below. The confusion on this subject likely stems from the complexity of the phenomenon itself: One can easily clog a porous medium by inducing a rapid, homogeneous precipitation directly from solution, or have limited precipitation occur that does not affect permeability or even porosity substantially. It is more difficult to engineer mineral precipitation in order to obtain a specific outcome, such as filling all available pore space over a targeted area for the purposes of contaminant sequestration. However, breakthrough discoveries could occur in the next five to ten years that enhance our ability to predict robustly and finely control precipitation in porous media by understanding how porosity and permeability evolve in response to system perturbations. These discoveries will likely stem (at least in part) from advances in our ability to 1) perform and interpret X-ray/neutron scattering experiments that reveal the extent of precipitation and its locales within porous media (Anovitz and Cole 2015, this volume), and 2) utilize increasingly powerful simulations to test concepts and models about the evolution of porosity and permeability as precipitation occurs (Steefel et al. 2015, this volume). A further important technique to isolate specific phenomena and understand reactivity is also microfluidics cell experiments that allow specific control of flow paths and fluid velocities (Yoon et al. 2012). An improved ability to synthesize idealized porous media will allow for tailored control of pore distributions, mineralogy and will allow more reproducible results. This in turn may allow us to isolate specific processes without the competing and obfuscatory effects that hinder generalization of observations when working with solely natural samples. It is likely that no one single experiment, or simulation technique will provide the key discoveries: to make substantive progress will require a collaborative effort to understand the interplay between fluid transport and geochemistry. Finally, where rock fracturing and elevated pressures are of concern, an understanding and capability to model geomechanical properties are necessary (Scherer 1999).

58 GEOSCIENCES↗
DOE OSTI2011

Determination of Nickel Species in Stack Emissions from Eight Residual Oil-Fired Utility Steam-Generating Units

XAFS spectroscopy has been used to determine the Ni species in particulate matter collected on quartz thimble filters in the stacks of eight residual (No. 6 fuel) oil-burning electric utility steam-generating units. Proper speciation of nickel in emitted particulate matter is necessary to correctly anticipate potential health risks. Analysis of the spectroscopic data using least-squares linear combination methods and a newly developed method specific for small quantities of Ni sulfide compounds in such emissions show that potentially carcinogenic Ni sulfide compounds are absent within the detection limits of the method ({le}3% of the total Ni) in the particulate matter samples investigated. In addition to the major nickel sulfate phase (NiSO{sub 4} {center_dot} 6H{sub 2}O), lesser amounts of (Ni,Mg)O and/or NiFe{sub 2}O{sub 4} were also identified in most emission samples. On the basis of the results from these emission characterization studies, the appropriateness of the U.S. Environmental Protection Agency's assumption that the Ni compound mixture emitted from residual oil-fired power plants is 50% as carcinogenic as nickel subsulfide (Ni{sub 3}S{sub 2}) should be re-evaluated.

54 ENVIRONMENTAL SCIENCES↗
DOE OSTI2016

The evolution of the galaxy stellar mass function at z = 4-8: a steepening low-mass-end slope with increasing redshift

We present galaxy stellar mass functions (GSMFs) at z = 4–8 from a rest-frame ultraviolet (UV) selected sample of ∼4500 galaxies, found via photometric redshifts over an area of ∼280 arcmin{sup 2} in the Cosmic Assembly Near-infrared Deep Extragalactic Legacy Survey (CANDELS)/Great Observatories Origins Deep Survey (GOODS) fields and the Hubble Ultra Deep Field. The deepest Spitzer/IRAC data to date and the relatively large volume allow us to place a better constraint at both the low- and high-mass ends of the GSMFs compared to previous space-based studies from pre-CANDELS observations. Supplemented by a stacking analysis, we find a linear correlation between the rest-frame UV absolute magnitude at 1500 Å (M{sub UV}) and logarithmic stellar mass (logM{sub ∗}) that holds for galaxies with log(M{sub ∗}/M{sub ⊙})≲10. We use simulations to validate our method of measuring the slope of the logM{sub ∗}–M {sub UV} relation, finding that the bias is minimized with a hybrid technique combining photometry of individual bright galaxies with stacked photometry for faint galaxies. The resultant measured slopes do not significantly evolve over z = 4–8, while the normalization of the trend exhibits a weak evolution toward lower masses at higher redshift. We combine the logM{sub ∗}–M {sub UV} distribution with observed rest-frame UV luminosity functions at each redshift to derive the GSMFs, finding that the low-mass-end slope becomes steeper with increasing redshift from α=−1.55{sub −0.07}{sup +0.08} at z = 4 to α=−2.25{sub −0.35}{sup +0.72} at z = 8. The inferred stellar mass density, when integrated over M{sub ∗}=10{sup 8}–10{sup 13} M {sub ⊙}, increases by a factor of 10{sub −2}{sup +30} between z = 7 and z = 4 and is in good agreement with the time integral of the cosmic star formation rate density.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2019

The Relation between Galaxy ISM and Circumgalactic O vi Gas Kinematics Derived from Observations and ΛCDM Simulations

We introduce the first galaxy–O vi absorption kinematic study for 20 absorption systems (EW > 0.1 Å) associated with isolated galaxies (0.15 ≤ z ≤ 0.55) that have accurate redshifts and rotation curves obtained using Keck/ESI. Our sample is split into two azimuthal angle bins: major axis (Φ < 25°) and minor axis (Φ > 33°). O vi absorption along the galaxy major axis is not correlated with galaxy rotation kinematics, with only 1/10 of systems that could be explained with rotation/accretion models. This is in contrast to corotation commonly observed for Mg ii absorption. O vi along the minor axis could be modeled by accelerating outflows, but only for small opening angles, while the majority of the O vi is decelerating. Along both axes, stacked O vi profiles reside at the galaxy systemic velocity with the absorption kinematics spanning the entire dynamical range of their galaxies. The O vi found in AMR cosmological simulations exists within filaments and in halos of ~50 kpc surrounding galaxies. Simulations show that major-axis O vi gas inflows along filaments and decelerates as it approaches the galaxy, while increasing in its level of corotation. Minor-axis outflows in the simulations are effective within 50–75 kpc; beyond that they decelerate and fall back onto the galaxy. While the simulations show clear O vi kinematic signatures, they are not directly comparable to observations. When we compare kinematic signatures integrated through the entire simulated galaxy halo, we find that these signatures are washed out owing to full velocity distribution of O vi throughout the halo. We illustrate that O vi alone does not serve as a useful kinematic indicator of gas accretion, outflows, or star formation and likely best probes the halo virial temperature.

79 ASTRONOMY AND ASTROPHYSICS↗
NASA NTRS1993

Red edge spectral measurements from sugar maple leaves

Many sugar maple stands in the northeastern United States experienced extensive insect damage during the 1988 growing season. Chlorophyll data and high spectral resolution spectrometer laboratory reflectance data were acquired for multiple collections of single detached sugar maple leaves variously affected by the insect over the 1988 growing season. Reflectance data indicated consistent and diagnostic differences in the red edge portion (680-750 nm) of the spectrum among the various samples and populations of leaves. These included differences in the red edge inflection point (REIP), a ratio of reflectance at 740-720 nm (RE3/RE2), and a ratio of first derivative values at 715-705 nm (D715/D705). All three red edge parameters were highly correlated with variation in total chlorophyll content. Other spectral measures, including the Normalized Difference Vegetation Index (NDVI) and the Simple Vegetation Index Ratio (VI), also varied among populations and over the growing season, but did not correlate well with total chlorophyll content. Leaf stacking studies on light and dark backgrounds indicated REIP, RE3/RE2 and D715/D705 to be much less influenced by differences in green leaf biomass and background condition than either NDVI or VI.

Vogelmann, J. E.↗
NASA NTRS2004

Epoxy Adhesives for Stator Magnet Assembly in Stirling Radioisotope Generators (SRG)

As NASA seeks to fulfill its goals of exploration and understanding through missions planned to visit the moons of Saturn and beyond, a number of challenges arise from the idea of deep space flight. One of the first problems associated with deep space travel is electrical power production for systems on the spacecraft. Conventional methods such as solar power are not practical because efficiency decreases substantially as the craft moves away from the Sun. The criterion for power generation during deep space missions are very specific, the main points requiring high reliability, low mass, minimal vibration and a long lifespan. A Stirling generator, although fairly old in concept, is considered to be a potential solution for electrical power generation for deep space flight. A Stirling generator works on the same electromagnetic principles of a standard generator, using the linear motion of the alternator through the stationary stator which produces electric induction. The motion of the alternator, however, is produced by the heating and cooling dynamics of pressurized gases. Essentially heating one end and cooling another of a contained gas will cause a periodic expansion and compression of the gas from one side to the other, which a displacer translates into linear mechanical motion. NASA needs to confirm that the materials used in the generator will be able to withstand the rigors of space and the life expectancy of the mission. I am working on the verification of the epoxy adhesives used to bond magnets to the steel lamination stack to complete the stator; in terms of in-service performance and durability under various space environments. Understanding the proper curing conditions, high temperature properties, and degassing problems as well as production difficulties are crucial to the long term success of the generator. system and steel substrate used in the stator. To optimize the curing conditions of the epoxies, modulated differential scanning calorimetry analysis was done as a function of cure time and temperatures. Adhesion bond strength was tested at various temperatures with lap shear samples using Hiperco 50 substrate to ensure that the proper adhesive is being used. To try and solve the problem of bondline thickness, micro glass beads of 0.0017" in diameter were investigated to see if any other physical properties of the epoxy were affected. Efforts will be made to develop a standard, optimized, fabrication process/procedure of sub-scale magnet-stator assemblies for various adhesive performance evaluation studies under simulated generator conditions. Also, accelerated aging testing will be done in a pressurized canister with stator assembly samples for three years to verify if any degassing or thermal degradation of the epoxy occurs. The necessity of verifying the correct epoxy adhesive system for the stator magnet in the SRG is crucial because failure of the stator assembly would jeopardize the electrical system, and thereby the entire mission itself. My work involves specimen fabrications, testing, and data analyses of the epoxy adhesive system for the stator magnet in the SRG is crucial because failure of the stator assembly would jeopardize the electrical system, and thereby the entire mission itself.

Cater, George M.↗
DOE OSTI2010

Ion Mobility Spectrometry (IMS) and Mass Spectrometry

In a media of finite viscosity, the Coulomb force of external electric field moves ions with some terminal speed. This dynamics is controlled by “mobility” - a property of the interaction potential between ions and media molecules. This fact has been used to separate and characterize gas-phase ions in various modes of ion mobility spectrometry (IMS) developed since 1970. Commercial IMS devices were introduced in 1980-s for field detection of volatile traces such as explosives and chemical warfare agents. Coupling to soft-ionization sources, mass spectrometry (MS), and chromatographic methods in 1990-s had allowed IMS to handle complex samples, enabling new applications in biological and environmental analyses, nanoscience, and other areas. Since 2003, the introduction of commercial systems by major instrument vendors started bringing the IMS/MS capability to broad user community. The other major development of last decade has been the differential IMS or “field asymmetric waveform IMS” (FAIMS) that employs asymmetric time-dependent electric field to sort ions not by mobility itself, but by the difference between its values in strong and weak electric fields. Coupling of FAIMS to conventional IMS and stacking of conventional IMS stages have enabled two-dimensional separations that dramatically expand the power of ion mobility methods.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2018

Image registration of low signal-to-noise cryo-STEM data

Combining multiple fast image acquisitions to mitigate scan noise and drift artifacts has proven essential for picometer precision, quantitative analysis of atomic resolution scanning transmission electron microscopy (STEM) data. For very low signal-to-noise ratio (SNR) image stacks – frequently required for undistorted imaging at liq- uid nitrogen temperatures – image registration is particularly delicate, and standard approaches may either fail, or produce subtly specious reconstructed lattice images. We present an approach which effectively registers and averages image stacks which are challenging due to their low-SNR and propensity for unit cell misalignments. Registering all possible image pairs in a multi-image stack leads to significant information surplus. In combination with a simple physical picture of stage drift, this enables identi cation of incorrect image registrations, and determination of the optimal image shifts from the complete set of relative shifts. Here, we demonstrate the effectiveness of our approach on experimental, cryogenic STEM datasets, highlighting subtle artifacts endemic to low-SNR lattice images and how they can be avoided. High-SNR average images with information transfer out to 0.72 Å are achieved at 300 kV and with the sample cooled to near liquid nitrogen temperature.

47 OTHER INSTRUMENTATION↗
DOE OSTI2014

Constraining the low-mass Slope of the star formation sequence at 0.5 < z < 2.5

We constrain the slope of the star formation rate (SFR; log Ψ) to stellar mass (log M {sub *}) relation down to log (M {sub *}/M {sub ☉}) = 8.4 (log (M {sub *}/M {sub ☉}) = 9.2) at z = 0.5 (z = 2.5) with a mass-complete sample of 39,106 star-forming galaxies selected from the 3D-HST photometric catalogs, using deep photometry in the CANDELS fields. For the first time, we find that the slope is dependent on stellar mass, such that it is steeper at low masses (log Ψ∝log M {sub *}) than at high masses (log Ψ∝(0.3-0.6)log M {sub *}). These steeper low-mass slopes are found for three different star formation indicators: the combination of the ultraviolet (UV) and infrared (IR), calibrated from a stacking analysis of Spitzer/MIPS 24 μm imaging; β-corrected UV SFRs; and Hα SFRs. The normalization of the sequence evolves differently in distinct mass regimes as well: for galaxies less massive than log (M {sub *}/M {sub ☉}) < 10 the specific SFR (Ψ/M {sub *}) is observed to be roughly self-similar with Ψ/M {sub *}∝(1 + z){sup 1.9}, whereas more massive galaxies show a stronger evolution with Ψ/M {sub *}∝(1 + z){sup 2.2-3.5} for log (M {sub *}/M {sub ☉}) = 10.2-11.2. The fact that we find a steep slope of the star formation sequence for the lower mass galaxies will help reconcile theoretical galaxy formation models with the observations.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2017

Bayesian seismic inversion based on rock-physics prior modeling for the joint estimation of acoustic impedance, porosity and lithofacies

We propose a Bayesian approach for seismic inversion to estimate acoustic impedance, porosity and lithofacies within the reservoir conditioned to post-stack seismic and well data. The link between elastic and petrophysical properties is given by a joint prior distribution for the logarithm of impedance and porosity, based on a rock-physics model. The well conditioning is performed through a background model obtained by well log interpolation. Two different approaches are presented: in the first approach, the prior is defined by a single Gaussian distribution, whereas in the second approach it is defined by a Gaussian mixture to represent the well data multimodal distribution and link the Gaussian components to different geological lithofacies. The forward model is based on a linearized convolutional model. For the single Gaussian case, we obtain an analytical expression for the posterior distribution, resulting in a fast algorithm to compute the solution of the inverse problem, i.e. the posterior distribution of acoustic impedance and porosity as well as the facies probability given the observed data. For the Gaussian mixture prior, it is not possible to obtain the distributions analytically, hence we propose a Gibbs algorithm to perform the posterior sampling and obtain several reservoir model realizations, allowing an uncertainty analysis of the estimated properties and lithofacies. Both methodologies are applied to a real seismic dataset with three wells to obtain 3D models of acoustic impedance, porosity and lithofacies. The methodologies are validated through a blind well test and compared to a standard Bayesian inversion approach. Using the probability of the reservoir lithofacies, we also compute a 3D isosurface probability model of the main oil reservoir in the studied field.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2011

Effects of barrier composition and electroplating chemistry on adhesion and voiding in copper/dielectric diffusion barrier films

The effects of electroplating chemistry and dielectric diffusion barrier composition on copper voiding and barrier adhesion are reported. Adhesion was quantified using the four-point bend thin film adhesion technique, and voiding in the Cu films was quantified using scanning electron microscopy. A total of 12 different film stacks were investigated, including three different Cu electroplating chemistries and four different barrier materials (SiN, N-doped SiC, O-doped SiC, and dual-layer SiC). Both plating chemistry and barrier composition have a large effect on interface adhesion and voiding in the Cu film. X-ray photoelectron spectroscopy was used to investigate the segregation of Cu electroplating impurities, such as S and Cl, to the Cu/barrier interface. Secondary ion mass spectrometry was used to quantify oxygen content at the Cu/barrier interface in a subset of samples. This interface oxygen content is correlated with measured adhesion values.

36 MATERIALS SCIENCE↗