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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 919 records · Page 51
All sourcesNASA NTRSDOE OSTI
DOE OSTI2023

SULI Internship Deliverables (Flow Orifice Design: Measuring Degas Flow of Experiment Loops at the Advanced Test Reactor)

These deliverables present a design for a new orifice flow meter to be installed in three experiment loops at the Advanced Test Reactor. The current configuration of the experiment loop system has an orifice that is not properly sized to the low flow rates of the degas line of the pressurizer system, causing inaccurate flow measurements. Under consideration of flow conditions and system constraints, an iterative procedure was utilized to determine the optimal sizing for a new orifice. This orifice is designed to accurately and precisely measure the flow rate of the degas line, which will consequently improve control of the pressure and chemistry of the loop pressurizer system. The scope of this project includes recommendations for orifice sizing, material, flange type, face type, and installation location on the loop piping spools. The design is suitable for experiment loops 1D-N, 2B-SE, and 2D-SW and meets all necessary standards.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗
NASA NTRS1989

Laser light scattering review

Since the development of laser light sources and fast digital electronics for signal processing, the classical discipline of light scattering on liquid systems experienced a strong revival plus an enormous expansion, mainly due to new dynamic light scattering techniques. While a large number of liquid systems can be investigated, ranging from pure liquids to multicomponent microemulsions, this review is largely restricted to applications on Brownian particles, typically in the submicron range. Static light scattering, the careful recording of the angular dependence of scattered light, is a valuable tool for the analysis of particle size and shape, or of their spatial ordering due to mutual interactions. Dynamic techniques, most notably photon correlation spectroscopy, give direct access to particle motion. This may be Brownian motion, which allows the determination of particle size, or some collective motion, e.g., electrophoresis, which yields particle mobility data. Suitable optical systems as well as the necessary data processing schemes are presented in some detail. Special attention is devoted to topics of current interest, like correlation over very large lag time ranges or multiple scattering.

Schaetzel, Klaus↗
NASA NTRS2011

Size Optimization for Mirror Segments for X-Ray Optics

The flight mirror assemblies (FMA) for X-ray telescopes similar to that of the International X-ray Observatory (IXO) concept consist of several thousands of individual mirror segments. The size, shape, and location of these mirrors affect many characteristics of the telescope design. Mission requirements among other factors in turn restrict mirror segment parameters such as thickness, axial- length, azimuthal span, and mass density. This paper provides an overview of the critical relationships relating to mirror segment size and configuration throughout the design and analysis of an X-ray mirror assembly. A computational analysis is presented in the form of ray tracing pairs of thin X-ray mirror segments of varying sizes aligned in gravity and supported using kinematic constraints with corresponding self weight distortions calculated using finite element analysis (FEA). The work in this paper may be used as a starting point for determining mirror segment sizes for X-ray missions like that of IXO and beyond.

Biskach, Michael P.↗
DOE OSTI2024

Automated Gold Nanorod Spectral Morphology Analysis Pipeline

The development of a colloidal synthesis procedure to produce nanomaterials with high shape and size purity is often a time-consuming, iterative process. This is often due to quantitative uncertainties in the required reaction conditions and the time, resources, and expertise intensive characterization methods required for quantitative determination of nanomaterial size and shape. Absorption spectroscopy is often the easiest method for colloidal nanomaterial characterization. However, due to the lack of a reliable method to extract nanoparticle shapes from absorption spectroscopy, it is generally treated as a more qualitative measure for metal nanoparticles. This work demonstrates a gold nanorod (AuNR) spectral morphology analysis tool, called AuNR-SMA, which is a fast and accurate method to extract quantitative structural information from colloidal AuNR absorption spectra. To demonstrate the practical utility of this model, we apply it to three distinct applications. First, we demonstrate this model's utility as an automated analysis tool in a high-throughput AuNR synthesis procedure by generating quantitative size information from optical spectra. Second, we use the predictions generated by this model to train a machine learning model to predict the resulting AuNR size distributions under specified reaction conditions. Third, we apply this model to spectra extracted from the literature where no size distributions are reported and impute unreported quantitative information on AuNR synthesis. This approach can potentially be extended to any other nanocrystal system where absorption spectra are size dependent, and accurate numerical simulation of absorption spectra is possible. In addition, this pipeline could be integrated into automated synthesis apparatuses to provide interpretable data from simple measurements, help explore the synthesis science of nanoparticles in a rational manner, or facilitate closed-loop workflows.

36 MATERIALS SCIENCE↗
NASA NTRS1984

An approach for automated analysis of particle holograms

A simple method for analyzing droplet holograms is proposed that is readily adaptable to automation using modern image digitizers and analyzers for determination of the number, location, and size distributions of spherical or nearly spherical droplets. The method determines these parameters by finding the spatial location of best focus of the droplet images. With this location known, the particle size may be determined by direct measurement of image area in the focal plane. Particle velocity and trajectory may be determined by comparison of image locations at different instants in time. The method is tested by analyzing digitized images from a reconstructed in-line hologram, and the results show that the method is more accurate than a time-consuming plane-by-plane search for sharpest focus.

Stanton, A. C.↗
NASA NTRS1977

Sizes and albedos of the larger asteroids

The purpose of the present paper is to review all asteroid diameter measurements, current through mid-1976, and to combine them in a consistent way to give the best available estimates for a sample totalling 187 objects. From these diameters it is possible to determine the size-distributions of minor planets down to diameters of 50 km in the inner belt and 100 km in the outer belt. The associated albedos further indicate the distribution of objects of the C, S, and M classes throughout the belt.

Morrison, D.↗
DOE OSTI2023

Functionalized porous organic polymers as uranium nano-traps for efficient uranium extraction

Compositions are provided for efficient uranium extraction, for example from wastewater, seawater, or other water sources. The compositions can include a functionalized porous organic polymer functionalized with one or more uranium binding moieties, e.g. having a plurality of amidoxime or amidrazone groups covalently attached thereto. The compositions can include covalent organic frameworks, porous aromatic frameworks, and various porous organic polymers, especially those having a hierarchical pore size distribution over a range of pore sizes. The compositions can have functional groups such as amidoxime or an amidrazone covalently attached thereto. The hierarchical pore size distribution can be determined based upon at least 60% of the pore sizes in the range of pore sizes having a pore volume of at least 0.01 cm 3 g −1 in the pore size distribution at 77 K. Methods of making the compositions and methods of using the compositions are also provided.

Ma, Shengqian↗
DOE OSTI2016

A morphology independent methodology for quantifying planview river change and characteristics from remotely sensed imagery

Remotely sensed imagery of rivers has long served as a means for characterizing channel properties and detection of planview change. In the last decade the dramatic increase in the availability of satellite imagery and processing tools has created the potential to greatly expand the spatial and temporal scale of our understanding of river morphology and dynamics. To date, the majority of GIS and automated analyses of planview changes in rivers from remotely sensed data has been developed for single-threaded meandering river systems. These methods have limited applicability to many of the earth's rivers with complex multi-channel planforms. Here we present the methodologies of a set of analysis algorithms collectively called Spatially Continuous Riverbank Erosion and Accretion Measurements (SCREAM). SCREAM analyzes planview river metrics regardless of river morphology. These algorithms quantify both the erosion and accretion rates of riverbanks from binary masks of channels generated from imagery acquired at two time periods. Additionally, the program quantifies the area of change between river channels and the surrounding floodplain and area of islands lost or formed between these two time periods. To examine variations in erosion rates in relation to local channel attributes and make rate comparisons between river systems of varying sizes, the program determines channel widths and bank curvature at every bank pixel. SCREAM was developed and tested on rivers with diverse and complex planform morphologies in imagery acquired from a range of observational platforms with varying spatial resolutions. Here, validation and verification of SCREAM-generated metrics against manual measurements show no significant measurement errors in determination of channel width, erosion, and bank aspects. SCREAM has the potential to provide data for both the quantitative examination of the controls on erosion rates and for the comparison of these rates across river systems ranging broadly in size and planform morphology.

47 OTHER INSTRUMENTATION↗
NASA NTRS1978

Elemental characteristics of aerosols emitted from a coal-fired heating plant

Size differentiated aerosols were collected downstream from a heating plant fueled with eastern coal and analyzed using particle induced X-ray emission technique. Based on aerosol masses collected in various size ranges, the aerosol size distribution is determined to be trimodal, with the three peaks centered at 0.54 microns, 4.0 microns, and 11.0 microns, respectively. Of the various trace elements present in the aerosols, sulphur is the only element that shows very strong concentration in the smallest size group. Iron is strongly concentrated in the 4.0 micron group. Potassium, calcium, and titanium also exhibit stronger concentration in the 4.0 micron group than any other group. Other trace elements - vanadium, chromium, manganese, nickel, copper, and barium - are equally divided between the 0.54 microns and the 4.0 microns groups. Apparently, all of the trace elements - except S - enter aerosols during the initial formation and subsequent condensation phases in the combustion process. Excess concentration of sulphur in the 0.54 microns group can only be accounted for by recondensation of sulphur vapors on the combustion aerosols and gas-to-particle phase conversion of sulfate vapors at the stack top.

Singh, J. J.↗
NASA NTRS1987

Centrifuge impact cratering experiments: Scaling laws for non-porous targets

A geotechnical centrifuge was used to investigate large body impacts onto planetary surfaces. At elevated gravity, it is possible to match various dimensionless similarity parameters which were shown to govern large scale impacts. Observations of crater growth and target flow fields have provided detailed and critical tests of a complete and unified scaling theory for impact cratering. Scaling estimates were determined for nonporous targets. Scaling estimates for large scale cratering in rock proposed previously by others have assumed that the crater radius is proportional to powers of the impactor energy and gravity, with no additional dependence on impact velocity. The size scaling laws determined from ongoing centrifuge experiments differ from earlier ones in three respects. First, a distinct dependence of impact velocity is recognized, even for constant impactor energy. Second, the present energy exponent for low porosity targets, like competent rock, is lower than earlier estimates. Third, the gravity exponent is recognized here as being related to both the energy and the velocity exponents.

Schmidt, Robert M.↗
NASA NTRS1972

The determination and optimization of (rutile) pigment particle size distributions

A light scattering particle size test which can be used with materials having a broad particle size distribution is described. This test is useful for pigments. The relation between the particle size distribution of a rutile pigment and its optical performance in a gray tint test at low pigment concentration is calculated and compared with experimental data.

Richards, L. W.↗
NASA NTRS1980

Determination of the complex refractive index and size distribution of atmospheric particulates from bistatic-monostatic lidar and solar radiometer measurements

A method is presented for inferring both the size distribution and the complex refractive index of atmospheric particulates from combined bistatic-monostatic lidar and solar radiometer observations. The basic input measurements are spectral optical depths at several visible and near-infrared wavelengths as obtained with a solar radiometer and backscatter and angular scatter coefficients as obtained from a biostatic-monostatic lidar. The spectral optical depth measurements obtained from the radiometer are mathematically inverted to infer a columnar particulate size distribution. Advantage is taken of the fact that the shape of the size distribution obtained by inverting the particulate optical depth is relatively insensitive to the particle refractive index assumed in the inversion. Bistatic-monostatic angular scatter and backscatter lidar data are then processed to extract an optimum value for the particle refractive index subject to the constraint that the shape of the particulate size distribution be the same as that inferred from the solar radiometer data. Specifically, the scattering parameters obtained from the bistatic-monostatic lidar data are compared with corresponding theoretical computations made for various assumed refractive index values. That value which yields best agreement, in a weighted least squares sense, is selected as the optimal refractive index estimate. The results of this procedure applied to a set of simulated measurements as well as to measurements collected on two separate days are presented and discussed.

Reagan, J. A.↗
NASA NTRS1985

Determination of Mineral Type, Abundance, and Grain Size with Remotely Obtained Reflectance Spectra

To derive the abundances of minerals in a surface composed of more then one mineral in an intimate mixture, the bidirectional reflectance spectrum must be measured at several angles of incidence and emission. From these measurements, the scattering parameters may be derived, and the effective single scattering albedo can be computed from the models. If the scattering parameters are not derived, and the particles scatter anisotropically, then the computed effective single scattering albedo has been computed, the solution to the model is a nonlinear least squares problem with three unknowns per particle type. The solution is feasible when the complex indices of refraction and the densities of each mineral component are known. The unknowns are: the grain size of each particle type, the mass fraction of each particle type, and a grain internal scattering coefficient that describes grain imperfections.

Clark, R. N.↗
NASA NTRS1975

Comparisons of ground-based monitor data with Pioneers 8, 9, 10 and 11 observations in 1968-1974

The paper examines ground-based neutron monitor data and the counting rates in different energy channels on the Pioneer 8, 9, 10 and 11 spacecraft to determine the scale size of the transient cosmic-ray variations (Forbush decreases) and the relationship of these variations to changes in the interplanetary magnetic field. Since the Pioneer spacecraft sampled the inner modulating region extensively, the spatial extent of Forbush decreases (Fd's) can be determined. In some cases the Fd modulating region was co-rotating and in others radially expanding. The azimuthal extent of the Fd region was variable but was typically about 45 deg in extent. These observations will be interpreted in terms of models proposed for Fds.

Lockwood, J. A.↗
NASA NTRS1970

Design problems of small turbomachinery

Advanced design and testing techniques developed at NASA Lewis to achieve high efficiency in small turbomachines are described. Small radial and axial turbines and compressors were built for space power systems and associated studies at the Lewis Research Center. A six stage axial compressor of 3.5 inches diameter and axial turbines of 5 and 8.5 inches diameter were included. Radial turbines and compressors ranged from 3.5 to 6 inches. Topics discussed include maximum efficiency as a function of speed, the effect of compressibility on passage size, the use of quasi-orthogonals to calculate cross-channel velocity gradients, a design point velocity diagram study for axial turbines, and estimating off-design performance. Special turbine instruments and calibration procedures were developed to test compressors and turbines, to determine Reynolds and size number effects clearance, specific speed effects, and compressor performance. Laboratory tests conducted to study system operation and shaft and bearing motions are also reviewed.

Rohlik, H. E.↗
NASA NTRS2009

Residual Stresses and Critical Initial Flaw Size Analyses of Welds

An independent assessment was conducted to determine the critical initial flaw size (CIFS) for the flange-to-skin weld in the Ares I-X Upper Stage Simulator (USS). A series of weld analyses are performed to determine the residual stresses in a critical region of the USS. Weld residual stresses both increase constraint and mean stress thereby having an important effect on the fatigue life. The purpose of the weld analyses was to model the weld process using a variety of sequences to determine the 'best' sequence in terms of weld residual stresses and distortions. The many factors examined in this study include weld design (single-V, double-V groove), weld sequence, boundary conditions, and material properties, among others. The results of this weld analysis are included with service loads to perform a fatigue and critical initial flaw size evaluation.

Brust, Frederick W.↗
DOE OSTI2021

Magnetic properties of the Shastry-Sutherland lattice material BaNd 2 ZnO 5

We investigate the physical properties of the Shastry-Sutherland lattice material BaNd 2 ZnO 5 . Neutron diffraction, magnetic susceptibility, and specific heat measurements reveal antiferromagnetic order below 1.65 K. The magnetic order is found to be a 2–Q magnetic structure with the magnetic moments lying in the Shastry-Sutherland lattice planes comprising the tetragonal crystal structure of BaNd 2 ZnO 5 . The ordered moment for this structure is 1.9(1) μB per Nd ion. Inelastic neutron scattering measurements reveal that the crystal field ground state doublet is well separated from the first excited state at 8 meV. The crystal field Hamiltonian is determined through simultaneous refinement of models with both the LS coupling and intermediate coupling approximations to the inelastic neutron scattering and magnetic susceptibility data. The ground state doublet indicates that the magnetic moments lie primarily in the basal plane with magnitude consistent with the size of the determined ordered moment.

36 MATERIALS SCIENCE↗