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At least 937 records · Page 52

Autoregressive distributed lag-based dynamic uniformity modeling and monitoring approaches for superconductor manufacturing

High-temperature superconductors (HTS), known for their high efficiency and low energy loss, have found profound applications across various fields, driving the demand for long, uniformly performing tapes. However, ensuring uniform performance over extended lengths of HTS tapes, often characterized by the consistency of critical current, remains challenging due to fluctuations in growth conditions during manufacturing. Here, to elucidate the mechanisms underlying variations in tape uniformity and enable real-time monitoring of associated parameters, we propose an Autoregressive Distributed Lag (ADL)-based Dynamic Uniformity Modeling and Monitoring (ADUM2) approach. This method integrates uniformity measurement, the identification of critical process parameters and real-time monitoring within the manufacturing process. The ADUM2 approach is applied to the advanced metal organic chemical vapor deposition (A-MOCVD) process, a pilot-scale method for superconductor manufacturing. Our model demonstrates superior performance compared to benchmark methods, accounting for over 80% of the total variance in the data and identifying 13 key process parameters influencing the uniformity of HTS tapes. This study offers significant insights into the high-temperature superconductor manufacturing process and holds the potential to facilitate the production of cost-effective, uniformly performing long superconducting tapes in the future.

autoregressive distributed lag analysis↗

Cryogenic and safety design of the future high field cable test facility at Fermilab

The HFVMTF (High Field Vertical Magnet Test Facility) is a new experimental facility under development at Fermi National Accelerator Laboratory (FNAL) to test large superconducting magnets (up to 20 tons weight and 1.3 m diameter) in a double bath superfluid helium cryostat (1.9 K and 1.2 bar). Coupled with a superconducting dipole magnet fabricated by Lawrence Berkeley National Laboratory (LBNL), this facility will be able to test future high-temperature superconductor (HTS) cables under a background magnetic field of 15 T for fusion magnets. This paper describes the design of the cryostat and its 1.4-meter diameter lambda plate, as well as the different components for a safe operation of the facility, even during critical events such a magnet quench or a vacuum breaking situation. The project is funded by US DOE Offices of Science, High Energy Physics (HEP), and Fusion Energy Sciences (FES).

43 PARTICLE ACCELERATORS↗

Investigations Towards Ultra-Low Cost Nb 3 Sn SRF Fabrication via Melt Casted Bronze Route Processing

Here, a novel approach to fabricating Nb 3 Sn SRF cavities and other RF components using an ultra-low-cost melt casting fabrication process has been investigated. This simple, low cost melt casting technique has the potential to be used to fabricate nearly any superconducting Nb3Sn structure using either the Bronze Route (BR), Internal Tin (IT), External Tin (ET) processes as well as normal conducting pure copper (Cu) cavities. Most of the heat treated samples that were examined using SEM/EDX seemed to show a reasonable correlation of T c onset and transition width (ΔT c ) of the ingots initial/starting Sn content to the desired stoichiometric Nb 3 Sn phase, where the lower starting Sn content coupons resulted in lower T c 's with broader transition widths and the higher starting Sn coupons resulted in higher T c 's with narrower ΔT c ’s. The best samples had T c onsets ~17-18 K and ΔT c 's < 2 K. Two samples were further tested for RF surface resistance (R s ) and Quality Factor (Q) at JLAB. Here, these RF measurements were performed at 7.4 GHz using a calorimetric technique and showed two transitions, one at ~ 8 K and another at ~ 14 K; values of R s were at least two orders of magnitude higher than similar high quality Nb 3 Sn films directly deposited substrates by JLAB and with another superconducting transition close to the superconducting transition temperature of niobium. Substantial improvements in the processing variables ranging from higher quality of the initial ingots with higher Sn content, to better electropolishing and reaction heat treatment regimens will be necessary to realize improved RF performance metrics.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Quality and Loss Factor Analysis of YBCO Superconducting Transmission Lines for Axion Dark Matter Detection

Axion haloscope experiments aim to detect the conversion of axions into microwave photons in a magnetic field, which produces extremely small signals requiring low-loss cryogenic transmission lines for readout to reduce noise and attenuation. Yttrium Barium Copper Oxide (YBCO) cables are a promising candidate. Unlike commonly used low-loss superconducting cables such as Niobium (Nb) and Niobium Titanium (NbTi), which have low critical fields, YBCO is a high-temperature superconductor that can remain stable in strong magnetic fields. We evaluate their suitability by characterizing the quality and loss factors of five stripline resonators (three YBCO, and copper and silver references) from the Brookhaven Technology Group at 77 K without an external field, and cooled to 30 mK in a 14 T magnet. For measurements at 77 K we recorded scattering parameter data and employed Lorentzian and circle-fitting analysis techniques. We identified the best-performing resonator and developed a cryogenic probe for future testing in the magnet at millikelvin temperatures.

Marinos, Zoe [UCLA]↗

Cryogenic cooling for spacecraft sensors, instruments, and experiments

Several disciplines requiring in-space cryogenic cooling are identified including high-energy, gamma-ray, and IR astronomy, relativity missions, and superconducting devices. Radiant coolers are limited in terms of temperature ranges and cooling loads. Other spacecraft cryogenic systems include stored solid cryogenic coolers using materials such as hydrogen, neon, argon, and methane. Two such cooler designs are described including one for the Nimbus F limb radiance inversion radiometer and one for the Nimbus G limb infrared monitoring of the atmosphere. Suggestions for increasing the performance of solid cryogenic coolers are made, such as a multimission cooler, a mechanical refrigerator, Stirling-cycle refrigerators, and Vuilleumier mechanized coolers. Techniques for obtaining cryogenic cooling in the milli-K range are identified as dilution refrigeration and adiabatic demagnetization.

Sherman, A.↗

Landau-Ginzburg theory of charge density wave formation accompanying lattice and electronic long-range ordering

Here we propose an analytical Landau-Ginzburg (LG) theory of the charge density waves coupled with lattice and electronic long-range order parameters. Examples of long-range order include the electronic wave function of superconducting Cooper pairs, structural distortions, electric polarization, and magnetization. We formulate the LG free energy density as a power expansion with respect to the charge density and other long-range order parameters as well as their spatial gradients and biquadratic coupling terms. We introduced a biquadratic coupling between the charge density gradient and long-range order parameters as well as nonlinear higher gradients of the long-range order parameters. The biquadratic gradient coupling is critical to the appearance of different spatially modulated phases in charge-ordered ferroics and high-temperature superconductors. We derived the thermodynamic conditions for the stability of the spatially modulated phases, which are the intertwined spatial waves of charge density and lattice/electronic long-range order. The analytical expressions for the energies of different phases, corresponding order parameters, charge density waves amplitudes, and modulation periods obtained in this paper can be employed to guide the comprehensive physical explanation, deconvolution, and Bayesian analysis of experimental data on quantum materials ranging from charge-ordered ferroics to high-temperature superconductors.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Effect of duration of 120 oC baking on the performance on superconducting radio frequency niobium cavities

Over the last decade much attention was given in increasing the quality factor of superconducting radio frequency (SRF) cavities by impurity doping. Prior to the era of doping, the final cavity processing technique to achieve the high accelerating gradient includes the ?in situ? low temperature baking of SRF cavities at temperature ~ 120 oC for several hours. Here, we present the results of a series of measurements on 1.3 GHz TESLA shape single-cell cavities with successive low temperature baking at 120 oC up to 96 hours. The experimental data were analyzed with available theory of superconductivity to elucidate the effect of the duration of low temperature baking on the superconducting properties of cavity materials as well as the rf performance. In addition, the rf loss related to the trapping of residual magnetic field refereed as flux trapping sensitivity was measured with respect to the duration of 120 oC bake.

Khanal, B. D.↗

Anomalous transport in high-mobility superconducting SrTiO 3 thin films

The study of subtle effects on transport in semiconductors requires high-quality epitaxial structures with low defect density. Using hybrid molecular beam epitaxy (MBE), SrTiO 3 films with a low-temperature mobility exceeding 42,000 cm 2 V -1 s -1 at a low carrier density of 3 × 10 17 cm -3 were achieved. A sudden and sharp decrease in residual resistivity accompanied by an enhancement in the superconducting transition temperature were observed across the second Lifshitz transition where the third band becomes occupied, revealing dominant intraband scattering. These films further revealed an anomalous behavior in the Hall carrier density as a consequence of the antiferrodistortive (AFD) transition and the temperature dependence of the Hall scattering factor. Using hybrid MBE growth, phenomenological modeling, temperature-dependent transport measurements, and scanning superconducting quantum interference device imaging, we provide critical insights into the important role of inter- versus intraband scattering and of AFD domain walls on normal-state and superconducting properties of SrTiO 3 .

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Enhanced Electron-Phonon Coupling for Charge-Density-Wave Formation in La 1.8-$x$ Eu 0.2 Sr $x$ CuO 4+$δ$

Charge density wave (CDW) correlations are prevalent in all copper-oxide superconductors. While CDWs in conventional metals are driven by coupling between lattice vibrations and electrons, the role of the electron-phonon coupling (EPC) in cuprate CDWs is strongly debated. Using Cu L 3 edge resonant inelastic x-ray scattering, we study the CDW and Cu-O bond-stretching phonons in the stripe-ordered cuprate La 1.8-x Eu 0.2 Sr x CuO 4+δ . In this work, we investigate the interplay between charge order and EPC as a function of doping and temperature and find that the EPC is enhanced in a narrow momentum region around the CDW ordering vector. By detuning the incident photon energy from the absorption resonance, we extract an EPC matrix element at the CDW ordering vector of M ≃ 0.36 eV , which decreases to M ≃ 0.30 eV at high temperature in the absence of the CDW. Our results suggest a feedback mechanism in which the CDW enhances the EPC which, in turn, further stabilizes the CDW.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Origins of quench in buffered chemical polished and low temperature baked SRF cavities

Electropolishing (EP) and buffered chemical polishing (BCP) are conventional surface preparation techniques for superconducting radiofrequency (SRF) cavities that remove damaged material from the cavity surface. One main issue with EP and BCP treated SRF cavities is high field Q-slope (HFQS), a drop in quality factor at high gradients that limits quench field. High gradient performance in EP cavities can be improved by applying a low temperature bake (LTB), but LTB does not consistently remove HFQS in BCP cavities. There is no consensus as to the why LTB is not effective on BCP prepared cavities, and the cause of HFQS in BCP cavities is not well understood. We examine the origins of quench in EP, BCP, EP+LTB, and BCP+LTB treated SRF cavities. We also show the effect of these treatments on the onset of HFQS, heating within the cavity up to quench, concentration of free hydrogen, and surface roughness.

43 PARTICLE ACCELERATORS↗

Phonon modes and electron–phonon coupling at the FeSe/SrTiO 3 interface

The remarkable increase in superconducting transition temperature (T c ) observed at the interface of one-unit-cell FeSe films on SrTiO3 substrates (1 uc FeSe/STO) has attracted considerable research into the interface effects. Although this high T c is thought to be associated with electron-phonon coupling (EPC), the microscopic coupling mechanism and its role in the superconductivity remain elusive. Here we use momentum-selective high-resolution electron energy loss spectroscopy to atomically resolve the phonons at the FeSe/STO interface. We uncover new optical phonon modes, coupling strongly with electrons, in the energy range of 75-99 meV. These modes are characterized by out-of-plane vibrations of oxygen atoms in the interfacial double-TiO x layer and the apical oxygens in STO. Our results also demonstrate that the EPC strength and superconducting gap of 1 uc FeSe/STO are closely related to the interlayer spacing between FeSe and the TiOx terminated STO. These findings shed light on the microscopic origin of the interfacial EPC and provide insights into achieving large and consistent T c enhancement in FeSe/STO and potentially other superconducting systems.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Temperature, rf field, and frequency dependence performance evaluation of superconducting niobium half-wave coaxial cavity

Recent advancement in superconducting radio frequency cavity processing techniques, with diffusion of impurities within the RF penetration depth, resulted in high quality factor with increase in quality factor with increasing accelerating gradient. The increase in quality factor is the result of a decrease in the surface resistance as a result of nonmagnetic impurities doping and change in electronic density of states. The fundamental understanding of the dependence of surface resistance on frequency and surface preparation is still an active area of research. Here, we present the result of RF measurements of the TEM modes in a coaxial half-wave niobium cavity resonating at frequencies between 0.3 ? 1.3 GHz. The temperature dependence of the surface resistance was measured between 4.2 K and 1.6 K. The field dependence of the surface resistance was measured at 2.0 K. The baseline measurements were made after standard surface preparation by buffered chemical polishing.

Dhakal, P.↗

Comparative study of bolometric and non-bolometric switching elements for microwave phase shifters

The performance of semiconductor and high critical temperature superconductor switches is compared as they are used in delay-line-type microwave and millimeter-wave phase shifters. Such factors as their ratios of the off-to-on resistances, parasitic reactances, power consumption, speed, input-to-output isolation, ease of fabrication, and physical dimensions are compared. Owing to their almost infinite off-to-on resistance ratio and excellent input-to-output isolation, bolometric superconducting switches appear to be quite suitable for use in microwave phase shifters; their only drawbacks are their speed and size. The SUPERFET, a novel device whose operation is based on the electric field effect in high critical temperature ceramic superconductors is also discussed. Preliminary results indicate that the SUPERFET is fast and that it can be scaled; therefore, it can be fabricated with dimensions comparable to semiconductor field-effect transistors.

Tabib-Azar, Massood↗

Comparative study of bolometric and non-bolometric switching elements for microwave phase shifters

The performance of semiconductor and high critical temperature superconductor switches is compared as they are used in delay-line-type microwave and millimeter-wave phase shifters. Such factors as their ratios of the off-to-on resistances, parasitic reactances, power consumption, speed, input-to-output isolation, ease of fabrication, and physical dimensions are compared. Owing to their almost infinite off-to-on resistance ratio and excellent input-to-output isolation, bolometric superconducting switches appear to be quite suitable for use in microwave phase shifters; their only drawbacks are their speed and size. The SUPERFET, a novel device whose operation is based on the electric field effect in high critical temperature ceramic superconductors is also discussed. Preliminary results indicate that the SUPERFET is fast and that it can be scaled; therefore, it can be fabricated with dimensions comparable to semiconductor field-effect transistors.

Tabib-Azar, Massood↗

Processing Bi-Pb-Sr-Ca-Cu-O superconductors from amorphous state

Researchers produced superconducting ceramics of the Bi-Pb-Sr-Ca-Cu-O system started from a glass. To form the glass, the mixed oxide powder was melted at 1200 C in air. The liquid was quenched rapidly by pouring it onto an aluminum plate and rapidly pressing with another plate. The quenched compound was in the form of black amorphous solid, whose x-ray powder pattern has no crystalline peaks. After heat treatment at high temperatures, the glass crystallized into a superconductor. The crystalline phases in the superconductor identified using x-ray diffraction patterns. These phases were that associated with the superconducting phases of T(sub c) = 80 K (Bi2Ca1Sr2Cu2Ox) and of T(sub c) = 110 K (Bi2Ca2Sr2Cu3Ox). The dc resistivity and the ac susceptibility of these superconductors were studied.

Chiang, C. K.↗

The Fast Alternative Cryogenic Experiment Testbed

One of the challenges in the area of cryogenics for space exploration in the next millennium is providing the capability for inexpensive, frequent, access to space. Faced with this challenge during the International Space Station (ISS) build era, when other Space Shuttle manifesting opportunities are unavailable, a "proof of concept" cryostat has been developed to demonstrate the ability to accommodate low temperature science investigations within the constraints of the Hitchhiker siderail carrier. The Hitchhiker siderail carrier is available on a "mass available" basis during the ISS build era. In fact, several hitchhiker payloads flew with the deployment of the Unity module. Hitchhiker siderail carrier payloads have historically flown an average of about four times a year. A hybrid Solid Neon - Superfluid Helium cryostat has been developed with Janis Research Company to accommodate instruments of 16.5 cm diameter and 30 cm. length. This hybrid approach was taken in part to provide adequate on-orbit lifetime for instruments with high (conducted) heat loads from the instrumentation wiring. Mass, volume, lifetime and the launch hold scenario were all design drivers. In addition, with Ball Aerospace and Technologies Corporation, a multichannel VME architecture Germanium Resistance Thermometer (GRT) readout and heater control servo system has been developed. In a flight system, the cryostat and electronics payloads would be umbilically attached in a paired Hitchhiker siderail mount, and permit on-orbit command and telemetry capability. The results of performance tests of both the cryostat, and a helium sample instrument will be presented. The instrument features a self contained, miniaturized, nano-Kelvin resolution High Resolution Thermometer (HRT). This high level of thermal resolution is achieved through the utilization of a dc Superconducting Quantum Interference Device (SQUID). Although developed for the Low Temperature Microgravity Fundamental Physics investigator community, many design features are applicable in fields such as infrared and x-ray astronomy.

Nash, Alfred↗

Thermal conductivity of RHIC superconducting magnet insulation materials at low temperatures

The Electron-Ion Collider (EIC) is planned to be built upon the Relativistic Heavy Ion Collider (RHIC), which vacuum chamber will need to be upgraded to host the EIC hadron beams. For the beam pipe section running through the RHIC superconducting (SC) magnets, the baseline is to insert a screen that will get cooled by thermal contact to the 4.55 K beam pipe of RHIC. Knowing the material properties of the cold mass is thus crucial to understand which is the final temperature that the screen and the superconducting coils in the magnets will reach during the passage of the EIC beams. The thermal conductivities of two insulation materials in the RHIC superconducting magnets and a reference material were measured at cryogenic temperatures at the Magnet Science and Technology division of the National High Magnetic Field Laboratory (NHMFL). The measurements were performed in a Quantum Design physical property measurement system. This report explains the motivation behind this work and summarizes the measurement method and results.

43 PARTICLE ACCELERATORS↗