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At least 919 records · Page 51
All sourcesNASA NTRSDOE OSTI
NASA NTRS1985

Bonding and nondestructive evaluation of graphite/PEEK composite and titanium adherends with thermoplastic adhesives

Bonded single overlap shear specimens were fabricated from Graphite/PEEK (Polyetheretherketone) composite adherends and titanium adherends. Six advanced thermoplastic adhesives were used for the bonding. The specimens were bonded by an electromagnetic induction technique producing high heating rates and high-strength bonds in a few minutes. This contrasts with conventionally heated presses or autoclaves that take hours to process comparable quality bonds. The Graphite/PEEK composites were highly resistant to delamination during the testing. This allowed the specimen to fail exclusively through the bondline, even at very high shear loads. Nondestructive evaluation of bonded specimens was performed ultrasonically by energizing the entire thickness of the material through the bondline and measuring acoustic impedance parameters. Destructive testing confirmed the unique ultrasonic profiles of strong and weak bonds, establishing a standard for predicting relative bond strength in subsequent specimens.

Hodges, W. T.↗
NASA NTRS1987

Polyenamines for Films, Coatings, and Adhesives

Easy process makes polymers with good mechanical properties. Synthesis involves Michael-type addition polymerization of two diacetylenic diketones, with various aromatic diamines in m-cresol at 60 to 130 degrees C. Technique provides synthetic route to high-molecular-weight polyenamines with moderate thermal stability and good mechanical properties. Polyenamines produced exhibit potential for use as films, coatings, adhesives, molding compounds, and composite matrices.

Hergenrother, Paul M.↗
NASA NTRS1987

High-Temperature Copolyimide Adhesive

Random Copolyimide, called STPI/LARC, prepared from commercially available materials. Being investigated for use as adhesive or matrix resin for aircraft applications.

Progar, Donald J.↗
NASA NTRS1987

Testing Adhesive Bonds to Cloths

Nondestructive tool simple and inexpensive. Easy-to-use tool nondestructively tests strength of adhesive bond between cloth and straight rigid edge. Developed for testing advanced flexible reusable surface insulation.

Thomann, David G.↗
NASA NTRS1986

The role of damage-softened material behavior in the fracture of composites and adhesives

Failure mechanisms of materials under very high strains experienced at and ahead of the crack tip such as formation, growth, and interaction of microvoids in ductile materials, microcracks in brittle solids or crazes in polymers and adhesives are represented by one-dimensional, nonlinear stress-strain relations possessing different ways by which the material loses capacity to carry load up to fracture or total separation. A double cantilever beam (DCB) type specimen is considered. The nonlinear material is confined to a thin strip between the two elastic beams loaded by a wedge. The problem is first modeled as a beam on a nonlinear foundation. The pertinent equation is solved numerically as a two-point boundary value problem for both the stationary and the quasi-stationay propagating crack. A finite element model is then used to model the problem in more detail in order to assess the adequacy of the beam model for the reduction of experimental data to determine in-situ properties of the thin interlayer.

Ungsuwarungsri, T.↗
NASA NTRS1986

Effect of adherend thickness and mixed mode loading on debond growth in adhesively bonded composite joints

Symmetric and unsymmetric double cantilever beam (DCB) specimens were tested and analyzed to assess the effect of: (1) adherend thickness, and (2) a predominantly mode I mixed mode loading on cyclic debond growth and static fracture toughness. The specimens were made of unidirectional composite (T300/5208) adherends bonded together with EC3445 structural adhesive. The thickness was 8, 16, or 24 plies. The experimental results indicated that the static fracture toughness increases and the cyclic debond growth rate decreases with increasing adherend thickness. This behavior was related to the length of the plastic zone ahead of the debond tip. For the symmetric DCB specimens, it was further found that displacement control tests resulted in higher debond growth rates than did load control tests. While the symmetric DCB tests always resulted in cohesive failures in the bondline, the unsymmetric DCB tests resulted in the debond growing into the thinner adherend and the damage progressing as delamination in that adherend. This behavior resulted in much lower fracture toughness and damage growth rates than found in the symmetric DCB tests.

Mangalgiri, P. D.↗
NASA NTRS1977

Aminophenoxycyclotriphosphazene cured epoxy resins and the composites, laminates, adhesives and structures thereof

Aminophenoxy cyclotriphosphazenes such as hexakis (4-aminophenoxy) cyclotriphosphazene and tris (4-aminophenoxy)-tris phenoxy cyclotriphosphazene are used as curing agents for epoxy resins. These 1,2-epoxy resins are selected from di- or polyepoxide containing organic moieties of the formula (CH2-CHO-CH2) m-W-R-W- (CH2CH-CH2O)m where R is diphenyl dimethylmethane, diphenylmethane; W is a nitrogen or oxygen atom; and m is 1 when W is oxygen and 2 when W is nitrogen. The resins are cured thermally in stages at between about 110 to 135 C for between about 1 and 10 min, then at between about 175 to 185 C for between 0.5 to 10 hr and post cured at between about 215 and 235 C for between 0.1 and 2 hr. These resins are useful for making fire resistant elevated temperature stable composites, laminates, molded parts, and adhesives and structures, usually for aircraft secondary structures and for spacecraft construction.

Kumar, Devendra↗
NASA NTRS1987

The role of damage-softened material behavior in the fracture of composites and adhesives

The failure mechanism of polymer composites and adhesives with high strain in the zone near and ahead of the crack tip is investigated analytically, summarizing the findings of Ungsuwarungsri (1986). A double-cantilever-beam specimen with the nonlinear material confined to a thin strip between two wedge-loaded elastic beams is modeled as a beam on a nonlinear foundation; the two-point boundary-value problem for stationary and propagating cracks is solved numerically; and an FEM approach is applied to study the behavior of the nonlinear strip in detail. Typical results are presented in extensive graphs, and the accuracy and efficiency of the present method are shown to be superior to those of the Berry (1963) procedure.

Ungsuwarungsri, T.↗
NASA NTRS1988

Adhesive properties of LARC-CPI, a new semi-crystalline polyimide

As part of an effort on high temperature structural resins for aerospace applications, a new family of polyimides containing carbon and ether connecting groups between aromatic rings were prepared. Several of these polyimides were semicrystalline. One polyimide, designated LARC-CPI, with a glass transition temperature of 222 C and a crystalline melt temperature of 350 C, was evaluated in the form of an adhesive, film, and molding. Unoriented films exhibited excellent resistance to solvents and strong bases and high tensile properties. Compact tension specimens gave very high fracture toughness values. Titanium tensile shear specimens provided exceptional strength under a variety of test conditions. The chemistry and the physical and mechanical properties of LARC-CPI are discussed.

Hergenrother, P. M.↗
NASA NTRS1988

Poly(imide-siloxane) segmented copolymer structural adhesives prepared by bulk and solution thermal imidization

The improved properties that have been demonstrated through thermal solution imidization in the case of polyimides and poly(imide-siloxane) segmented copolymers suggests significant potential for application of these new materials. Specifically, the enhancement in solubility, moisture reduction, and processability observed through this solution technique is quite dramatic. Previous work has shown that the presence of low amounts of siloxane does not detract significantly from the lap shear strength of these materials to titanium in the case of bulk thermal imidization synthesis. In addition, the siloxane incorporation results in the added advantage of resistance to hot, wet environments. This added durability is presumably due to the hydrophobic siloxane segments preventing the uptake of water at the critical interphase between the adhesive and the adherend. This paper discusses the extension of this work to the solution imidization synthesis technique recently developed in our laboratory. Results dealing with the absolute bond strengths as well as durability and failure surface analysis will be presented.

Bott, R. H.↗
NASA NTRS1988

Particle adhesion to surfaces under vacuum

The release of glass beads and standard dust from aluminum and glass substrates under centrifugation (simulating atmospheric pressure, low vacuum, and high vacuum conditions) was measured, with application to the estimation of contaminant particle release during spacecraft launch. For particles in the 10-100 micron range, dust was found to adhere more strongly than glass beads in all the cases considered. For most of the cases, dust and glass beads adhered more strongly to glass than to aluminum at all pressures. The adhesion force for dust on glass at 10 torr was shown to be as small as the value for dust on aluminum.

Barengoltz, Jack B.↗
NASA NTRS1988

Improving the fatigue resistance of adhesive joints in laminated wood structures

The premature fatigue failure of a laminated wood/epoxy test beam containing a cross section finger joint was the subject of a multi-disciplinary investigation. The primary objectives were to identify the failure mechanisms which occurred during the finger joint test and to provide avenues for general improvements in the design and fabrication of adhesive joints in laminated wood structures.

Laufenberg, Theodore L.↗
NASA NTRS1987

Adhesive properties of a semi-crystalline polyimide

Adhesive and film properties of a new semi-crystalline polyimide, designated LARC-CPI, having a glass transition temperature of 222 C and a crystalline melt temperature of 350 C are presented. The films exhibited excellent resistance to solvents and strong base. Compact tension specimens from LARC-CPI moldings displayed a fracture energy of 37.8 lb/sq in. Titanium tensile shear specimens gave strengths of 6250 psi initially at 25 C, 7120 psi at 25 C after 1000 hours at 232 C, 2800 psi at 232 C after annealing for 5 hours at 300 C, and 3670 psi at 232 C after 100 hours at 316 C in air.

Hergenrother, P. M.↗
NASA NTRS1988

Adhesion scratch testing - A round-robin experiment

Six sets of samples, TiN coated by chemical or physical vapor deposition methods (CVD or PVD) onto cemented carbide or high-speed steel (HSS), and TiC coated by CVD onto cemented carbide have been scratch tested using three types of commercially available scratch adhesion tester. With exception of one cemented carbide set, the reproducibility of the critical loads for any given set with a given stylus is excellent, about + or - 5 percent, and is about + or - 20 percent for different styli. Any differences in critical loads recorded for any given sample set can be attributed to the condition of the stylus (clean, new, etc.), the instrument used, the stylus itself (friction coefficient, etc.), and the sample set itself. One CVD set showed remarkably large differences in critical loads for different styli, which is thought to be related to a mechanical interaction between stylus and coating which is enhanced by a plastic deformability in the film related to the coating microstructure. The critical load for TiN on HSS increases with coating thickness, and differences in frictional conditions led to a systematic variation in the critical loads depending on the stylus used.

Perry, A. J.↗
NASA NTRS1990

Evaluation of two bisimide additives in LARC-TPI adhesive

The processability of aromatic polyimides can be improved by the addition of bis (amide) acids or bisimides to LARC-TPI. These low molecular weight additives apparently lower the melt viscosity of aromatic polyimides without affecting the glass transition temperature. Well-consolidated, fiber reinforced composites were fabricated using this technology. LARC-TPI can be processed as a thermoplastic polyimide to form high strength bonds, however, this is generally accomplished by processing at relatively high bonding pressures. An adhesive investigation is presented on the effects of two bisimide additives to LARC-TPI in an attempt to improve the bonding process by lowering the viscosity of the material to achieve improved bond strength properties. Apparently, the high flow which is exhibited by the additives when they melt, tended to be masked by the more viscous LARC-TPI.

Progar, Donald J.↗
NASA NTRS1991

Synthesis of imide/arylene ether copolymers for adhesives and composite matrices

A series of imide/arylene ether copolymers were prepared from the reaction of an amorphous arylene ether oligomer and a semi-crystalline imide oligomer. These copolymers were thermally characterized and mechanical properties were measured. One block copolymer was endcapped and the molecular weight was controlled to provide a material that displayed good compression moldability and attractive adhesion and composite properties.

Jensen, B. J.↗
NASA NTRS1991

Early focus development effort, ultrasonic inspection of fixed housing metal-to-adhesive bondline

An ultrasonic technique was developed for the fixed housing metal-to-adhesive bondline that will support the Flight 15 time frame and subsequent motors. The technique has the capability to detect a 1.0 inch diameter unbond with a 90 percent probability of detection (POD) at a 95 percent confidence level. The technique and support equipment will perform within the working envelope dictated by a stacked motor configuration.

Hartmann, John K.↗
NASA NTRS1989

Adhesive bond evaluation using phase sensitive detection techniques

Quadrature phase detection techniques have been used to monitor the amplitude and phase of a toneburst ultrasonic wave normally reflected from adhesively-bonded steel/rubber interface. The measured phase change values of the reflected signals were found to correlate with variations in sample preparation. It was determined that measured phase shift changes were larger for samples with weaker bonds as manifested by smaller measured values of the applied tensile loads at failure. A model calculation which incorporates the concept of interfacial strength into the usual problem of wave propagation in multi-layered isotropic elastic media was used to deduce a bond-quality parameter from an experimentally measured phase shift.

Smith, Alphonso C.↗