Results for “Tank testing” — Page 52

NASA NTRS1987

Development of the helium signature test for orbiter main propulsion system revalidation between flights

This paper presents the development of a test technique for revalidation of the Space Shuttle Orbiter Main Propulsion System during ground turnaround operations between flights of the Space Transportation System (STS). The Main Propulsion System consists of the three Space Shuttle Main Engines (SSME's) and the Main Propulsion System (MPS) connecting the SSME's to the orbiter/ground and orbiter/External Tank (ET) interfaces. The Helium Signature Test (HST) performs an end-to-end leak check of the MPS/SSME subsystems that serves as a final validation of those systems for reuse. The test was initially developed during the ground processing flow prior to the STS-6 launch of orbiter Challenger. The test was developed to fulfill a requirement for an overall subsystem leak check as a result of experience gained during the STS-6 Challenger Flight Readiness Firing (FRF) series, during which leaks were encountered in the SSME's that were not detected by routine fluid joint leak checks. The HST technique is described in detail, including orbiter and test equipment configuration, and compared to other leak detection methods used to revalidate MPS/SSME systems for reuse. The HST data base accumulated since STS-6 is summarized and future test applications are described.

Bilardo, Vincent J., Jr.↗

NASA NTRS1976

Heat transfer test of an 0.006-scale thin-skin thermocouple space shuttle model (50-0, 41-T) in the NASA-Ames Research Center 3.5-foot hypersonic wind tunnel at Mach 5.3 (IH28), volume 1

Data obtained from a heat transfer test conducted on an 0.006-scale space shuttle orbiter and external tank in the NASA-Ames Research Center 3.5-foot Hypersonic Wind Tunnel are presented. The purpose of this test was to obtain data under simulated return-to-launch-site abort conditions. Configurations tested were integrated orbiter and external tank, orbiter alone, and external tank alone at angles of attack of 0, + or - 30, + or - 60, + or - 90, and + or - 120 degrees. Runs were conducted at Mach numbers of 5.2 and 5.3 for Reynolds numbers of 1.0 and 4.0 million per foot, respectively. Heat transfer data were obtained from 75 orbiter and 75 external tank iron-constantan thermocouples.

Cummings, J. W.↗

NASA NTRS2015

Results of Microgravity Fluid Dynamics Captured With the Spheres-Slosh Experiment

This paper provides an overview of the SPHERES-Slosh Experiment (SSE) aboard the International Space Station (ISS) and presents on-orbit results with data analysis. In order to predict the location of the liquid propellant during all times of a spacecraft mission, engineers and mission analysts utilize Computational Fluid Dynamics (CFD). These state-of-the-art computer programs numerically solve the fluid flow equations to predict the location of the fluid at any point in time during different spacecraft maneuvers. The models and equations used by these programs have been extensively validated on the ground, but long duration data has never been acquired in a microgravity environment. The SSE aboard the ISS is designed to acquire this type of data, used by engineers on earth to validate and improve the CFD prediction models, improving the design of the next generation of space vehicles as well as the safety of current missions. The experiment makes use of two Synchronized Position Hold, Engage, Reorient Experimental Satellites (SPHERES) connected by a frame. In the center of the frame there is a plastic, pill shaped tank that is partially filled with green-colored water. A pair of high resolution cameras records the movement of the liquid inside the tank as the experiment maneuvers within the Japanese Experimental Module test volume. Inertial measurement units record the accelerations and rotations of the tank, making the combination of stereo imaging and inertial data the inputs for CFD model validation.

slosh↗

NASA NTRS2015

Results of Microgravity Fluid Dynamics Captured with the Spheres-Slosh Experiment

This paper provides an overview of the SPHERES-Slosh Experiment (SSE) aboard the International Space Station (ISS) and presents on-orbit results with data analysis. In order to predict the location of the liquid propellant during all times of a spacecraft mission, engineers and mission analysts utilize Computational Fluid Dynamics (CFD). These state-of-the-art computer programs numerically solve the fluid flow equations to predict the location of the fluid at any point in time during different spacecraft maneuvers. The models and equations used by these programs have been extensively validated on the ground, but long duration data has never been acquired in a microgravity environment. The SSE aboard the ISS is designed to acquire this type of data, used by engineers on earth to validate and improve the CFD prediction models, improving the design of the next generation of space vehicles as well as the safety of current missions. The experiment makes use of two Synchronized Position Hold, Engage, Reorient Experimental Satellites (SPHERES) connected by a frame. In the center of the frame there is a plastic, pill shaped tank that is partially filled with green-colored water. A pair of high resolution cameras records the movement of the liquid inside the tank as the experiment maneuvers within the Japanese Experimental Module test volume. Inertial measurement units record the accelerations and rotations of the tank, making the combination of stereo imaging and inertial data the inputs for CFD model validation.

slosh↗

NASA NTRS2015

Result of Microgravity Fluid Dynamics Captured with the SPHERES-Slosh Experiment

This paper provides an overview of the SPHERES-Slosh Experiment (SSE) aboard the International Space Station (ISS) and presents on-orbit results with data analysis. In order to predict the location of the liquid propellant during all times of a spacecraft mission, engineers and mission analysts utilize Computational Fluid Dynamics (CFD). These state-of-the-art computer programs numerically solve the fluid flow equations to predict the location of the fluid at any point in time during different spacecraft maneuvers. The models and equations used by these programs have been extensively validated on the ground, but long duration data has never been acquired in a microgravity environment. The SSE aboard the ISS is designed to acquire this type of data, used by engineers on earth to validate and improve the CFD prediction models, improving the design of the next generation of space vehicles as well as the safety of current missions. The experiment makes use of two Synchronized Position Hold, Engage, Reorient Experimental Satellites (SPHERES) connected by a frame. In the center of the frame there is a plastic, pill shaped tank that is partially filled with green-colored water. A pair of high resolution cameras records the movement of the liquid inside the tank as the experiment maneuvers within the Japanese Experimental Module test volume. Inertial measurement units record the accelerations and rotations of the tank, making the combination of stereo imaging and inertial data the inputs for CFD model validation.

slosh↗

NASA NTRS2017

NASA's Space Launch System: Progress Report

NASA and its commercial industry team achieved significant progress in 2016 in manufacturing and testing of the Block 1 vehicle for the first launch of the Space Launch System (SLS). Test and flight article hardware for the liquid hydrogen fuel tank as well as the engine section for the core stage were completed at Michoud Assembly Facility (MAF) in New Orleans. Test stands neared completion at Marshall Space Flight Center for the propellant tanks, engine section, intertank and payload section. Stennis Space Center completed major structural renovations on the B2 test stand, where the core stage "green run" test program will be conducted. The SLS team completed a hotfire test series at Stennis to successfully demonstrate the ability of the RS-25 engine to operate under SLS environments and performance conditions. The team also test fired the second qualification five-segment solid rocket motor and cast the first six motor segments for the first SLS mission. The Interim Cryogenic Propulsion Stage (ICPS) test article was delivered to Marshall for structural tests, and work is nearly finished on the flight stage. Flight software testing completed at Marshall included power quality and command and data handling. In 2017, that work continues. SLS completed Preliminary Design Review (PDR) on the Exploration Upper Stage (EUS), a powerful, human-rated spacecraft that will propel explorers to cis-lunar space. In 2017, hardware will continue to be integrated at MAF for core stage structural test articles and the first two operational flights. RS-25 hotfire testing will continue to explore engine performance, as well as test flight-like software and four new Engine Controller Units (ECUs) for the first mission. Production of development components for a more affordable RS-25 design is underway. Core stage structural test articles have begun arriving at Marshall. While engineering challenges typical of a new development are possible, SLS is working toward launch readiness in late 2018. This paper will discuss these and other technical and programmatic successes and challenges over the past year and provide a preview of work ahead before first flight

Cook, Jerry↗

NASA NTRS1985

Fuel containment, lightning protection and damage tolerance in large composite primary aircraft structures

The damage-tolerance characteristics of high strain-to-failure graphite fibers and toughened resins were evaluated. Test results show that conventional fuel tank sealing techniques are applicable to composite structures. Techniques were developed to prevent fuel leaks due to low-energy impact damage. For wing panels subjected to swept stroke lightning strikes, a surface protection of graphite/aluminum wire fabric and a fastener treatment proved effective in eliminating internal sparking and reducing structural damage. The technology features developed were incorporated and demonstrated in a test panel designed to meet the strength, stiffness, and damage tolerance requirements of a large commercial transport aircraft. The panel test results exceeded design requirements for all test conditions. Wing surfaces constructed with composites offer large weight savings if design allowable strains for compression can be increased from current levels.

Griffin, Charles F.↗

NASA NTRS1999

Design Optimization and Analysis of a Composite Honeycomb Intertank

Intertanks, the structure between tanks of launch vehicles, are prime candidates for weight reduction of rockets. This paper discusses the optimization and detailed follow up analysis and testing of a 96 in. diameter, 77 in. tall intertank. The structure has composite face sheets with an aluminum honeycomb core. The ends taper to a thick built up laminate for a double lap bolted splice joint interface. It is made in 8 full length panels joined with bonded double lap joints. The nominal load is 4000 lb/in. Optimization is by Genetic Algorithm and minimizes weight by varying core thickness, number and orientation of acreage and buildup plies, and the size, number and spacing of bolts. A variety of design cases were run with populations up to 2000 and chromosomes as long as 150 bits. Constraints were buckling; face stresses (normal, shear, wrinkling and dimpling); bolt stress; and bolt hole stresses (bearing, net tension, wedge splitting, shear out and tension/shear out). Analysis is by a combination of elasticity solutions and empirical data. After optimization, a series of coupon tests were performed in conjunction with a rigorous analysis involving a variety of finite element models. This analysis and testing resulted in several small changes to the optimized design. The equation used for hole bearing strength was found to be inadequate, resulting in thicker ends. The core thickness increased 0.05", and potting compound was added in the taper to strengthen the facesheet bond. The intertank has undergone a 250,000 lb limit load test and been mated with a composite liquid hydrogen tank. The tank/intertank unit is being installed in a test stand where it will see 200 thermal/load cycles. Afterwards the intertank will be demated and loaded in compression to failure.

Finckenor, Jeff↗

NASA NTRS2015

Composite Cryotank Technologies and Demonstration

NASA is exploring advanced composite materials and processes to reduce the overall cost and weight of liquid hydrogen (LH2) cryotanks while maintaining the reliability of existing metallic designs. The fundamental goal of the composite cryotank project was to provide new and innovative technologies that enable human space exploration to destinations beyond low-Earth orbit such as the Moon, near-Earth asteroids, and Mars. In September 2011, NASA awarded Boeing the contract to design, manufacture, and test two lightweight composite cryogenic propellant tanks. The all-composite tanks shown iare fabricated with an automated fiber placement machine using a prepreg system of IM7 carbon fiber/CYCOM 5320-1 epoxy resin. This is a resin system developed for out-of-autoclave applications. Switching from metallic to composite construction holds the potential to dramatically increase the performance capabilities of future space systems through a dramatic reduction in weight. Composite Cryotank Technologies and Demonstration testing was an agency-wide effort with NASA Marshall Space Flight Center (MSFC) leading project management, manufacturing, and test; Glenn Research Center leading the materials; and Langley Research Center leading the structures effort for this project. Significant contributions from NASA loads/stress personnel contributed to the understanding of thermal/mechanical strain response while undergoing testing at cryogenic temperatures. The project finalized in September 2014.

Vickers, John↗

NASA NTRS1974

Simulated lightning test shuttle .03 scale model

Lightning Attach Point tests were conducted for the space shuttle launch configuration (Orbiter, External Tank and Solid Rocket Boosters). A series of 250 long spark tests (15 to 20 foot sparks) determined that the orbiter may be struck on the nose, windshield brow, tail and wingtips during launch but not on the main engine nozzles which have been shown to be vulnerable to lightning damage. The orbiter main engine and SRB exhaust plumes were simulated electrically with physical models coated with graded resistance paints. The tests showed that the exhaust plumes from the SRB provide additional protection for the main engine nozzles. However, the tests showed that the Orbiter Thermal Protection System (TPS), which has also been shown to be vulnerable to lightning damage, may be struck during launch. Therefore further work is indicated in the areas of swept stroke studies on the model and on TPS panels. Further attach point testing is also indicated on the free-flying orbiter. Photographs of the test setup are shown.

Clifford, D. W.↗

NASA NTRSDate not supplied

Design of a GRCop-42 Regeneratively Cooled Thrust Chamber Assembly and Feed System

An additively manufactured thrust chamber assembly was designed and printed using laser powder bed fusion. The NASA-developed material GRCop-42 was used for its high strength and high temperature characteristics. The combustion chamber and nozzle utilize regenerative coolant channels to achieve long duration hot fire tests. Design for additive manufacturing was used to create geometries not easily attainable with traditional machining. The thrust chamber assembly was post processed to ensure print quality and verify for testing. A feed system – encompassing all propellant lines, valves, sensors, and tanks – was designed and built to enable steady state, pressure regulated testing. Pressure transducers, thermocouples, and load cells were placed to enable measurements of the propellant properties and engine performance. Venturis and orifices were used throughout the system to control the flow rates to the thrust chamber. Aside from providing propellants, the feed system provides pressure using nitrogen, and purges the lines during shutdown. The design process for this testing platform is described. A testing campaign on the hardware will be conducted by the Akronauts Rocket Design Team at the University of Akron in Spring 2023.

Dillon M. Petty↗

NASA NTRSDate not supplied

Design of a GRCop-42 Regeneratively Cooled Thrust Chamber Assembly and Feed System

An additively manufactured thrust chamber assembly was designed and printed using laser powder bed fusion. The NASA-developed material GRCop-42 was used for its high strength and high temperature characteristics. The combustion chamber and nozzle utilize regenerative coolant channels to achieve long duration hot fire tests. Design for additive manufacturing was used to create geometries not easily attainable with traditional machining. The thrust chamber assembly was post processed to ensure print quality and verify for testing. A feed system – encompassing all propellant lines, valves, sensors, and tanks – was designed and built to enable steady state, pressure regulated testing. Pressure transducers, thermocouples, and load cells were placed to enable measurements of the propellant properties and engine performance. Venturis and orifices were used throughout the system to control the flow rates to the thrust chamber. Aside from providing propellants, the feed system provides pressure using nitrogen, and purges the lines during shutdown. The design process for this testing platform is described. A testing campaign on the hardware will be conducted by the Akronauts Rocket Design Team at the University of Akron in Spring 2023.

Dillon M. Petty↗

DOE OSTI2020

NDE Technology Engineering Program for Hanford DST Non-Visual Volumetric Inspection Technology: Phase II RAVIS Radiation Tolerance Test Report

This test report provides the results of radiation tolerance robustness testing that was performed on samples of robotic components and an ultrasonic guided wave air-slot sensor that represent components/sub-systems of the Robotic Air-slot Volumetric Inspection System (RAVIS) that has been engineered for volumetric inspection of Hanford tank bottom plates via under-tank refractory pad air-slots. The specific components tested for 1) functionality during active irradiation and 2) tolerance to cumulative radiation dose (until failure or upon reaching a cumulative dose test limit) were: • four samples each of a printed circuit board (PCB) and direct current (DC) motor, which are robotic components, and • 26 ultrasonic piezoelectric elements (samples) inside an air-slot sensor. The robotic components are part of the RAVIS air-slot inspection crawler drive control system that is responsible for remote communication with and actuation of the air-slot inspection crawler. The failure of either of these components during under-tank deployment would require manual retrieval via the crawler’s tether, which risks damage to the robot/refractory/tank. Preemptive replacement of the components at appropriately conservative dose/time intervals informed by failure dose would reduce the likelihood of under-tank failure. The components were included in radiation tolerance testing to quantify their failure doses to inform replacement intervals. The air-slot sensor is responsible for collecting ultrasonic inspection data (scan images) for the tank bottom plates during under-tank deployment. Compromised signal quality due to elevated noise levels caused by gamma radiation would compromise inspection performance. The air-slot sensor was included in radiation tolerance testing to quantify the impact of active irradiation on sensor signal quality. The irradiation and in-situ functional tests of the PCBs, DC motors and air-slot sensor took place in June and July 2020 at the Pacific Northwest National Laboratory. Testing was performed at a gamma dose rate near 300 rad/hr., which, in the absence of under-tank dose rate data, has been conservatively estimated to be the upper-bound dose rate beneath the primary tanks at Hanford. Irradiation took place at elevated temperatures of 150-200°F to determine failure doses that reflect the compounding effects of gamma radiation and heat. The test results revealed: • The DC motors can tolerate being actively irradiated at the high dose rate at 200°F and can tolerate a cumulative dose of 300,000 rad, that which would be incurred after 5 years of service at the 300 rad/hr dose rate. The component therefore meets minimum and preferred radiation tolerance and lifecycle requirements for robotic components. • The air-slot sensor can tolerate being actively irradiated at the high dose rate at 150°F and can tolerate a cumulative dose of 60,000 rad, that which would be incurred after 1 year of service at the 300 rad/hr dose rate. The sensor therefore meets minimum radiation tolerance and lifecycle requirements. • The PCB can tolerate being actively irradiated at the high dose rate, but can only tolerate a cumulative dose of 19,000 rad at 150-200°F. The PCB does not meet minimum radiation tolerance and lifecycle requirements; however, because the component is considered replaceable, it can be replaced before a cumulative dose of 19,000 rad is reached, determined through either monitoring with a dosimeter or scheduled time intervals that are calculated based on conservative estimates of under-tank dose rates.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

DOE OSTI2021

Influence of Heave Plate Topology on Reaction Force

In this study, we explore the role of heave plate topology on fluid reaction forces using three, representative shapes: a hexagonal flat plate, a hexagonal conic with an open top, and the same with a closed top that encloses a fluid mass. We force each test article sinusoidally in a quiescent tank and decompose the reaction force using forms of the Morison equation for phase-invariant and phase-dependent parameterizations. We find that a flat plate generates 5.3 % more fluid reaction force than the open conic topology, and 21.4% more than the enclosed conic. Asymmetric topologies generate asymmetric reaction forces, but the magnitude of asymmetry is limited by nearly symmetric fluid inertia forces, which dominate over drag for these test articles. Additionally, we observe asymmetric vortex dynamics for the flat plate when the Keulegan-Carpenter number is between 1 and 2, accompanied by a shift in the phase of the peak force by of the oscillation period. As a consequence of this shift, the hydrodynamic coefficients estimated from the phase-dependent Morison equation decomposition are asymmetric, suggesting that phase-dependent representations may not provide physical insight in some hydrodynamic regimes.

added mass↗

NASA NTRS2008

Return to Mercury: A Comparison of Solar Simulation and Flight Data for the MESSENGER Spacecraft

The MErcury, Surface, Space, ENvironment GEochemistry and Ranging (MESSENGER) spacecraft is a NASA Discovery Mission spacecraft developed and operated by the Johns Hopkins University Applied Physics Laboratory. It was launched on August 3, 2004 and is currently on a course for Mercury orbit insertion in March 2011. To date the mission trajectory has taken the spacecraft to minimum solar distances of 0.332 and 0.313 AU and on January 14, 2008 the first flyby of Mercury in 33 years. From launch through the latest perihelion passage temperature performance data has been collected for the sun facing Digital Sun Sensors (DSS), the sun facing phased array and low gain (omni) antennas, the solar arrays, the sunshade and the two sun facing attitude control 4.4 N thrusters. Prior to launch, extensive solar simulation testing was conducted at the Glenn Research Center, Tank 6 solar simulation facility in Cleveland Ohio. Flight hardware qualification units representing these Sun exposed components were tested in solar environments that represented near mission minimum solar distance as to verify the thermal designs and the material used in fabrication. The paper will review the thermal designs of these components and their thermal performance to date as compared to the solar simulation testing.

Ercol, Carl J.↗

DOE OSTI2022

Ion Exchange Processing of AP-105 Hanford Tank Waste through Crystalline Silicotitanate in a Staged 2- then 3-Column System (Rev.1)

The Tank Side Cesium Removal (TSCR) system, under development by Washington River Protection Solutions LLC (WRPS), will send initial low-activity Hanford waste tank supernate feeds to the Hanford Waste Treatment and Immobilization Plant (WTP) Low-Activity Waste (LAW) Facility. In addition to entrained solids removal from the supernate, the primary goal of TSCR is to remove cesium-137 ( 137 Cs) by ion exchange, allowing contact handling of the liquid effluent product at the WTP. Crystalline silicotitanate (CST) ion exchange media, manufactured by Honeywell UOP, LLC (product IONSIVTM R9140-B), was selected as the ion exchange media at TSCR. CST is a non-elutable inorganic material that has demonstrated robust chemical, physical, and radiation tolerance while maintaining functionality. However, exchange kinetics of Cs onto CST is slow, resulting in low utilization of the CST Cs load capacity before unacceptable Cs breakthrough. Two process flow designs have been tested, as follows. 1. Lead-lag column processing: The lead column was removed after the lag column effluent reached the waste acceptance criteria (WAC) limit, the lag column was moved into the lead position, and a new lag column was installed. This format used ~52% Cs load capacity on the lead column. 2. Lead-lag-polish column processing: The processing was stopped when the polish column effluent reached the WAC limit. This format resulted in 81% Cs load capacity on the lead column. Testing with diluted feed from Hanford tank AP-105 (AP-105DF) incorporated a nuanced change to the lead-lag-polish column system where the polish column was inserted when the lag column effluent reached WAC limit. A 10.9-L volume of AP-105DF (diluted to 5.6 M Na) was processed through the Direct Feed Test Platform system, established at Pacific Northwest National Laboratory to support small-scale waste qualification efforts. The columns consisted of 10-mL CST beds (CST Lot 2002009604, sieved to screen out >30-mesh particles) placed in 1.5-cm-inner-diameter columns. Feed was processed at 1.83 bed volumes (BV) per hour; the flowrate, in terms of contact time with the CST bed, matched the expected flowrate at TSCR. The <30-mesh CST sieve cut was expected to provide appropriate performance scaling to a full-height column. The installation of the polish column later in processing (after processing 523 BVs) did not appear to fundamentally change the utilization of the lead column for Cs exchange nor did it extend the total feed processing volume when compared to the previous test with AP-107 feed. Table ES.1 and Figure ES.1 summarize the measured AP-105DF Cs load performance.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

DOE OSTI2023

Non-Fouling, Low Cost Electrolytic Coagulation & Disinfection for Treating Flowback and Produced Water for Reuse

Executive Summary This Final Report is composed of two major sections. The first section presents experimental results obtained in the laboratory during Budget Period 1. The second section presents results from the field test conducted during Budget Period 2. Laboratory Results This research investigated a novel electrochemical process for producing a ferric iron coagulant for use in treating flowback and produced water from hydraulic fracturing and oil production operations. The treatment system improves the effectiveness and lowers the cost of coagulation processes using Fe3+ as the coagulant. The electrolytic coagulant generation (ECG) system uses an electrochemical cell to produce acid and base from oilfield brine solutions. The acid is used to dissolve scrap iron to provide a Fe3+ coagulating agent. The base is used to neutralize the treated water. Compared to conventional electrocoagulation (EC), the main advantage of the ECG system is an order of magnitude lower cost for the source of iron. The second advantage over conventional EC is that it can deliver Fe3+ doses greater than 1 mM, since it is not limited by the amount of dissolved oxygen in the water required to oxidize ferrous to ferric iron. The capital costs for conventional EC and the ECG system are similar, but the operational costs for the ECG system are an order of magnitude lower than conventional EC. The combined costs for iron and electrical energy for treating 1 m3 of FPW with 1 mM Fe3+ is estimated to be $0.87 for conventional EC, and $0.087 for the ECG system. The estimated all-in cost for treating FPW with a 2 mM Fe3+ dose is $0.73/m3 ($0.12/bbl). Field Test Results The field test was conducted at the Paul Foster Central Tank Battery (CTB) in Lea County, New Mexico from November 10, 2022 through December 15, 2022. The feed water to the system was produced water from the Tatanka 1H formation. After approximately two weeks of testing, the initial batch of produced water had been treated and no untreated produced water was available. Thus, after this time, the feed water to the system consisted of previously treated water (i.e., recycled water). The recycled water had nearly all colloidal particles removed, and had a much lower alkalinity due to precipitation of carbonate minerals during the first pass through the system. Although the recycled water was not an ideal test solution due to its low particulate concentrations, its lower alkalinity did allow us to identify the main problem with the treatment system. The main problem with the treatment system was caused by the high alkalinity of the initial feed water (5.4 meq/L) that consumed a significant fraction of the electrochemically generated acid. This resulted in pH values exiting the iron contact tank that were too high to dissolve enough iron to effectively treat the produced water. Tests performed with recycled water with lower alkalinity did not have this issue, and dissolved iron concentrations greater than 20 mM could be achieved. One consistent observation was that effluent water from the iron contact tank was always free of particulates, even when fed with circumneutral solutions. This suggests that there is no need to dissolve high concentrations of iron if all the water to be treated is passed through the scrap iron canister. In this case, dissolved O2 and hypochlorous acid can promote sufficient iron corrosion to provide an effective coagulating agent – even in neutral pH water. This solves the problem resulting from highly alkaline produced water. Modifications to the design of the treatment system were made based on the field test results. These modifications will add minimal additional cost, and were tested in bench-scale laboratory experiments. In short-term testing, the modified treatment process was able to remove colloidal FeS particulates to levels below detection. Long-term, steady state testing will be required to determine whether the modified process is suitable for commercial treatment systems.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2020

Testing of an AP-105 Precipitation Simulant

A tank AP-105 chemical simulant was developed and diluted with Washington River Protection Solutions (WRPS)-supplied raw water to evaluate the stability of AP Farm wastes with respect to precipitation under Direct Feed Low-Activity Waste (DFLAW)-typical waste feed staging operations. The current report provides a high-level summary of the basis for simulant selection, the recommended (and prepared) simulant chemistry, and observed stability with respect to solids formation upon simulant preparation and subsequent dilution with raw water.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗