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At least 937 records · Page 52
All sourcesNASA NTRSDOE OSTI
DOE OSTI2022

Porosity evolution under increasing tension in wire-arc additively manufactured aluminum using in-situ micro-computed tomography and convolutional neural network

Internal defects such as porosities are often formed in additively manufactured metal components. The pores nucleate, grow, and coalesce to form cracks under loads, leading to eventual catastrophic failure. Here, in this paper, the full-field porosity evolution, including pore growth and coalescence in a wire-arc additively manufactured (WAAM) aluminum alloy cylinder under tension is observed with in-situ X-ray micro-computed tomography (μCT). The pore size distribution, density, and tensile stress are calculated from the volumetric images analyzed by a convolutional neural network (CNN) algorithm, which provides rapid analysis of 12,950 slice images from μCT volumetric images at the reference state and 13 tensile strains. The results show the quantitative evolution of the growth and coalescence of macropores under tension. A strong correlation is found between the local pore volume fraction and the true tensile stress when the tensile strain is larger than 5%.

36 MATERIALS SCIENCE↗
DOE OSTI2021

Iodine Vapor Reactions with Pure Metal Wires at Temperatures of 100–139 °C in Air

In this work, I 2(g) reactions with 11 metal wires (i.e., Al, Ag, Cu, In, Mo, Nb, Ni, Pd, Pt, Sn, Ta) were evaluated at three temperatures (i.e., 100 ± 3°C, 123 ± 4°C, 139 ± 5°C) with exposure times of 24 hours at each temperature. Over these temperatures, some of the metals showed increased mass gain with higher temperatures (i.e., In, Ag, Cu), Sn showed decreased iodine capture at increased temperatures, and most metals (i.e., Mo, Nb, Ni, Pd, Pt, and Ta) showed little to no mass gain at all temperatures. Silver mordenite (AgZ) was used as a standard during these studies and showed a consistent mass gain (m% I ) of 10.6 → 12.8% over this temperature range. The values of mass of iodine captured per mass of starting metal (g g -1 ) ranged widely across the study with the highest values achieved for (in descending order) Sn-T 100°C (4.37), In-T 139°C (3.34), Sn-T 123°C (1.98), In-T 123°C (1.57), Ag-T 139°C (1.19), In-T 100°C (0.97), and Cu-T 139°C (0.71). In some cases, the metal-iodide complex was not stable at the experimental temperature and it was clear some volatility had occurred during the experiment based on discoloration in the vials. These results show that some metals can have extensive reactions with I 2(g) without showing metal-iodide preferences over metal-oxide formation based on thermodynamic predictions. It is possible that materials such as these could be implemented near nuclear facilities to getter I 2(g) in the event of a nuclear accident.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2023

Theoretical Investigations on the Plasmon-Mediated Dissociation of Small Molecules in the Presence of Silver Atomic Wires

Plasmonic nanoparticles can promote bond activation in adsorbed molecules under relatively benign conditions via excitation of the nanoparticle’s plasmon resonance. As the plasmon resonance often falls within the visible light region, plasmonic nanomaterials are a promising class of catalysts. However, the exact mechanisms through which plasmonic nanoparticles activate the bonds of nearby molecules are still unclear. Herein, we evaluate Ag 8 –X 2 (X = N, H) model systems via real-time time-dependent density functional theory (RT-TDDFT), linear response time-dependent density functional theory (LR-TDDFT), and Ehrenfest dynamics in order to better understand the bond activation processes of N 2 and H 2 facilitated by the presence of the atomic silver wire under excitation at the plasmon resonance energies. We find that dissociation is possible for both small molecules at high electric field strength. Activation of each adsorbate is symmetry- and electric field-dependent, and H 2 activates at lower electric field strengths than N 2 . Furthermore, this work serves as a step toward understanding the complex time-dependent electron and electron–nuclear dynamics between plasmonic nanowires and adsorbed small molecules.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2014

Effect of the wire width on the intrinsic detection efficiency of superconducting-nanowire single-photon detectors

A thorough spectral study of the intrinsic single-photon detection efficiency in superconducting TaN and NbN nanowires with different widths has been performed. The experiment shows that the cut-off of the intrinsic detection efficiency at near-infrared wavelengths is most likely controlled by the local suppression of the barrier for vortex nucleation around the absorption site. Beyond the cut-off quasi-particle diffusion in combination with spontaneous, thermally activated vortex crossing explains the detection process. For both materials, the reciprocal cut-off wavelength scales linearly with the wire width where the scaling factor agrees with the hot-spot detection model.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2014

Application of one-dimensional stagnation solutions to three-dimensional simulation of compact wire array in absence of radiation

We investigate the stagnation phase of a three-dimensional (3D), magnetohydrodynamic simulation of a compact, tungsten wire-array Z pinch, under the simplifying assumption of negligible radiative loss. In particular, we address the ability of one-dimensional (1D) analytic theory to describe the time evolution of spatially averaged plasma properties from 3D simulation. The complex fluid flows exhibited in the stagnated plasma are beyond the scope of 1D theory and result in centrifugal force as well as enhanced thermal transport. Despite these complications, a 1D homogeneous (i.e., shockless) stagnation solution can capture the increase of on-axis density and pressure during the initial formation of stagnated plasma. Later, when the stagnated plasma expands outward into the imploding plasma, a 1D shock solution describes the decrease of on-axis density and pressure, as well as the growth of the shock accretion region.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2014

Field effect in the quantum Hall regime of a high mobility graphene wire

In graphene-based electronic devices like in transistors, the field effect applied thanks to a gate electrode allows tuning the charge density in the graphene layer and passing continuously from the electron to the hole doped regime across the Dirac point. Homogeneous doping is crucial to understand electrical measurements and for the operation of future graphene-based electronic devices. However, recently theoretical and experimental studies highlighted the role of the electrostatic edge due to fringing electrostatic field lines at the graphene edges [P. Silvestrov and K. Efetov, Phys. Rev. B 77, 155436 (2008); F. T. Vasko and I. V. Zozoulenko, Appl. Phys. Lett. 97, 092115 (2010)]. This effect originates from the particular geometric design of the samples. A direct consequence is a charge accumulation at the graphene edges giving a value for the density, which deviates from the simple picture of a plate capacitor and also varies along the width of the graphene sample. Entering the quantum Hall regime would, in principle, allow probing this accumulation thanks to the extreme sensitivity of this quantum effect to charge density and the charge distribution. Moreover, the presence of an additional and counter-propagating edge channel has been predicted [P. Silvestrov and K. Efetov, Phys. Rev. B 77, 155436 (2008)] giving a fundamental aspect to this technological issue. In this article, we investigate this effect by tuning a high mobility graphene wire into the quantum Hall regime in which charge carriers probe the electrostatic potential at high magnetic field close to the edges. We observe a slight deviation to the linear shift of the quantum Hall plateaus with magnetic field and we study its evolution for different filling factors, which correspond to different probed regions in real space. We discuss the possible origins of this effect including an increase of the charge density towards the edges.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2014

Localized states in a semiconductor quantum ring with a tangent wire

We extend a special kind of localized state trapped at the intersection due to the geometric confinement, first proposed in a three-terminal-opening T-shaped structure [L. A. Openov, Europhys. Lett. 55, 539 (2001)], into a ring geometry with a tangent connection to the wire. In this ring geometry, there exists one localized state trapped at the intersection with energy lying inside the lowest subband. We systematically study this localized state and the resulting Fano-type interference due to the coupling between this localized state and the continuum ones. It is found that the increase of inner radius of the ring weakens the coupling to the continuum ones and the asymmetric Fano dip fades away. A wide energy gap in transmission appears due to the interplay of two types of antiresonances: the Fano-type antiresonance and the structure antiresonance. The size of this antiresonance gap can be modulated by adjusting the magnetic flux. Moreover, a large transmission amplitude can be obtained in the same gap area. The strong robustness of the antiresonance gap is demonstrated and shows the feasibility of the proposed geometry for a real application.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2015

Polariton dispersion of a quantum wire superlattice system

Superlattices have drawn considerable attention in the recent years. In this work, the behaviour of polaritons in a quantum wire superlattice is analysed both at the brillouin zone edge and at centre of the brillouin zone using LiNbO3/ LiTaO3 as an example. The significance of the polariton modes in both the cases are analysed. New modes on the polaritonic gap, where the propagation of electromagnetic wave is forbidden, is obtained in the system as suggested by some recent literature. The effect on nonlinear interactions of phonon polaritons in LiNbO3/ LiTaO3 superlattices is also discussed.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2015

Dynamics of a wire-to-cylinder atmospheric pressure high-voltage nanosecond discharge

The dynamics of a wire-to-cylinder atmospheric pressure high-voltage nanosecond discharge is studied by the one-dimensional Particle-in-Cell Monte Carlo collisions model in cylindrical coordinates. The x-ray photons emitted from the anode are found to be inconsequential to the generation of dense plasma in the gap. Rather, the electron impact ionization resulting from acceleration of naturally occurring background electrons in the discharge gap are enough to explain the generation of high-density (∼10{sup 15 }cm{sup −3}) non-equilibrium plasma. The influence of the high-voltage rise time on the plasma parameters is discussed.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2016

Experimental results from an X-ray imaging crystal spectrometer utilizing multi-wire proportional counter for KSTAR

The inconsistency of the first experimental results from the X-ray imaging crystal spectrometer for the Korea Superconducting Tokamak Advanced Research device utilizing a multi-wire proportional counter (MWPC) is clarified after improving the photon-count rate of the data acquisition system for the MWPC and ground loop isolator for the whole spectrometer system. The improved MWPC is successfully applied to pure Ohmic plasmas as well as plasmas with high confinement modes.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2022

Pressure Drop in Seven-Pin Wire-Wrapped Rod Bundle for the Sodium Cartridge Loop in Versatile Test Reactor

This work studies the hydrodynamics of the seven pin wire-wrapped rod bundle in the sodium cartridge loop for the Versatile Test Reactor (VTR) through scaled water experiments and computational fluid dynamics (CFD) simulations. Here, the scaling analysis is first performed to demonstrate the hydrodynamic similarity between water and sodium flows at the same Reynolds number Re. A separate-effects test facility is designed and constructed based on the scaling analysis. Detailed experimental data on the pressure drop covering a wide range of Re values (1165 to 27 689) are obtained, which are used to evaluate existing correlations for friction factor and to benchmark CFD simulations. The experimentally determined friction factors f Exp agree well with the Upgraded Cheng and Todreas Detailed Correlation and Pacio-Chen-Todreas Detailed Model within ±7% but are significantly underpredicted by Rehme's correlation by 25%. Various CFD near-wall treatment methods are tested using ANSYS Fluent and evaluated by experimental data. It is found that when the recommended wall y + values are met, most of the near-wall treatment methods can give accurate friction factor predictions. The resolved near-wall method (y + ~ 1) with the Shear Stress Transport k - ω turbulence model and the scalable wall functions (y + > 12) with the realizable k - ε turbulence model can predict f Exp within ±5% The standard wall functions (y + > 30) and nonequilibrium wall functions (y + > 30) with the realizable k - ε model can predict f Exp within ±10%.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗
DOE OSTI2021

Mechanical rolling and annealing of wire-arc additively manufactured stainless steel plates

Thin walls of 304L stainless steel were fabricated by wire-arc additive manufacturing (WAAM) followed by post build thermomechanical processing to modify the as built microstructure and properties. The walls were made using a high-deposition-rate robotically controlled gas-metal arc welding system and were characterized using optical microscopy and tensile tested for mechanical properties. Post processing consisted of mechanical rolling the walls to 25% and 40% strains, followed by annealing at 1050°C to demonstrate a wide range of properties. Results show that WAAM can be used to build custom sized semi-finished parts or blanks that can later be thermomechanically processed to increase strength and ductility through recrystallization of the as built microstructure, and/or processed into desired shapes with improved mechanical properties.

304L stainless steel↗
DOE OSTI2024

Aging heat treatment design for Haynes 282 made by wire-feed additive manufacturing using high-throughput experiments and interpretable machine learning

Wire-feed additive manufacturing (WFAM) produces superalloys with complex thermal cycles and unique microstructures, often requiring optimized heat treatments. To address this challenge, we present a hybrid approach that combines high-throughput experiments, precipitation simulation, and machine learning to design effective aging conditions for the WFAM Haynes 282 superalloy. Our results demonstrate that the γ’ radius is the critical microstructural feature for strengthening Haynes 282 during post-heat treatment compared with the matrix composition and γ’ volume fraction. New aging conditions at 770°C for 50 hours and 730°C for 200 hours were discovered based on the machine learning model and were applied to enhance yield strength, bringing it on par with the wrought counterpart. This approach has significant implications for future AM alloy production, enabling more efficient and effective heat treatment design to achieve desired properties.

CALPHAD↗
DOE OSTI2017

Numerical Stress Analysis during Cooldown and Compressive Loading in an Imperfect Nb 3 Sn Wire

In this paper, high field superconductors are critical to the success of next step magnetic fusion confinement devices such as ITER and DEMO. The low-temperature superconducting material that is currently favored for these applications, Nb 3 Sn, is susceptible to performance due to its brittleness and high strain-sensitivity. Under extreme loads, an irreversible degradation in the maximum critical current density has been shown to occur and believed to be strongly influenced by two factors: plasticity and cracked filaments. Cracks in filaments are induced when sufficiently high stress concentrations occur in the wire. In this paper, we explore using finite element analysis the impact that voids have on the stress distributions and peak stresses under two loading conditions: transverse compressive loading in a 2D model, and a full cool down phase in a 3D model.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2024

Nonreciprocal Coulomb drag between quantum wires in the quasi-one-dimensional regime

Coulomb drag experiments have been an essential tool to study strongly interacting low-dimensional systems. Historically, this effect has been explained in terms of momentum transfer between electrons in the active and the passive layer. We report Coulomb drag measurements between laterally coupled GaAs/AlGaAs quantum wires in the multiple one-dimensional (1D) sub-band regime that break Onsager's reciprocity upon both layer and current direction reversal, in contrast to prior 1D Coulomb drag results. The drag signal shows nonlinear current-voltage (I-V) characteristics, which are well characterized by a third-order polynomial fit. These findings are qualitatively consistent with a rectified drag signal induced by charge fluctuations. However, the nonmonotonic temperature dependence of this drag signal suggests that strong electron-electron interactions, expected within the Tomonaga-Luttinger liquid framework, remain important and standard interaction models are insufficient to capture the qualitative nature of rectified 1D Coulomb drag.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2016

Comparison of tungsten films grown by CVD and hot-wire assisted atomic layer deposition in a cold-wall reactor

In this work, the authors developed hot-wire assisted atomic layer deposition (HWALD) to deposit tungsten (W) with a tungsten filament heated up to 1700–2000 °C. Atomic hydrogen (at-H) was generated by dissociation of molecular hydrogen (H{sub 2}), which reacted with WF{sub 6} at the substrate to deposit W. The growth behavior was monitored in real time by an in situ spectroscopic ellipsometer. In this work, the authors compare samples with tungsten grown by either HWALD or chemical vapor deposition (CVD) in terms of growth kinetics and properties. For CVD, the samples were made in a mixture of WF{sub 6} and molecular or atomic hydrogen. Resistivity of the WF{sub 6}-H{sub 2} CVD layers was 20 μΩ·cm, whereas for the WF{sub 6}-at-H-CVD layers, it was 28 μΩ·cm. Interestingly, the resistivity was as high as 100 μΩ·cm for the HWALD films, although the tungsten films were 99% pure according to x-ray photoelectron spectroscopy. X-ray diffraction reveals that the HWALD W was crystallized as β-W, whereas both CVD films were in the α-W phase.

36 MATERIALS SCIENCE↗
DOE OSTI2015

Electric explosion of fine wires: Three groups of materials

Experimental data demonstrating differences in the structures of channels formed during nanosecond discharges through fine wires made of different materials are presented. In addition to the traditional two classes of metals and alloys (the copper and tungsten groups), a new class is proposed to which materials of the nickel type belong. Their properties combine the characteristic properties of the two traditional groups, due to which they occupy an intermediate position between the latter. This manifests itself in the unstable character of explosion, the type of which can change drastically when changing the ambient medium or other conditions. Most of the reported results were obtained at a small setup with maximum values of the current and voltage of 10 kA and 20 kV, respectively, the current rise time being about 300 ns. An attempt is made to construct a scenario of the development of a nanosecond explosion that would make it possible to qualitatively describe the formation of the discharge channel structure. The analysis is based on the recent experimental results indicating that the cores formed in the course of the discharge have a tubular structure.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2016

Distribution of leakage currents in the cylindrical and conical sections of the magnetically insulated transmission line of the Angara-5-1 facility in experiments with wire arrays

Current leakages in the magnetically insulated transmission lines (MITL) impose restrictions on the transmission of electromagnetic pulses to the load in high-power electrophysical facilities. The multimodule Angara-5-1 facility with an output electric power of up to 6 TW is considered. In this work, the experimental and calculated profiles of leakage currents in two sections of the line are compared when the eight-module facility is loaded by a wire array. The azimuthal distribution of the current in the cylindrical section of the MITL is also considered.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗