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At least 937 records · Page 52

Downhole Elemental Analysis with LIBS

In this paper we discuss a novel instrument, currently under development at Honeybee Robotics with SBIR funding from NASA. The device is designed to characterize elemental composition as a function of depth in non-terrestrial geological formations. The instrument consists of a miniaturized laser-induced breakdown spectrometer (LIBS) analyzer integrated in a 2" diameter drill string. While the drill provides subsurface access, the LIBS analyzer provides information on the elemental composition of the borehole wall. This instrument has a variety of space applications ranging from exploration of the Moon for which it was originally designed, to Mars, as well as a variety of terrestrial applications. Subsurface analysis is usually performed by sample acquisition through a drill or excavator, followed by sample preparation and subsequent sample presentation to an instrument or suite of instruments. An alternative approach consisting in bringing a miniaturized version of the instrument to the sample has many advantages over the traditional methodology, as it allows faster response, reduced probability of cross-contamination and a simplification in the sampling mechanisms. LIBS functions by focusing a high energy laser on a material inducing a plasma consisting of a small fraction of the material under analysis. Optical emission from the plasma, analyzed by a spectrometer, can be used to determine elemental composition. A triangulation sensor located in the sensor head determines the distance of the sensor from the borehole wall. An actuator modifies the position of the sensor accordingly, in order to compensate for changes due to the profile of the borehole walls. This is necessary because LIBS measurements are negatively affected by changes in the relative position of the focus of the laser with respect to the position of the sample (commonly referred to as the "lens to sample distance"). Profiling the borehole is done by adjusting the position of the sensor with a vertical stage; a second actuator at the top of the downhole probe allows radial scanning of the borehole. Analysis of iron and titanium in lunar simulant with LIBS was performed in air using the method of standard addition. The results for lunar simulant NU-LHT-2M show a value for the concentration of iron ranging between 2.29% and 3.05% depending on the atomic line selected. The accepted value for the sample analyzed is 2.83%, showing the capability for the system in development to provide qualitative and semi-quantitative analysis in real-time.

Moreschini, Paolo↗

Eliminating Crystals in Non-Oxide Optical Fiber Preforms and Optical Fibers

Non ]oxide fiber optics such as heavy metal fluoride and chalcogenide glasses are extensively used in infrared transmitting applications such as communication systems, chemical sensors, and laser fiber guides for cutting, welding and medical surgery. The addition of rare earths such as erbium, enable these materials to be used as fiber laser and amplifiers. Some of these glasses however are very susceptible to crystallization. Even small crystals can lead to light scatter and a high attenuation coefficient, limiting their usefulness. Previously two research teams found that microgravity suppressed crystallization in heavy metal fluoride glasses. Looking for a less expensive method to suppress crystallization, ground based research was performed utilizing an axial magnetic field. The experiments revealed identical results to those obtained via microgravity processing. This research then led to a patented process for eliminating crystals in optical fiber preforms and the resulting optical fibers. In this paper, the microgravity results will be reviewed as well as patents and papers relating to the use of magnetic fields in various material and glass processing applications. Finally our patent to eliminate crystals in non ]oxide glasses utilizing a magnetic field will be detailed.

Tucker, Dennis S.↗

Design and Preliminary Testing of the International Docking Adapter's Peripheral Docking Target

The International Docking Adapter's Peripheral Docking Target (PDT) was designed to allow a docking spacecraft to judge its alignment relative to the docking system. The PDT was designed to be compatible with relative sensors using visible cameras, thermal imagers, or Light Detection and Ranging (LIDAR) technologies. The conceptual design team tested prototype designs and materials to determine the contrast requirements for the features. This paper will discuss the design of the PDT, the methodology and results of the tests, and the conclusions pertaining to PDT design that were drawn from testing.

Foster, Christopher W.↗

Effect of Additives: Gamma-Ray Sensors Based on Ionizing Organic Nanocomposites

We have developed ionizing organic-based composites which have demonstrated great promise for radiation sensing. Nickel oxide has been proven as an active material for detecting high energy radiation. The oxidation state of unusual oxides such as nickel oxide in nanocomposites of ionizing organics changes much faster than thin film or bulk, and hence increases the sensitivity for radiation sensing. The resistivity of the oxide composite increases following sequential irradiation processes because of the decrease in holes' concentration. In this paper, we will present the effect of additional oxidizing agent on the morphology, processing and sensing of gamma-rays by oxides - urea based nanocomposites. It was observed that addition of MnO2 decreases the sensitivity. However, it recovers to original properties after irradiation much faster than undoped composites.

Vishall Dayal↗

Micromechanical Broadband Infrared Sensors based on Piezoelectric Bending Resonators

There is a high demand for high-performance and low-cost uncooled infrared (IR) detectors. In order to meet this need we are investigating the use of MEMS piezoelectric resonator technology using aluminum nitride (AlN) thin films. Recent research has shown that piezoelectric resonators have the potential to be used as a core element for highly sensitive, low-noise, and low-power uncooled IR detectors. A novel design of an AlN IR sensor based on piezoelectric bending resonator is described and analyzed in this paper. The detector is constructed by using thermally mismatched materials which stress the resonator and shift the resonance frequency. The IR thermal input is sensed by monitoring the frequency shift induced by the in-plan thermal stress. These designs have the potential for very high sensitivity and are compatible with commercially viable CMOS fabrication technology.

Rais-Zadeh, Mina↗

Magnetoelastic sensor for characterizing properties of thin-film/coatings

An apparatus for determining elasticity characteristics of a thin-film layer. The apparatus comprises a sensor element having a base magnetostrictive element at least one surface of which is at least partially coated with the thin-film layer. The thin-film layer may be of a variety of materials (having a synthetic and/or bio-component) in a state or form capable of being deposited, manually or otherwise, on the base element surface, such as by way of eye-dropper, melting, dripping, brushing, sputtering, spraying, etching, evaporation, dip-coating, laminating, etc. Among suitable thin-film layers for the sensor element of the invention are fluent bio-substances, thin-film deposits used in manufacturing processes, polymeric coatings, paint, an adhesive, and so on. A receiver, preferably remotely located, is used to measure a plurality of values for magneto-elastic emission intensity of the sensor element in either characterization: (a) the measure of the plurality of values is used to identify a magneto-elastic resonant frequency value for the sensor element; and (b) the measure of the plurality of successive values is done at a preselected magneto-elastic frequency.

Bachas, Leonidas G.↗

Thermal Protection Materials and Systems at NASA Ames Research Center

Thermal Protection Systems (TPS) are critical for enabling NASA missions involving high-speed atmospheric flight where the entries usually include descending into the atmosphere followed by a trajectory that aims to burn off energy and result in a controlled landing. NASA Ames focuses on qualifying and certifying TPS for current missions, sustaining TPS for future missions, and developing new TPS for upcoming missions where a heritage solution is not viable. More recently there is also a focus on advancing and transferring technologies that can benefit both commercial and government space needs. Developing mature thermal protection systems is a lengthy process involving advanced tools, extensive research, and testing. Design and analysis tools are used to predict aerothermal environments, aid the design of test and flight hardware, and support the testing for the thermal/mechanical response of thermal protection systems. More recently, advances in computational methods help reduce the time and cost of technological advances, aid in optimized material architecture design, and improve material properties and performance. While high-enthalpy testing that simulates the conditions of space flight remains essential for the evaluation and development of TPS materials, computational tools are already showing promise in reducing the need for widespread testing and can help fast-track the design cycle. With the exploration of new destinations EDL instrumentation remains an important element of the heatshield and NASA Ames and partners have developed and delivered instrumentation flight hardware in support of recent Mars missions (MSL and M2020) as well as Artemis Orion. Sensors installed on the heatshield and backshell of spacecraft provide coveted information about the aerodynamic and aerothermal environment during entry. Over the years NASA Ames has brought several reusable and ablative TPS materials to a level of readiness to hand off to missions and the branch continues to serve as a TPS steward for the agency. This presentation will cover current developments in the above areas that have enabled recent missions, and look to future TPS needs for missions such as Ice Giants.

thermal protection materials↗

Thermographic Imaging of Defects in Anisotropic Composites

Composite materials are of increasing interest to the aerospace industry as a result of their weight versus performance characteristics. One of the disadvantages of composites is the high cost of fabrication and post inspection with conventional ultrasonic scanning systems. The high cost of inspection is driven by the need for scanning systems which can follow large curve surfaces. Additionally, either large water tanks or water squirters are required to couple the ultrasonics into the part. Thermographic techniques offer significant advantages over conventional ultrasonics by not requiring physical coupling between the part and sensor. The thermographic system can easily inspect large curved surface without requiring a surface following scanner. However, implementation of Thermal Nondestructive Evaluations (TNDE) for flaw detection in composite materials and structures requires determining its limit. Advanced algorithms have been developed to enable locating and sizing defects in carbon fiber reinforced plastic (CFRP). Thermal Tomography is a very promising method for visualizing the size and location of defects in materials such as CFRP. However, further investigations are required to determine its capabilities for inspection of thick composites. In present work we have studied influence of the anisotropy on the reconstructed image of a defect generated by an inversion technique. The composite material is considered as homogeneous with macro properties: thermal conductivity K, specific heat c, and density rho. The simulation process involves two sequential steps: solving the three dimensional transient heat diffusion equation for a sample with a defect, then estimating the defect location and size from the surface spatial and temporal thermal distributions (inverse problem), calculated from the simulations.

Plotnikov, Y. A.↗

Stress Tuning of Laser Crystals

The topic of stress tunable laser crystals is addressed in this study with the purpose of determining the piezo-optic coefficients of a new laser material. This data was collected using a quadruple pass birefringence technique because of its high degree of sensitivity relative to the other methods examined including fringe shift analysis using a Mach-Zender interferometer. A green He-Ne laser was passed through a light chopper and Glan-Thompson prism before entering a crystal of Erbium doped Yttrium Aluminum Garnet (Er:YAG) (used in order to validate the experimental technique). The Er:YAG crystal is mounted in a press mechanism and the laser is quadruple passed through test specimen before being returned through the prism and the orthogonally polarized portion of the beam measured with a optical sensor. At a later stage, the Er:YAG crystal was replaced with a new crystal in order to determine the piezo-optic coefficients of this uncharacterized material. The applied load was monitored with the use of a 50 lb. load cell placed in line with the press. Light transmission readings were taken using a lock-in amplifier while load cell measurements were taken with a voltmeter from a 5 volt, 0.5 amp power supply. Despite the fact that an effective crystal press damping system was developed, size limitations precluded the use of the complete system. For this reason, data points were taken only once per full turn so as to minimize the effect of non uniform load application on the collected data. Good correlation was found in the transmission data between the experimentally determined Er:YAG and the previously known peizo-optic constants of non-doped crystal with which it was compared. The variation which was found between the two could be accounted for by the aforementioned presence of Erbium in the experimental sample (for which exact empirical data was not known). The same test procedure was then carried out on a Yttrium Gallium Aluminum garnet (YGAG) for the purpose of establishing values of its unknown piezo-optic constant tensor using experimentally collected transmission data. Significant variation between the piezo-optic constants of YAG and YGAG crystals was found however, the excellent data correlation of separate experimental runs carried out on the YGAG sample demonstrates the validity of these results. The data collected during the stressing of the YGAG was of high quality, however the amount of data collected was somewhat limited by a fracture of YGAG specimen which undoubted altered the crystalline lattice structure and hence precluded any further testing.

Carty, Atherton A.↗

Acoustic emission used as weld quality monitor

Acoustic emission technique is described for use as quality control tool in nondestructive inspection of welds. Stress mounts around weld defect until it exceeds yield strength of material. Pressure wave relieving the stress is emitted and followed by oscillations caused by multiple reflections. Acoustic emissions are then detected by sensor similar to ultrasonic sensor.

Jolly, W. O.↗

Analysis and preliminary design of optical sensors for propulsion control

A fiber-optic sensor concept screening study was performed. Twenty sensor subsystems were identified and evaluated. Two concepts selected for further study were the Fabry-Perot fiber-optic temperature sensor and the pulse-width-modulated phosphorescent temperature sensor. Various designs suitable for a Fabry-Perot temperature sensor to be used as a remote fiber-optic transducer were investigated. As a result, a particular design was selected and constructed. Tests on this device show that spectral peaks are produced from visible white light, and the change in wavelength of the spectral peaks produced by a change in temperature is consistent with theory and is 36 nm/C for the first order peak. A literature search to determine a suitable phosphor for implementing the pulse-width-modulated fiber optic temperature sensor was conducted. This search indicated that such a device could be made to function for temperatures up to approximately 200 C. Materials like ZnCdS and ZnSe activated with copper will be particularly applicable to temperature sensing in the cryogenic to room temperature region. While this sensing concept is probably not applicable to jet engines, the simplicity and potential reliability make the concept highly desirable for other applications.

James, K. A.↗

Signature evaluation of natural targets using high spectral resolution techniques

The concept of 'spectral signature' identification has been applied to LANDSAT and other broad-band multi-spectral scanner data to classify various materials on the earth's surface. A large amount of the spectral information available is invisible, however, to the broad-band sensors. Although the natural targets of interest in remote sensing do not exhibit fine line features such as those associated with gaseous media, there is significant information to be extracted from smoothly varying spectral reflection functions of most natural targets. Subtle variations observed recently in the high resolution 'spectral signatures' of vegetation targets, in particular, promise to open new avenues of application using higher spectral and radiometric resolution techniques. This research was accomplished using a 500-band spectroradiometer system specially adapted to rapid airborne operations

Collins, W.↗

Air Force cryocooler development for spacecraft

An overview is given of Air Force sponsored cryocooler development for long duration spacecraft missions. Alternate approaches are being pursued to insure eventual success. The types of closed cycle cryocoolers that are now in advanced development include Vuilleumier, turbo-Brayton, and rotary-reciprocating refrigerators. Linear Stirling coolers with magnetic bearings have also been jointly sponsored by NASA and the Air Force. Technology is also being explored for future coolers using magnetic materials at low temperatures and for refrigerators with sorption compresssors. All of these cryocoolers are presently configured primarily for use with infrared sensor systems, but the designs could be adapted for use with cryogenic fluid storage systems or other applications.

Haskin, William L.↗

Optical signal processing of spatially distributed sensor data in smart structures

Smart structures which contain dense two- or three-dimensional arrays of attached or embedded sensor elements inherently require signal multiplexing and processing capabilities to permit good spatial data resolution as well as the adequately short calculation times demanded by real time active feedback actuator drive circuitry. This paper reports the implementation of an in-line optical signal processor and its application in a structural sensing system which incorporates multiple discrete optical fiber sensor elements. The signal processor consists of an array of optical fiber couplers having tailored s-parameters and arranged to allow gray code amplitude scaling of sensor inputs. The use of this signal processor in systems designed to indicate the location of distributed strain and damage in composite materials, as well as to quantitatively characterize that damage, is described. Extension of similar signal processing methods to more complicated smart materials and structures applications are discussed.

Bennett, K. D.↗

Intelligent processing of intermetallic composite consolidation

Intermetallic composites based upon titanium aluminide matrices and silicon carbide of aluminum oxide fibers are emerging candidates for future hypersonic vehicle airframes and engines. To tailor the properties of these 'engineered' materials for specific application, to increase process yield, and to reduce costs, 'intelligent processing of materials' (IPM) control strategies are being explored for their processing. Recent progress is evaluated in the development of predictive process models, advanced sensors and control methodologies (the components of the IPM approach) for the critical near net-shape consolidation process step of continuous fiber reinforced intermetallic composite manufacture.

Wadley, H. N. G.↗

Fiber optic smart structures and skins V; Proceedings of the Meeting, Boston, MA, Sept. 8, 9, 1992

The present conference discusses the materials used in applications of fiber-optics (F-O) to smart structures, extrinsic Fabry-Perot interferometric F-O sensors, sapphire F-O sensors, two-mode F-O sensors with photoinduced refractive index, an F-O accelerometer using two-mode fibers, and embedded F-O acoustic sensors for flaw detection. Also discussed are an optoelectronic smart structure interface, F-O sensors for simultaneous detection of strain and temperature, an optical Mach-Zehnder interferometer for smart skins, a split-cavity cross-coupled extrinsic fiber interferometer, and an embedded Bragg grating F-O sensor for composite flexbeams, an Er-doped ring-laser strain sensor.

Claus, Richard O.↗

Earth observational research using multistage EOS-like data

This grant is funded as a part of a program in which both research and educational impact are intended. Research work under this grant is directed at the understanding and use of future hyperspectral data such as that from imaging spectrometers. Specifically, the objectives of the work are (1) to prepare suitable means for analyzing data from sensors which have large numbers of spectral bands, (2) to advance the fundamental understanding of the manner in which soils and vegetative materials reflect high spectral resolution optical wavelength radiation, and (3) to maximize the impact of the results on the educational community. Over the life of the grant, the work has thus involved basic Earth science research and information system technique understanding and development in a mutually supportive way, however, more recently it has become necessary to focus the work primarily on areas (1) and (3). During the last year, the level of effort on this grant has been reduced to half its previous value. We have also been advised that this grant will end with the current year, thus this will be the penultimate semiannual progress summary.

Johannsen, C. J.↗

Advances in Thin Film Thermocouple Durability Under High Temperature and Pressure Testing Conditions

Thin film thermocouples for measuring material surface temperature have been previously demonstrated on several material systems and in various hostile test environments. A well-developed thin film fabrication procedure utilizing shadow masking for patterning the sensors elements had produced thin films with sufficient durability for applications in high temperature and pressure environments that exist in air-breathing and hydrogen-fueled burner rig and engine test facilities. However, while shadow masking had been a reliable method for specimens with flat and gently curved surfaces, it had not been consistently reliable for use on test components with sharp contours. This work reports on the feasibility of utilizing photolithography processing for patterning thin film thermocouples. Because this patterning process required changes in the thin film deposition process from that developed for shadow masking, the effect of these changes on thin film adherence during burner rig testing was evaluated. In addition to the results of changing the patterning method, the effects on thin film adherence of other processes used in the thin film fabrication procedure is also presented.

Martin, Lisa C.↗