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All sourcesNASA NTRSDOE OSTI
NASA NTRS2009

Stability of Dosage Forms in the Pharmaceutical Payload Aboard Space Missions

Efficacious pharmaceuticals with adequate shelf lives are essential for successful space medical operations. Stability of pharmaceuticals, therefore, is of paramount importance for assuring the health and wellness of astronauts on future space exploration missions. Unique physical and environmental factors of space missions may contribute to the instability of pharmaceuticals, e.g., radiation, humidity and temperature variations. Degradation of pharmaceutical formulations can result in inadequate efficacy and/or untoward toxic effects, which could compromise astronaut safety and health. Methods: Four identical pharmaceutical payload kits containing 31 medications in different dosage forms (liquid, tablet, capsule, ointment and suppository) were transported to the International Space Station aboard the Space Shuttle (STS-121). One of the 4 kits was stored on the Shuttle and the other 3 were stored on the International Space Station (ISS) for return to Earth at 6-month interval aboard a pre-designated Shuttle flight for each kit. The kit stored on the Shuttle was returned to Earth aboard STS-121 and 2 kits from ISS were returned on STS 117 and STS-122. Results: Analysis of standard physical and chemical parameters of degradation was completed for pharmaceuticals returned by STS-121 after14 days, STS - 117 after11 months and STS 122 after 19 months storage aboard ISS. Analysis of all flight samples along with ground-based matching controls was completed and results were compiled. Conclusion: Evaluation of results from the shuttle (1) and ISS increments (2) indicate that the number of formulations degraded in space increased with duration of storage in space and was higher in space compared to their ground-based counterparts. Rate of degradation for some of the formulations tested was faster in space than on Earth. Additionally, some of the formulations included in the medical kits were unstable, more so in space than on the ground. These results indicate that the space flight environment may adversely affect the shelf life of pharmaceuticals aboard space missions.

Du, Brian J.↗
NASA NTRS2011

Changes in the High-Latitude Topside Ionospheric Vertical Electron-Density Profiles in Response to Solar-Wind Perturbations During Large Magnetic Storms

The latest results from an investigation to establish links between solar-wind and topside-ionospheric parameters will be presented including a case where high-latitude topside electron-density Ne(h) profiles indicated dramatic rapid changes in the scale height during the main phase of a large magnetic storm (Dst < -200 nT). These scale-height changes suggest a large heat input to the topside ionosphere at this time. The topside profiles were derived from ISIS-1 digital ionograms obtained from the NASA Space Physics Data Facility (SPDF) Coordinated Data Analysis Web (CDA Web). Solar-wind data obtained from the NASA OMNIWeb database indicated that the magnetic storm was due to a magnetic cloud. This event is one of several large magnetic storms being investigated during the interval from 1965 to 1984 when both solar-wind and digital topside ionograms, from either Alouette-2, ISIS-1, or ISIS-2, are potentially available.

Benson, Robert F.↗
NASA NTRS2019

High-Fidelity Multidisciplinary Sensitivity Analysis Framework for Multipoint Rotorcraft Optimization

A multidisciplinary, gradient-based sensitivity-analysis methodology is evaluated for optimization of rotorcraft configurations. The tightly coupled discipline models include physics-based fluid dynamics and rotorcraft comprehensive analysis. A discretely-consistent adjoint method accounts for sensitivities of the unsteady flow and unstructured, dynamic, over set grids, while sensitivities of structural responses to aerodynamic loads are computed using a complex-variable method. The methodology is applied to optimize the shape of UH-60A Blackhawk helicopter blades for hover and forward flight conditions. The objective of the multipoint design is to simultaneously increase the rotorcraft figure of merit in a hover flight and reduce the rotor power in a forward flight. Trimmed loose-coupling solutions for the baseline configuration are used to initiate the tight-coupling multidisciplinary analysis. Target thrust and rolling and pitching moments are enforced as optimization constraints. The optimized configuration improves the optimization metrics at both design points. The improved performance and all constraints are maintained over many revolutions beyond the optimization interval, satisfying the required flight conditions. Computational cost of the optimization cycle is assessed in a high-performance computing environment and found affordable for design of rotorcraft in general level-flight conditions.

Wang, Li↗
NASA NTRS1985

Analysis of low-altitude wind speed and direction shears

Horizontal wind profile measurements recorded at the NASA 150-Meter Ground Winds Tower Facility at the Kennedy Space Center, Fla., are analyzed to evaluate wind shears known to be hazardous to the ascent and descent of conventional aircraft and the Space Shuttle. Twenty 5-s intervals of high (between 10 and 18 m/s) and gale force (18 to 33 m/s) surface winds provided instantaneous recordings every 0.1 s per speed, direction, and tower level from 3-150 m. Mathematical (maximum, mean, standard deviation) and graphical (percentage frequency distribution) descriptions of absolute, positive, and negative speed and direction shears with altitude (six vertical layers) and along flight path (one horizontal distance) are presented as functions of the intensity categories and significant values.

Alexander, M. B.↗
DOE OSTI2022

Global soil profiles indicate depth-dependent soil carbon losses under a warmer climate

Soil organic carbon (SOC) changes under future climate warming are difficult to quantify in situ. Here we apply an innovative approach combining space-for-time substitution with meta-analysis to SOC measurements in 113,013 soil profiles across the globe to estimate the effect of future climate warming on steady-state SOC stocks. We find that SOC stock will reduce by 6.0 ± 1.6% (mean±95% confidence interval), 4.8 ± 2.3% and 1.3 ± 4.0% at 0–0.3, 0.3–1 and 1–2 m soil depths, respectively, under 1 °C air warming, with additional 4.2%, 2.2% and 1.4% losses per every additional 1 °C warming, respectively. The largest proportional SOC losses occur in boreal forests. Existing SOC level is the predominant determinant of the spatial variability of SOC changes with higher percentage losses in SOC-rich soils. Our work demonstrates that warming induces more proportional SOC losses in topsoil than in subsoil, particularly from high-latitudinal SOC-rich systems.

54 ENVIRONMENTAL SCIENCES↗
NASA NTRS1985

Remarks on the ATMAP Campaigns in November 1981 and May 1982 at Collm (52 Deg N, 15 Deg E)

The results given are based on daily nighttime L. F. wind measurements over Central Europe on three measuring paths at 179, 227, and 272 kHz. Absolute reflection height measurements were carried out for the first time in August 1982 so that values of the months of 1982 and 1983 have been taken for the campaigns in November 1981 and May 1982. The prevailing wind and the semidiurnal tidal wind components are calculated daily. Means of the month or means of parts of a month are formed for climatological investigations. A 24 hour analysis is not possible due to the very different reflection heights during the daytime and nighttime, even with measurements being carried out the whole ay long in the winter season. The critical examination of the choice of the measuring intervals selected is dependent on the visual angle. A wind ield change is observed over Central Europe very often around the 20th of November 1981 this wind field variation being in the core period and leading over to a more stable tidal wind.

Schminder, R.↗
NASA NTRS1990

Analysis of pressure-broadened ozone spectra in the 3 micron region

The Molecular Spectroscopy Lab at NASA-Langley has been involved in a long term effort to carefully characterize the infrared spectra of small molecules of atmospheric interest, including methane, water vapor, ozone, and their isotopic counterparts. High resolution gas phase infrared spectra are obtained using both a tunable diode laser system, and the McMath Fourier transform spectrometer at the Kitt Peak Solar Observatory. Spectra are obtained at various pressures and temperatures for pure gas samples, and for samples containing mixtures of the species of interest in nitrogen, oxygen, or air. From these spectra, using a nonlinear least squares fitting technique, spectral parameters of position, intensity, and half-width were determined for varying laboratory conditions that approximate atmospheric conditions experienced in remote sensing situations. These parameters are of interest in theoretical studies of these species, as well as in allowing more accurate interpretation of remote sensing data. The current work involves the analysis of a series of McMath FTIR spectra of ozone broadened by mixing with air, nitrogen, or oxygen. Each spectrum covers the region from 2396 to 4057/cm. Each vibrational band is analyzed by first diving its region into small intervals containing a few well isolated absorption lines of reasonable intensity. Each of these small intervals is fit by multiple iterations of the nonlinear least square program until residuals are minimized to a reasonable value which corresponds to the noise level of the measured spectrum. Intervals for the 3 nu(sub 3) ozone band in the region from 3000 to 3060 wavenumbers are being examined.

Prochaska, Eleanor S.↗
NASA NTRS1992

Viking 2 electron observations at Mars

An analysis of the electron mode sweeps made in Viking 2 above the ionosphere is presented. An observation of the electron energy spectrum over the range 0 to 78 eV was recorded in 1 s and observations were made at intervals of 4 or 8 s. The concentrations and temperatures were highly variable in the altitude range 14,000 to 9000 km. Evidence for two Maxwellian components were present in most of the records. The general trend of concentration and temperature for the predominant component was from 2/cu cm and 100,000 K at 15,600 km to 5/cu cm at 220,000 K and 900 km, in good agreement with the Mars 3 observations of Gringauz et al. (1974). The higher-temperature component was generally characterized by a temperature near 400,000 K and concentrations near 0.1/cu cm. The electron plasma pressures near 800 km were about a factor of 20 lower than those obtained from Viking 1, the difference being much greater than expected from the normal distribution around the stagnation point in the shocked solar wind.

Johnson, Francis S.↗
NASA NTRS2003

Toroidal wave frequency at L=6-10: AMPTE/CCE Observations and Comparison with Theoretical Model

Magnetospheric standing Alfven waves are guided along the ambient magnetic field and their frequency depends on the mass density of the plasma distributed along the field lines. These properties allow us to use Alfen waves to map time-dependent phenomena between space and ground and to estimate the mass density. In this paper we present a statistical study of the spatial variation of the fundamental frequency f(sub T1) of toroidal-mode standing Alfen waves in the L range from 6 to 10, where L indicates the maximum geocentric distance on the field line. The data used for this analysis are energetic particle flux anisotropy (proxy of transverse electric field) and magnetic field measurements from the Active Magnetospheric Particle Tracer Explorers Charge Composition Explorer (CCE) spacecraft. Using CCE data covering 4 years we obtained approximately 5000 20-min intervals containing a clear signature of toroidal waves. The median f(sub T1), is 6-10 mHz at L=7 and decreases to 4-8 mHz at L = . The frequency tends to be lower at noon than at midnight. The observed frequencies are compared with numerically derived frequencies using an empirical mass density model and a magnetic field model. We found a good agreement for 12-24 MLT but a large discrepancy near MLT= 3. This may indicate that the flux tubes at this local time are more heavily loaded than specified in the Gallagher et al. model.

Takahashi, Kazue↗
NASA NTRS2016

Bone Turnover Does Not Reflect Skeletal Aging in Older Hispanic Men with Type 2 Diabetes

The paradox of fragility fracture in the presence of non-osteoporotic bone mineral density in older patients with type 2 diabetes mellitus (DM2) makes it difficult to clinically predict fracture in this vulnerable group. Serum osteocalcin (OC), a marker of bone turnover, increases with normal skeletal aging indicating risk of fracture. However, OC has been reported to be lower in patients with DM2. An inverse association between higher glycated hemoglobin levels (HbA1c) and lower serum OC in older DM2 patients triggered discussions encouraging further investigation. A key question to be answered is whether changes in glucose metabolism is responsible for bone metabolic changes, ultimately leading to increased risk of fragility fractures in DM2 patients. While these studies were conducted among Caucasian and Asian populations, this has not been studied in Hispanic populations who suffer from a higher prevalence of DM2. The Cameron County Hispanic Cohort (CCHC) in Texas is a homogeneous Hispanic cohort known to have high prevalence of DM2 (30%). Our preliminary data from this cohort reported OC levels lower than the suggested threshold for fragility fracture in post-menopausal women. We further investigated whether bone turnover in older CCHC adults with DM2 show a normal pattern of skeletal aging. Samples and data were obtained from a nested cohort of 68 (21 men and 47 women) Hispanic older adults (≥50 years) who had a diagnosis of DM2. Given high prevalence of uncontrolled DM2 in this cohort, we divided population into two groups: i) poor DM2 control with HbA1c level ≥8 (48% men and 38% women) and ii) good DM2 control with HbA1c level <8). A crosssectional analysis documented associations between serum OC and age adjusted HbA1c levels. There was no direct association between age and OC concentrations in our study. Higher HbA1c was associated with lower serum OC in men (odds ratio -6.5, 95% confidence interval -12.7 to - 0.3, p < 0.04). No significant associations were identified in women. Bone turnover in older Hispanic men with DM2 in our study does not reflect normal pattern of skeletal aging. It is unclear why similar results were not identified in women. We will continue to follow this cohort to investigate longitudinal trend of changes of bone turnover and its relationship with HbA1c in both men and women of this cohort.

Rianon, N.↗
DOE OSTI2024

Analysis of differential scanning calorimetry data for aged plutonium

Differential scanning calorimetry data for samples of a 52 year old plutonium alloy with 3.3 at. % Ga that were heated beyond the melting point is analyzed using transition state theory to find activation energies for the δ to ε and ε to liquid phase transitions. A Bayesian statistical method involving a Gaussian process model is used to find mean values and confidence intervals for the activation energies. The activation energy for the δ to ε phase transition increases by 3.3 ± 3.8% per decade, relative to the case when all age related plutonium lattice point defects have been removed through annealing. The corresponding increase in activation energy for the ε to liquid transition is shown to be 7.1 ± 1.8% per decade. It is postulated that the change in activation energy with age for both phase transitions is caused, in part, by the accumulation of the same type of lattice point defects associated with the observed increase in elastic bulk modulus over time.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
NASA NTRS2000

RXTE and BATSE Observations of the Recent Outbursts of 2S 1417-624

25 1417-624 is a 57 mHz transient Be/X-ray pulsar system first discovered by SAS 3 in 1978. After the discovery outburst it was not seen again until 1994 when BATSE observed an outburst that peaked at 40 Srab (pulsed flux, 20-50 keV) and lasted 110 days, followed by a series of 5 shorter, 10-15 mCrab outbursts occurring every 42 days. Pulse timing analysis showed that these smaller outbursts began a few days after periastron passage of the system's eccentric, 42 day period orbit. Renewed activity from the source was detected by BATSE beginning in 1999 November. BATSE monitoring shows a 10 mCrab peak flux outburst lasting 10 days, followed in the next orbit by a 30 mCrab peak flux outburst, which to date has lasted 56 days. Regular monitoring with RXTE began during the 1999 November outburst and has continued in to the current outburst. The data provides good coverage of the low flux state between BATSE detections, which includes the periastron passage. Pulses are detected through this interval, showing that the source did not enter the propeller regime. The PCA monitoring from the lowest flux level, which occurs shortly before periastron, until the peak of the current outburst, show a continuous evolution of the pulse profile. These profiles contain a narrow notch feature which allow us to present a phase aligned history of this pulse evolution. We present a timing analysis of the PCA and BATSE observations that provide corrections to the binary orbit, and measurements of the torque during the observations. From the observed torque and flux we show that disc accretion is occurring in the current outburst, most probably was also occurring in the smaller outburst.

Finger, M. H.↗
NASA NTRS1998

Monitoring MRK 509: The Origin of the Reprocessor and Broad Band X-ray Spectrum of Narrow Line Seyfert 1 AKN 564

The ten monitoring observations of Mrk 509 were made successfully between October 20 and November 26 last year. These observations were simultaneously with RXTE observations. A preliminary analysis of the RXTE observations has been done, and the light curve is shown in figure 1. Our aim in this experiment is to determine the location of the emission region of the reflection component by reverberation mapping. This component could be emitted from the accretion disk, within 100 Scwartzschild radii (R(sub s)) from the source. Note that the monitoring interval of 2.5 days corresponds to 100 R(sub s) for a 2 x 10(exp 8) solar mass black hole, which may be appropriate for this luminous object. In that case, we would expect the reflected component to vary along the direct flux, and there should be no spectral variability between observations. Alternatively, the reflected emission could come from the molecular torus, several parsecs from the nucleus. In that case, the reflection component flux should not vary. The light curve in figure 1 shows that during the monitoring period, the target varied in an ideal way, since significant variability was observed between observations and yet the most rapid variability is apparently sampled. The analysis of this data is not yet completed. The measurement of the reflection component in the combined ASCa and RXTE spectra depends critically on the RXTE background subtraction and calibration, but these have not yet progressed to the point where the analysis can be done.

Halpern, Jules P.↗
NASA NTRS1994

Observed solar UV irradiance variations of importance to middle atmosphere energetics and photochemistry

Absorption of solar UV irradiance in the spectral interval 120-420 nm is chiefly responsible for radiative heating and photodissociation of important atmospheric constituents (e.g., O2, O3, H2O, NO2, etc.) in the stratosphere, mesosphere, and lower thermosphere. Thus, the absolute value and time perturbations of the UV irradiance could significantly affect the energetics, photochemistry, and subsequent dynamics of these regions. Analysis of preliminary data from the SOLSTICE (UARS) observations for a period of 244 days (3 Oct 1991-2 Jun 1992) is discussed in this paper. The data provide mean daily values of the spectral distribution of the observed irradiances at 1-nm resolution and their solar rotation and semirotation variations. The average amplitudes of the 27-day irradiance oscillations for the 244-day data period were 5.7% at Lyman-alpha (121 nm), 1% at 200 nm, 0.5% at 210 nm, and generally less than 0.2% at wavelengths longer than 280 nm. The average amplitudes of 13.5-day oscillations were, by and large, about half of these values. Solar irradiance variations at 10.7 cm are highly correlated with those at Ly-alpha and other chromospheric emission lines (r = 0.7 to 0.8) and only moderately correlated with irradiances at wavelengths of 180-208 nm (r = 0.5). The correlation decreases as the source region of the irradiance gets closer to the base of the photosphere. At the 2-nm interval 279-281 nm, however, which contains the cores of the Mg II h and k lines, the correlation is again approximately 0.8.

London, Julius↗
DOE OSTI2023

Topological Analysis of Temporal Hypergraphs

In this work we study the topological properties of temporal hypergraphs. Hypergraphs provide a higher dimensional generalization of a graph that is capable of capturing multi-way connections. As such, they have become an integral part of network science. A common use of hypergraphs is to model events as hyperedges in which the event can involve many elements as nodes. This provides a more complete picture of the event in comparison to the standard dyadic connection limitation of a graph. However, a common attribution to events is temporal information as an interval for when the event occurred. Consequently, a temporal hypergraph is born which accurately captures both the temporal information of events as well as their multi-way connections. Common tools for studying these temporal hypergraphs typically use summary statistics of snapshots from a sliding window procedure to capture changes in the underlying dynamics. However, these do not provide insight into how the changing structure of the hypergraph evolves and which components of the temporal hypergraph persist and are influential to the underlying system. To alleviate this need we leverage zigzag persistence from the field of Topological Data Analysis (TDA) to study the change in topological structure of time-evolving hypergraphs. We apply our pipeline to both a cyber security and social network dataset and show how the topological structure of their temporal hypergraphs change and can be used to understand the underlying dynamics.

hypergraphs, topological data analysis, zigzag per↗
DOE OSTI2023

Clear-sky detection for PV degradation analysis using multiple regression

A method is presented to detect clear-sky periods for plane-of-array irradiance time-averaged data that is based on the algorithm originally described by Reno and Hansen. Here we show this new method improves the state-of-the-art by providing accurate detection at longer data averaging intervals. Moreover, our new method detects clear periods in plane-of-array data, which is novel. The new method is developed by applying a Design of Experiment approach to optimize the parameters used in the Reno method, and Monte Carlo simulations are used to understand the robustness of the found parameters. Clear-sky detection accuracy is compared among four methods: the Reno method, the default clear-sky filter in RdTools, the Ellis method, and the method outlined in this work, using a hand-labeled two-year data set of 1-min plane-of-array irradiance for a fixed tilt system. The RdTools clear-sky filter is marred by excessive false positives. The other methods all perform well at 1-min data intervals; the method developed here provides more accurate detection at longer data averaging intervals. We show that the parameters are directly linked to the data frequency in the hope that these input variables may not have to be optimized for every data frequency and location. However, only a single fixed system in one location was carefully examined. Finally, we illustrate how accurate determination of clear-sky conditions helps to eliminate data noise and bias in the assessment of long-term performance of PV plants.

14 SOLAR ENERGY↗
DOE OSTI2025

Tracking cropland transitions: A comparative analysis of U.S. land cover change data

There are a growing number of land cover data available for the conterminous United States, supporting various applications ranging from biofuel regulatory decisions to habitat conservation assessments. These datasets vary in their source information, frequency of data collection and reporting, land class definitions, categorical detail, and spatial scale and time intervals of representation. These differences limit direct comparison, contribute to disagreements among studies, confuse stakeholders, and hamper our ability to confidently report key land cover trends in the U.S. Here we assess changes in cropland derived from the Land Change Monitoring, Assessment, and Projection (LCMAP) dataset from the U.S. Geological Survey and compare them with analyses of three established land cover datasets across the coterminous U.S. from 2008-2017: (1) the National Resources Inventory (NRI), (2) a dataset Lark et al. 2020 derived from the Cropland Data Layer (CDL), and (3) a dataset from Potapov et al. 2022. LCMAP reports more stable cropland and less stable noncropland in all comparisons, likely due to its more expansive definition of cropland which includes managed grasslands (pasture and hay). Despite these differences, net cropland expansion from all four datasets was comparable (5.18-6.33 million acres), although the geographic extent and type of conversion differed. LCMAP projected the largest cropland expansion in the southern Great Plains, whereas other datasets projected the largest expansion in the northwestern and central Midwest. Most of the pixel-level disagreements (86%) between LCMAP and Lark et al. 2020 were due to definitional differences among datasets, whereas the remainder (14%) were from a variety of causes. Cropland expansion in the LCMAP likely reflects conversions of more natural areas, whereas cropland expansion in other data sources also captures conversion of managed pasture to cropland. The particular research question considered (e.g., habitat versus soil carbon) should influence which data source is more appropriate.

60 APPLIED LIFE SCIENCES↗
NASA NTRS1992

The atmosphere of Neptune - An analysis of radio occultation data acquired with Voyager 2

The vertical structure of Neptune's atmosphere is studied on the basis of recordings of the tracking signals received from Voyager 2 during its occultation by Neptune. The measurements began at a planetographic latitude of 62 deg north and ended near 45 deg south, and cover an altitude interval of about 5000 km. The 1-bar isobaric surface has equatorial and polar radii of 24,766 +/-15 km and 24,342 +/-30 km, respectively, and a corresponding oblateness of 0.0171 +/-0.0014. At this pressure, the temperature was 72 +/-2 K. The tropopause was detected approximately 40 km above the 1-bar level at a pressure of about 100 mbar. A comparison with IR observations indicates that the gas at the tropopause consists of 78-84-percent hydrogen by number density with the rest being mostly helium. The temperature in this region was 52 +/-2 K.

Lindal, Gunnar F.↗