Engineering Papers⌕ Search

SEARCH · Engineering Papers

Results for “measured materials properties”

Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

Quote a phrase for an exact phrase match. Source license links do not imply unrestricted reuse.

At least 937 records · Page 52
All sourcesNASA NTRSDOE OSTI
NASA NTRS2004

Planetary Regolith Microstructure: An Unexpected Opposition Effect Result

The Opposition Effect (OE) is the non-linear increase in the intensity of light scattered from a surface as phase angle approaches 0 deg. It is seen in laboratory experiments and in remote sensing observations of planetary surfaces. Understanding the OE is a requirement to fitting photometric models which will produce meaningful results about regolith texture. Our previous laboratory studies are consistent with the hypothesis that the OE in particulate materials is due to two processes, Shadow Hiding (SHOE) and Coherent Backscattering (CBOE). SHOE arises because, as phase angle approaches zero, shadows cast by regolith grains on other grains become invisible to the observer. CBOE results from constructive interference between rays traveling the same path but in opposite directions. In this study we measured the angular scattering properties of 9 mixtures of Aluminum Oxide and Boron Carbide powders of the same particle diameter (25 microns). The reflectance of the materials ranged from 7% (pure B4C) to 91% (pure Al2O3). Along with the reflectance phase curve we measured the circular polarization ratio (CPR) - the ratio of the intensity of the light returned with the same helicity as the incident light to that with the opposite helicity. An increase in CPR with decreasing phase angle indicates increased multiple scattering and is consistent with CBOE (Hapke, 1993). Popular conceptions of CBOE (Belskaya et al, 2003) hold that materials of higher albedo would exhibit increased multiple scattering and that the contribution of CBOE to the OE would increase as albedo increases. Remarkably, we find the highest albedo samples did not have the strongest CBOE opposition peaks. Instead, the maximum CBOE contribution is observed in samples with reflectance between 15 and 40%.

Nelson, R. M.↗
DOE OSTI2025

A self-supervised robotic system for autonomous contact-based spatial mapping of semiconductor properties

Integrating robotically driven contact-based material characterization techniques into self-driving laboratories can enhance measurement quality, reliability, and throughput. While deep learning models support robust autonomy, current methods lack reliable pixel-precision positioning and require extensive labeled data. To overcome these challenges, we propose an approach for building self-supervised autonomy into contact-based robotic systems that teach the robot to follow domain expert measurement principles at high throughputs. We demonstrate the performance of this approach by autonomously driving a 4-DOF robotic probe for 24 hours to characterize semiconductor photoconductivity at 3025 uniquely predicted poses across a gradient of drop-casted perovskite film compositions, achieving throughputs of more than 125 measurements per hour. Spatially mapping photoconductivity onto each drop-casted film reveals compositional trends and regions of inhomogeneity, valuable for identifying manufacturing defects. With this self-supervised neural network–driven robotic system, we enable high-precision and reliable automation of contact-based characterization techniques at high throughputs, thereby allowing measurement of previously inaccessible yet important semiconductor properties for self-driving laboratories.

Science & Technology - Other Topics↗
DOE OSTI2024

Determination of electron-hole pair creation energy in Cd 0.9 Zn 0.1 Te 0.98 Se 0.02 quaternary semiconductor for room-temperature gamma-ray detection

We report the first-time measurement of the electron-hole pair (ehp) creation energy (W ehp ) in novel Cd 0.9 Zn 0.1 Te 0.98 Se 0.02 (CZTS) quaternary semiconductor. CZTS in single crystalline form is poised to be the future of large-volume room-temperature gamma-ray detectors due to its excellent compositional homogeneity with highly reduced defects, high-Z (atomic number) constituents, wide bandgap (1.6 eV), and superior charge transport properties. Despite a great deal of study of the material and device properties since its inception, the W ehp in CZTS has not been measured experimentally. Accurate determination of W ehp is essential for calibration of the spectrometer and other theoretical calculations. In this study we have used an absolute calibration approach, which is based on an iterative approach that yields the Wehp as the best-fit parameter. Using a 241 Am alpha emitting radioisotope and a planar CZTS detector, the Wehp in CZTS was calculated to be 4.47 eV. The obtained value has been validated by accurately predicting the peak energy for gamma rays emitted by a 137 Cs source and read by a CZTS detector with different dimensions. The dependences of the calculated W ehp value on the detector dimensions, type of interaction, and effect of charge trapping are also discussed.

42 ENGINEERING↗
NASA NTRS2000

Experimental and Numerical Characterization of a Cylindrical Blackbody Cavity

During hypersonic flight, high temperatures and high heat fluxes are generated on the surfaces of vehicles. The Flight Loads Laboratory (FLL) at Dryden Flight Research Center (DFRC) is equipped with a calibration furnace, capable of calibrating heat flux gages up to 1100kW per square meters, and temperature sensors up to 2600 C. One heating configuration of the calibration furnace is a cylindrical blackbody cavity. Throughout the blackbody there are temperature gradients due to various boundary conditions. These boundary conditions include resistance heating, radiant heat transfer, and conduction to water-cooled electrodes. Also, an inert gas is purged through the graphite blackbody to prevent it from oxidizing. Consequently, the various modes of heat transfer present during operation of the blackbody cavity must be well understood in order to produce accurate heat flux gage and temperature sensor calibrations for use in ground testing or flight testing of hypersonic vehicles. The first step towards understanding the heat transfer in the blackbody cavity was to perform experiments at 1100 C, with and without outer surface insulation, while taking detailed temperature measurements inside the blackbody cavity. Steady state thermal models of the blackbody cavity were then developed. These models included detailed thermal analysis using commercial thermal analysis software. Conduction, radiation, and convection were considered in the thermal models for two cases: one with the outside of the blackbody cavity insulated and the second without insulation. This paper describes the experimental and numerical efforts used to characterize the steady state operation of the blackbody cavity. It describes the analysis of the test measurements, the boundary conditions used in the numerical models, and how the models were calibrated to fit the experimental data. Effects of various uncertainties, such as material properties, and convection are discussed.Initial thermal models predicted temperatures in the deepest part of the blackbody cavity within 7 C of the measured value and produced trends comparable to the experimental data, throughout the models. Adjustment of the boundary conditions, which were included in the thermal models, produced good agreement with measured temperatures. Free and forced convection of the purge gas inside the blackbody was found to be insignificant.

Abdelmessih, Amanie N.↗
NASA NTRS1982

A method to determine the acoustical properties of locally and nonlocally reacting duct liners in grazing flow

The acoustical properties of locally and nonlocally reacting acoustical liners in grazing flow are described. The effect of mean flow and shear flow are considered as well as the application to rigid and limp bulk reacting materials. The axial wavenumber of the least attenuated mode in a flow duct is measured. The acoustical properties of duct liners is then deduced from the measured axial wavenumber and known flow profile and boundary conditions. This method is a natural extension of impedance-like measurements.

Succi, G.↗
DOE OSTI2024

Anomalous thermal effect in Zr Te 5 observed via photothermal measurements

In this study, we explore the magneto-thermoelectric power (MTP) of $ZrTe$ 5 , a canonical Dirac semimetal, through a novel photothermal technique. Unlike conventional thermoelectric studies that rely on on-chip heaters and are limited by fabrication processes, especially for stress-sensitive materials, our approach utilizes photothermal effects to induce temperature gradients. Our experiments, applying a magnetic field approximately parallel and transverse to the photocurrent detection direction, reveal that the photothermal method efficiently and reliably extracts both diagonal and off-diagonal components of the thermoelectric coefficient of $ZrTe$ 5 . Here, we observe that the longitudinal MTP reproduces features previously reported in thermal transport studies, while the photoinduced transverse MTP confirms the anomalous Nernst effect. This photothermal measurement technique opens new avenues for investigating transport properties in a wide range of quantum materials, both in 3D and 2D systems.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2020

Advanced Characterization Techniques for Overcoming Challenges of Perovskite Solar Cell Materials

Abstract In the last 10 years, organic–inorganic hybrid perovskite solar cells have achieved unprecedented advances, to the point where they now exhibit extremely high efficiency. However, long‐term stability and areal scalability limitations impede the commercial application of perovskite materials, and appropriate diagnosistic tools have become necessary to evaluate perovskite materials. Characterization of perovskite materials is regularly misinterpretated, due to unique intrinsic and extrinsic factors: degradation from the measurement source, ion migration, phase transition, and separation. Herein, studies on perovskites are reviewed that have used advanced characterization tools to overcome characterization challenges. Cryogenic temperature assisted measurements mitigate degradation or phase transitions induced by the measurement source. In situ measurements can track the variation of perovskite materials depending on external stimuli. Spatial material properties are able to be evaluated by the use of multidimensional mapping techniques. An overview of these advanced characterization tools that can overcome the challenges associated with established tools provides the opportunity for further understanding perovskite materials and solving the remaining challenges on the road to commercialization.

Kim, Min‐cheol↗
DOE OSTI2020

Experimental study of different silicon sensor options for the upgrade of the CMS Outer Tracker

During the high-luminosity phase of the LHC (HL-LHC), planned to start in 2027, the accelerator is expected to deliver an instantaneous peak luminosity of up to 7.5×10 34 cm –2 s –1 . A total integrated luminosity of 3000 or even 4000 fb –1 is foreseen to be delivered to the general purpose detectors ATLAS and CMS over a decade, thereby increasing the discovery potential of the LHC experiments significantly. The CMS detector will undergo a major upgrade for the HL-LHC,with entirely new tracking detectors consisting of an Outer Tracker and Inner Tracker. However, the new tracking system will be exposed to a significantly higher radiation than the current tracker, requiring new radiation-hard sensors. CMS initiated an extensive irradiation and measurement campaign starting in 2009 to systematically compare the properties of different silicon materials and design choices for the Outer Tracker sensors. Several test structures and sensors were designed and implemented on 18 different combinations of wafer materials, thicknesses, and production technologies. The devices were electrically characterized before and after irradiation with neutrons,and with protons of different energies, with fluences corresponding to those expected at different radii of the CMS Outer Tracker after 3000 fb –1 . The tests performed include studies with β sources, lasers, and beam scans. This paper compares the performance of different options for the HL-LHC silicon sensors with a focus on silicon bulk material and thickness.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2022

Temperature-driven changes in the Fermi surface of graphite

Here we report on temperature-dependent size and anisotropy of the Fermi pockets in graphite revealed by magnetotransport measurements. The magnetoresistances (MRs) obtained in fields along the c axis obey an extended Kohler's rule, with the carrier density following the prediction of a temperature-dependent Fermi energy, indicating a change in the Fermi pocket size with temperature. The angle-dependent magnetoresistivities at a given temperature exhibit a scaling behavior. The scaling factor that reflects the anisotropy of the Fermi surface is also found to vary with temperature. Our results demonstrate that temperature-driven changes in Fermi surface can be ubiquitous and need to be considered in understanding the temperature-dependent carrier density and MR anisotropy in semimetals.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2022

RUScal : Software for the analysis of resonant ultrasound spectroscopy measurements

Resonant ultrasound spectroscopy is used to nondestructively measure the elastic resonances of small solids to elucidate the material's elastic properties or other qualities like size, shape, or composition. In this work, we introduce the software RUScal for the purpose of determining elastic properties by analyzing the eigenfrequencies of solid specimens with common shapes, such as rectangular parallelepipeds, cylinders (solid and hollow tube), ellipsoids, and octahedrons, as well as irregularly shaped ellipsoids that can be described analytically. All symmetry classes are supported, from isotropic to triclinic, along with the option to add or remove up to three orthogonal mirror planes as well as the ability to reorient the crystal axes with respect the sample edges via Euler angles. Additional features include tools to help find initial sets of elastic constants, including grid exploration and Monte Carlo methods, a tool to analyze frequencies as a function of sample length or crystal orientation, an error analysis tool to assess fit quality, and formatting of the input and output files for batch fitting, e.g., as a function of temperature. This software was validated with published resonant ultrasound spectroscopy data for various materials, shapes, and symmetries with noted improvements in calculation time compared to finite element methods.

47 OTHER INSTRUMENTATION↗
DOE OSTI2023

The influence of secondary electron yield uncertainty on the single-sided multipacting in dielectrics

Multipacting is an electrical discharge caused by the emission of secondary electrons which can occur in vacuum radio frequency systems. Generally multipacting is highly undesirable obstacle, which increases the noise level as well as the return loss of radio frequency systems. Therefore, a prediction of multipacting is necessary to avoid it during radio frequency system design. In this regard, the accurate evaluation of the factors that affect multipacting is required. One of the critical factors determining the multipacting development is the secondary electron yield of the material. In practice the emission properties of materials are not known very accurately. There are uncertainties in the measured values of this yield. In this paper, the generalized Polynomial Chaos (gPC) method is used to quantify uncertainty of the secondary electron yield. This method is verified by Monte Carlo simulation. The effect of uncertainty for two secondary electron yield parameters is then investigated on the multipacting using gPC method.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2021

Bridging microscale to macroscale mechanical property measurements and predication of performance limitation for FeCrAl alloys under extreme reactor applications

Microscale mechanical testing has greatly benefited nuclear materials studies in at least two aspects: one is its feasibility to integrate with SEM and TEM microscopes for in situ atomic scale or microscale structural characterization to reveal fundamental details, and the other is its significance in development of accelerator-based ion irradiation technique as a surrogate method to simulate neutron damage. Ion irradiation is able to reach damage creation at a level at least three orders of magnitudes higher than test reactors. However, limited ion penetration depths, which are about a few microns for MeVs heavy ions and 10s microns for MeV light ions, make microscale mechanical tests a necessity. But, there is a great challenge to bridge microscale tests to macroscale tests because a bulk specimen of irradiated nuclear materials for high dose applications cannot be obtained in laboratory.

36 MATERIALS SCIENCE↗
DOE OSTI2021

Bridging microscale to macroscale mechanical property measurements and predication of performance limitation for FeCrAl alloys under extreme reactor applications

Microscale mechanical testing has greatly benefited nuclear materials studies in at least two aspects: one is its feasibility to integrate with SEM and TEM microscopes for in situ atomic scale or microscale structural characterization to reveal fundamental details, and the other is its significance in development of accelerator-based ion irradiation technique as a surrogate method to simulate neutron damage. Ion irradiation is able to reach damage creation at a level at least three orders of magnitudes higher than test reactors. However, limited ion penetration depths, which are about a few microns for MeVs heavy ions and 10s microns for MeV light ions, make microscale mechanical tests a necessity. But, there is a great challenge to bridge microscale tests to macroscale tests because a bulk specimen of irradiated nuclear materials for high dose applications cannot be obtained in laboratory.

36 MATERIALS SCIENCE↗
DOE OSTI2026

Neutron Diffraction Residual Stress Characterization of Large-Scale Components by WA-DED

Two large scale 316L stainless steel cylindrical shells were fabricated by wire arc directed energy deposition (WA DED). Residual stresses were measured by neutron diffraction, and the microstructure and mechanical properties of the printed material were characterized. Longitudinal and transverse residual stresses were compressive at the inner diameter, near neutral at mid wall, and tensile at the outer diameter; radial (through thickness) residual stresses were relatively low in magnitude, and peak tensile residual stresses occurred at the outer diameter surface along the longitudinal direction. The printed 316L SS exhibited a heterogeneous microstructure with finely dispersed δ ferrite, and demonstrated high yield and tensile strengths with large elongation and ductile fracture at ambient temperature and at 250 °C. These results indicate that the outer diameter surface and near surface regions—where tensile residual stress is highest—are the most vulnerable to residual stress–sensitive failure modes, such as stress corrosion cracking and fatigue.

36 MATERIALS SCIENCE↗
NASA NTRS1968

Properties of optics at high temperature and their measurement, a study

Bibliography lists, the sources containing emissivity and absorptivity data on materials at extremely high temperatures. The experimental techniques, equipment and efforts of the experimenters to characterize the materials used and methods to evaluate the errors are given in the sources in this bibliography.

Gates, D. W.↗