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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 955 records · Page 53
All sourcesNASA NTRSDOE OSTI
DOE OSTI2014

Active multispectral imaging system for photodiagnosis and personalized phototherapies

The proposed system has been designed to identify dermatopathologies or to apply personalized phototherapy treatments. The system emits electromagnetic waves in different spectral bands in the range of visible and near infrared to irradiate the target (skin or any other object) to be spectrally characterized. Then, an imaging sensor measures the target response to the stimulus at each spectral band and, after processing, the system displays in real time two images. In one of them the value of each pixel corresponds to the more reflected wavenumber whereas in the other image the pixel value represents the energy absorbed at each band. The diagnosis capability of this system lies in its multispectral design, and the phototherapy treatments are adapted to the patient and his lesion by measuring his absorption capability. This “in situ” absorption measurement allows us to determine the more appropriate duration of the treatment according to the wavelength and recommended dose. The main advantages of this system are its low cost, it does not have moving parts or complex mechanisms, it works in real time, and it is easy to handle. For these reasons its widespread use in dermatologist consultation would facilitate the work of the dermatologist and would improve the efficiency of diagnosis and treatment. In fact the prototype has already been successfully applied to pathologies such as carcinomas, melanomas, keratosis, and nevi.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2015

A new surrogate modeling technique combining Kriging and polynomial chaos expansions – Application to uncertainty analysis in computational dosimetry

In numerical dosimetry, the recent advances in high performance computing led to a strong reduction of the required computational time to assess the specific absorption rate (SAR) characterizing the human exposure to electromagnetic waves. However, this procedure remains time-consuming and a single simulation can request several hours. As a consequence, the influence of uncertain input parameters on the SAR cannot be analyzed using crude Monte Carlo simulation. The solution presented here to perform such an analysis is surrogate modeling. This paper proposes a novel approach to build such a surrogate model from a design of experiments. Considering a sparse representation of the polynomial chaos expansions using least-angle regression as a selection algorithm to retain the most influential polynomials, this paper proposes to use the selected polynomials as regression functions for the universal Kriging model. The leave-one-out cross validation is used to select the optimal number of polynomials in the deterministic part of the Kriging model. The proposed approach, called LARS-Kriging-PC modeling, is applied to three benchmark examples and then to a full-scale metamodeling problem involving the exposure of a numerical fetus model to a femtocell device. The performances of the LARS-Kriging-PC are compared to an ordinary Kriging model and to a classical sparse polynomial chaos expansion. The LARS-Kriging-PC appears to have better performances than the two other approaches. A significant accuracy improvement is observed compared to the ordinary Kriging or to the sparse polynomial chaos depending on the studied case. This approach seems to be an optimal solution between the two other classical approaches. A global sensitivity analysis is finally performed on the LARS-Kriging-PC model of the fetus exposure problem.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2016

Effects of catalyst support and chemical vapor deposition condition on synthesis of multi-walled carbon nanocoils

Multi-walled carbon nanocoil (MWCNC) is a carbon nanotube (CNT) with helical shape. We have synthesized MWCNCs and MWCNTs hybrid by chemical vapor deposition (CVD). MWCNCs are considered to be a potential material in nanodevices, such as electromagnetic wave absorbers and field emitters. It is very important to take into account the purity of MWCNCs. In this study, we aimed to improve the composition ratio of MWCNCs to MWCNTs by changing catalyst preparation and CVD conditions. As a catalyst, Fe{sub 2}O{sub 3}/zeolite was prepared by dissolving Fe{sub 2}O{sub 3} fine powder and Y-type zeolite (catalyst support material) in ethanol with an Fe density of 0.5wt.% and with a zeolite density of 3.5wt.%. The catalyst-coated Si substrate was transferred immediately onto a hotplate and was heated at 80°C for 5 min. Similarly, Fe{sub 2}O{sub 3}/Al{sub 2}O{sub 3}, Co/zeolite/Al{sub 2}O{sub 3}, Co/zeolite, and Co/Al{sub 2}O{sub 3} were prepared. The effect of the difference of the composite catalysts on synthesis of MWCNCs was considered. The CVD reactor was heated in a tubular furnace to 660-790°C in a nitrogen atmosphere at a flow rate of 1000 ml/min. Subsequently, acetylene was mixed with nitrogen at a flow rate ratio of C{sub 2}H{sub 2}/N{sub 2} = 0.02-0.1. The reaction was kept under these conditions for 10 min. MWCNTs and MWCNCs were well grown by the catalysts of Co/zeolite and Co/Al{sub 2}O{sub 3}. The composition ratio of MWCNCs to MWCNTs was increased by using a combination of zeolite and Al{sub 2}O{sub 3}. The highest composition ratio of MWCNCs to MWCNTs was 12%.

36 MATERIALS SCIENCE↗
DOE OSTI2019

Electron inertial effects on linearly polarized electromagnetic ion cyclotron waves at Earth's magnetosphere

We discuss a role of the electron inertial effect on linearly polarized electromagnetic ioncyclotron (EMIC) waves at Earth. The linearly polarized EMIC waves have been previouslysuggested to be generated via mode conversion from the fast compressional wave at the ion-ionhybrid (IIH) resonance. When the electron inertial effects are neglected, the wave normal angleof the mode-converted IIH waves is 90 degrees because the wavevector perpendicular to themagnetic field becomes infinite at the IIH resonance. When the electron inertial effect isconsidered, the mode-converted IIH waves can propagate across the magnetic field lines and thewavelength perpendicular to the magnetic field approaches the electron inertial length scale nearthe Buchsbaum resonance. These waves are referred to as electron inertial waves. Due to theelectron inertial effect, the perpendicular wavenumber to the ambient magnetic field near theIIH resonance remains finite and the wave normal angle is less than 90 degrees. The wave normalangle where the maximum absorption occurs in a dipole magnetic field is 30-80 degrees, whichis consistent with the observed values near the magnetic equator. Therefore, the numericalresults suggest that the linearly polarized EMIC wave generated via mode conversion near theIIH resonance can be detected in between the Buchsbaum and the IIH resonance frequencies,and these waves can have normal angle less than 90 degrees.

Kim, Eun-Hwa↗
DOE OSTI2017

Radial transport of radiation belt electrons in kinetic field-line resonances

A representative case study from the Van Allen Probes during a geomagnetic storm recovery phase reveals enhanced electron fluxes at intermediate pitch angles over energies from ~100 keV to 5 MeV coincident with broadband low-frequency electromagnetic waves. The statistical properties of these waves are used to build a model for radial diffusion via drift-bounce resonances in kinetic Alfvén eigenmodes/kinetic field-line resonances. Estimated diffusion coefficients indicate timescales for radial transport on the order of hours in storm time events at energies from <100 keV to MeVs over equatorial pitch angles from the edge of the loss cone to nearly perpendicular to the geomagnetic field. In conclusion, the correlation of kinetic resonances with electron depletions and enhancements during storm main phase and recovery, and the rapid diffusion these waves drive, suggests that they may modulate the outer radiation belt.

58 GEOSCIENCES↗
DOE OSTI2021

Orbital Angular Momentum from Self‐Assembled Concentric Nanoparticle Rings

Abstract Ring‐shaped nanostructures can focus, filter, and manipulate electromagnetic waves, but are challenging to incorporate into devices using standard nanofabrication techniques. Directed self‐assembly (DSA) of block copolymers (BCPs) on lithographically patterned templates has successfully been used to fabricate concentric rings and spirals as etching masks. However, this method is limited by BCP phase behavior and material selection. Here, a straightforward approach to generate ring‐shaped nanoparticle assemblies in thin films of supramolecular nanocomposites is demonstrated. DSA is used to guide the formation of concentric rings with radii spanning 150–1150 nm and ring widths spanning 30–60 nm. When plasmonic nanoparticles are used, ring nanodevice arrays can be fabricated in one step, and the completed devices produce high‐quality orbital angular momentum (OAM). Nanocomposite DSA simplifies and streamlines nanofabrication by producing metal structures without etching or deposition steps; it also introduces interparticle coupling as a new design axis. Detailed analysis of the nanoparticle ring assemblies confirms that the supramolecular system self‐regulates the spatial distribution of its components, and thus exhibits a degree of flexibility absent in DSA of BCPs alone, where structures are determined by polymer‐pattern incommensurability. The present studies also provide guidelines for developing self‐regulating DSA as an alternative to incommensurability‐driven methods.

Vargo, Emma↗
DOE OSTI2015

A new perspective on plasmonics: Confinement and propagation length of surface plasmons for different materials and geometries [A new perspective on materials for plasmonics]

Surface-plasmon polaritons are electromagnetic waves propagating on the surface of a metal. Thanks to subwavelength confinement, they can concentrate optical energy on the micrometer or even nanometer scale, enabling new applications in bio-sensing, optical interconnects, and nonlinear optics, where small footprint and strong field concentration are essential. The major obstacle in developing plasmonic applications is dissipative loss, which limits the propagation length of surface plasmons and broadens the bandwidth of surface-plasmon resonances. Here, a new analysis of plasmonic materials and geometries is presented which fully considers the tradeoff between propagation length and degree of confinement. It is based on a two-dimensional analysis of two independent figures of merit and the analysis is applied to relevant plasmonic materials, e.g., noble metals, aluminum, silicon carbide, doped semiconductors, graphene, etc. Furthermore, the analysis provides guidance on how to improve the performance of any particular plasmonic application and substantially eases the selection of the plasmonic material.

36 MATERIALS SCIENCE↗
DOE OSTI2025

Orchestrating Spontaneous Emission With Metasurfaces: Recent Advances in Engineering Thermal, Luminescent, and Quantum Emissions

Metasurfaces have emerged as powerful tools for controlling spontaneous emission, offering unprecedented control over light-matter interactions at sub-wavelength scales. While metasurfaces are traditionally utilized for shaping coherent electromagnetic waves, they have recently extended their capabilities to control incoherent or spontaneous emission. This examines review how metasurfaces can enhance and precisely control properties of thermal, luminescent, and quantum emission. In thermal emission, metasurfaces enable control over spatial, temporal, and spin coherence, offering new possibilities for applications such as energy harvesting, radiative cooling and heat assisted ranging and detection. For luminescent emission, metasurfaces significantly improve emission rates, quantum efficiency, and directionality, driving innovations in lighting and display technologies. For controlling quantized spontaneous emission, metasurfaces are instrumental in enhancing single-photon sources and enabling novel functionalities in quantum states through photon-pair generation, which is vital for quantum communication, meteorology, and computing. Here, despite these advancements several challenges to increase the operational bandwidths, accelerate and develop simulation strategies, and fabrication complexities persist. Emerging trends are also discussed, such as dynamic metasurfaces and their integration with nanophotonic platforms, which could further expand the capabilities of light-emitting metasurfaces.

Luminescence↗
DOE OSTI2023

Physics‐Informed Machine Learning for Inverse Design of Optical Metamaterials

Optical metamaterials manipulate light through various confinement and scattering processes, offering unique advantages like high performance, small form factor and easy integration with semiconductor devices. However, designing metasurfaces with suitable optical responses for complex metamaterial systems remains challenging due to the exponentially growing computation cost and the ill‐posed nature of inverse problems. To expedite the computation for the inverse design of metasurfaces, a physics‐informed deep learning (DL) framework is used. A tandem DL architecture with physics‐based learning is used to select designs that are scientifically consistent, have low error in design prediction, and accurate reconstruction of optical responses. The authors focus on the inverse design of a representative plasmonic device and consider the prediction of design for the optical response of a single wavelength incident or a spectrum of wavelength in the visible light range. The physics‐based constraint is derived from solving the electromagnetic wave equations for a simplified homogenized model. The model converges with an accuracy up to 97% for inverse design prediction with the optical response for the visible light spectrum as input, and up to 96% for optical response of single wavelength of light as input, with optical response reconstruction accuracy of 99%.

Sarkar, Sulagna↗
DOE OSTI2022

Integrated Solar-Driven Device with a Front Surface Semitransparent Catalysts for Unassisted CO 2 Reduction

Monolithic integrated photovoltaic-driven electrochemical (PV-EC) artificial photosynthesis is reported for unassisted CO 2 reduction. The PV-EC structures employ triple junction photoelectrodes with a front mounted semitransparent catalyst layer as a photocathode. The catalyst layer is comprised of an array of microscale triangular metallic prisms that redirect incoming light toward open areas of the photoelectrode to reduce shadow losses. Full wave electromagnetic simulations of the prism array (PA) structure guide optimization of geometries and length scales. An integrated device is constructed with Ag catalyst prisms covering 35% of the surface area. The experimental device has close to 80% of the transmittance with a catalytic surface area equivalent 144% of the glass substrate area. Experimentally this photocathode demonstrates a direct solar-to-CO conversion efficiency of 5.9% with 50 h stability. Selective electrodeposition of Cu catalysts onto the surface of the Ag triangular prisms allows CO2 conversion to higher value products enabling demonstration of a solar-to-C 2+ product efficiency of 3.1%. This design featuring structures that have a semitransparent catalyst layer on a PV-EC cell is a general solution to light loss by shadowing for front surface mounted metal catalysts, and opens a route for the development of artificial photosynthesis based on this scalable design approach.

14 SOLAR ENERGY↗
DOE OSTI2024

Magnetic nanoparticle‐induced sorbent regeneration for direct air capture

Direct air capture (DAC) is a promising technology for decarbonization through the removal of CO 2 from the atmosphere. In many DAC processes, the regeneration energy used to restore the capture capacity of sorbents accounts for a significant fraction of the energy required by the whole process. Here we report an effective and scalable sorbent regeneration method for liquid DAC solvents based on magnetic nanoparticles (MNPs) heating with AC magnetic fields. MNPs can be directly heated to provide uniform and rapid volumetric heating, as we demonstrate by promoting the release of captured CO 2 from an aqueous solution of potassium sarcosinate. Our results showed that 90% of the solvent can be regenerated within 7.5 min of heating through proposed technique. The MNPs and solvent are found to be stable during the regeneration process and the MNPs showed long-term stability in the CO 2 -saturated solvent. Cyclic experiments showed that the nanoparticles can be reused for multiple cycles without performance deterioration. The process is operated in a noncontact mode through electromagnetic waves, making it an adoptable approach for existing carbon capture systems. The MNPs heating provides an effective regeneration strategy for liquid solvents used in carbon capture processes, in particular for DAC.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2020

Design of High Efficient Mid-Wavelength Infrared Polarizer on ORMOCHALC Polymer

While an organically modified chalcogenide (ORMOCHALC) can be used to fabricate a polymeric mid-wavelength infrared (MWIR) polarizer with competitive extinction ratio compared to the commercial wire-grid polarizers, which are composed of fragile inorganic materials, there is still a knowledge gap regarding the systematic design process to obtain high transmission efficiency and extinction ratio. As such, a computational parameter study for design optimization is conducted with the geometric parameters of the bilayer grating ORMOCHALC polarizer. The computational study shows that the Fabry–Pérot cavity is the primary mechanism that determines the transmission behaviors and the extinction ratio. A bilayer grating design, guided by the parameter study, is realized through the thermal nanoimprint and metal deposition processes. The extinction ratios measured with the Fourier-transform infrared are 245, 304, and 351 at the wavelength of 3, 4, and 5 μm, respectively. Compared to the state-of-the-art of the polymeric MWIR linear polarizers, the extinction ratio is improved by 1.4 times, and the transmission efficiency is increased by 2.5 times. Theoretical analysis with the multiple-layer model based on the transfer matrix method predicts a matched transmission behavior with the experiment and a full-wave electromagnetic simulation.

42 ENGINEERING↗
DOE OSTI2018

Design and characterization of an electromagnetic-resonant cavity microwave plasma reactor for atmospheric pressure carbon dioxide decomposition

Plasma processes are ideally suited for the conversion of renewable electricity into gas-phase reactivity, such as for the decomposition of carbon dioxide (CO 2 ). The design, development, and characterization of a microwave plasma reactor for atmospheric pressure undiluted carbon dioxide decomposition are presented. The reactor operates as an electromagnetic-resonant cavity in which the generated plasma forms a bulb attached to a converging-diverging nozzle and stabilized by streams of tangentially-injected processing gas. Electromagnetic wave confinement, residence time, and critical gas vorticity constitute fundamental reactor sizing and operation parameters. Experimental findings demonstrate that flow rate plays a dual role in plasma stabilization and process performance, whereas deposited power has a minor role in CO 2 decomposition.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2019

One-Dimensional Metallo-Superconductor Photonic Crystals as a Smart Window

A new structure to control the electromagnetic waves has been successfully designed for smart windows applications. The present photonic crystals (PCs) smart window is designed from a unit cell of two different materials such as A (metal) and B (superconductor) of thicknesses that repeated for N periods. The numerical results are investigated based on the characteristic matrix method. It was found that the angle of incidence has a significant effect on the transmission values. At 10{sup o} angle of incidence, we found more than 80% of the visible light and a near IR is transmitted whereas at 60{sup o} angle of incidence, the photonic band gap (PBG) begins to appear at wavelengths greater than 800 nm and the visible light transmittance remains more than 80%. Also, the dependence of the transmittance values on the periodicity and thickness of the proposed design was investigated. The proposed structure could be of potential use as a smart window in low-temperature applications and space industry.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2019

Synthesis and Characterization of Nanocrystalline Fe{sub (100−x)}Ni{sub (x)} Alloy Powders by Auto-combustion and Hydrogen Reduction

Nanocrystalline Fe{sub 90}Ni{sub 10,} Fe{sub 70}Ni{sub 30} andFe{sub 50}Ni{sub 50} alloy powders were successfully synthesized using a simple auto-combustion route followed by hydrogen reduction. The experimental work consisted of two steps, where the first step was auto-combustion and, the second step was reduction of the combusted powders. Citric acid was used as fuel during combustion, and citrate to nitrate ratio (C/N) was maintained at 0.3. NiFe{sub 2}O{sub 4} and Fe{sub 2}O{sub 3} phase formation occurred in obtained powders. Obtained powders were reduced in a hydrogen atmosphere at 700 °C/1 h for alloy formation. X-ray diffraction results revealed the presence of BCC α-(Fe,Ni) and FCC γ-(Fe,Ni) phases in reduced powders. Rietveld refinement technique was used to confirm α-(Fe,Ni) and γ-(Fe,Ni) phases with Im-3 m and Fm-3 m space groups, respectively. The Fe{sub 50}Ni{sub 50} powder has been found to have a single γ-(Fe,Ni) phase. Crystallite size of synthesized powders was calculated using the Scherrer equation and transmission electron microscopic analysis, which has been found < 50 nm. The nanocrystalline powders of all three compositions have shown soft magnetic nature with high saturation magnetization (Ms) and low coercivity (Hc). Effect of composition on the phase formation, microstructure and magnetic behavior was investigated. This rapid and simple process for attaining nanoparticles of Fe-Ni alloys with high Ms is expected to be useful in potent applications such as sensors, biomedical applications and electromagnetic wave absorbers.

36 MATERIALS SCIENCE↗
DOE OSTI2018

Casimir self-stress in a dielectric sphere

The dielectric sphere has been an important test case for understanding and calculating the vacuum force of a dielectric body onto itself. Here we develop a method for computing this force in homogeneous spheres of arbitrary dielectric properties embedded in arbitrary homogeneous backgrounds, assuming only that both materials are isotropic and dispersionless. Our results agree with known special cases; most notably we reproduce the prediction of Boyer and Schwinger et al. of a repulsive Casimir force of a perfectly reflecting shell. Our results disagree with the literature in the dilute limit. We argue that the Casimir self-stress cannot be regarded as due to pair-wise Casimir–Polder interactions, but rather due to reflections of virtual electromagnetic waves.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗