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NASA NTRS1983

Damage tolerance evaluation of adhesively laminated titanium

Basic damage tolerance properties of Ti-6A1-4V titanium plate can be improved by laminating thin sheets of titanium with adhesives. Compact tension and center cracked tension specimens made from thick plate, thin sheet, and laminated plate (six plies of thin sheet) were tested. The fracture toughness of the laminated plate was 39 percent higher than the monolithic plate. The laminated plate's through the thickness crack growth rate was about 20 percent less than that of the monolithic plate. The damage tolerance life of the surface cracked laminate was 6 to over 15 times the life of a monolithic specimen. A simple method of predicting crack growth in a crack ply of a laminate is presented. Previously announced in STAR as N82-33737

Johnson, W. S.↗

NASA NTRS1985

Rapid Adhesive Bonding for Metals and Composites

Toroidal induction heater is key element in rapid bonding technique. Rapid adhesive bonding equipment features toroid induction heater for quick bonding of composites and metals. Process avoids damaging composites that cannot withstand high temperatures for long time intervals. Process scaled up for production. Technique suited to bonding of end tabs onto material test specimens.

Stein, B. A.↗

NASA NTRS1983

Nonlinear viscoelastic characterization of structural adhesives

Measurements of the nonliner viscoelastic behavior of two adhesives, FM-73 and FM-300, are presented and discussed. Analytical methods to quantify the measurements are given and fitted into a framework of an accelerated testing and analysis procedure. The single integral model used is shown to function well and is analogous to a time-temperature stress-superposition procedure (TTSSP). Advantages and disadvantages of the creep power law method used in this study are given.

Rochefort, M. A.↗

NASA NTRS1983

Thermal stresses in bonded solar cells - The effect of the adhesive layer

A two-dimensional, rectangular model of a proposed solar cell structure is analyzed as two plate elements bonded with an elastic continuum. The governing equations are formulated using the principle of minimum potential energy, with displacement components that vary linearly through the thickness of the adhesive layer. An approximate solution is constructed for a particular class of material properties and is characterized by a boundary layer near the unloaded edge. Both interface stress components achieve their largest values at the edge, and the maximum shear stress is independent of the Young's Modulus of the substrate.

Williams, H. E.↗

NASA NTRS1984

Geometrically nonlinear analysis of adhesively bonded joints

A geometrically nonlinear finite element analysis of cohesive failure in typical joints is presented. Cracked-lap-shear joints were chosen for analysis. Results obtained from linear and nonlinear analysis show that nonlinear effects, due to large rotations, significantly affect the calculated mode 1, crack opening, and mode 2, inplane shear, strain-energy-release rates. The ratio of the mode 1 to mode 2 strain-energy-release rates (G1/G2) was found to be strongly affected by the adhesive modulus and the adherend thickness. The ratios between 0.2 and 0.8 can be obtained by varying adherend thickness and using either a single or double cracked-lap-shear specimen configuration. Debond growth rate data, together with the analysis, indicate that mode 1 strain-energy-release rate governs debond growth. Results from the present analysis agree well with experimentally measured joint opening displacements. Previously announced in STAR as N83-13497

Dattaguru, B.↗

NASA NTRS1986

Adhesive-Bonded Fixture for Flexure Testing

Fixture for flexural tests of glass-fiber-reinforced epoxy rods 1/4 in. (6.4 mm) in diameter easy to fabricate. Little machining done by relatively unskilled. Flexural-test fixture allows bending stress applied to specimen rod while holding rod securely. Dowel pins, blocks, and plate that make up fixture joined by adhesive.

Clemons, J. M.↗

NASA NTRS1984

Universal binding energy relations in metallic adhesion

Rose, Smith, and Ferrante have discovered scaling relations which map the adhesive binding energy calculated by Ferrante and Smith onto a single universal binding energy curve. These binding energies are calculated for all combinations of Al(111), Zn(0001), Mg(0001), and Na(110) in contact. The scaling involves normalizing the energy by the maximum binding energy and normalizing distances by a suitable combination of Thomas-Fermi screening lengths. Rose et al. have also found that the calculated cohesive energies of K, Ba, Cu, Mo, and Sm scale by similar simple relations, suggesting the universal relation may be more general than for the simple free electron metals for which it was derived. In addition, the scaling length was defined more generally in order to relate it to measurable physical properties. Further this universality can be extended to chemisorption. A simple and yet quite accurate prediction of a zero temperature equation of state (volume as a function of pressure for metals and alloys) is presented. Thermal expansion coefficients and melting temperatures are predicted by simple, analytic expressions, and results compare favorably with experiment for a broad range of metals.

Ferrante, J.↗

NASA NTRS1985

Molecular orbital studies in oxidation: Sulfate formation and metal-metal oxide adhesion

The chemical mechanisms for sulfate formation from sodium chloride and sulfur trioxide, which is a product of jet fuel combustion was determined. Molten sodium sulfate leads to hot corrosion of the protective oxide layers on turbine blades. How yttrium dopants in nidkel-aluminum alloys used in turbine blades reduce the spalling rate of protective alumina films and enhance their adhesion was also determined. Two other fulfate mechanisms were deduced and structure of carbon monoxide on a clean chronium and clean platinum-titanium alloys surfaces was determined. All studies were by use of the atom superposition and electron delocalization molecular orbital (ASED-MO) theory. Seven studies were completed. Their titles and abstracts are given.

Anderson, A. B.↗

NASA NTRS1984

Rapid adhesive bonding concepts for specimen and panel fabrication and field repair

The NASA Langley Research Center has developed bonding concepts for aerospace composite materials which employ induction heating to directly apply heat to the bond line and/or adherends without simultaneously heating the entire structure, supports, and fixtures of a bonding assembly. These methods have demonstrated bonding process time reductions of two to three orders of magnitude, by comparison with conventional press molding. Attention is presently given to rapid adhesive bonding for lap shear specimens for aerospace panel bonding or field repair, as well as for the field repair requirements of metallic and advanced polymeric matrix composite structures.

Stein, B. A.↗

NASA NTRS1985

Comparison of Bond in Roll-bonded and Adhesively Bonded Aluminums

Lap-shear and peel test measurements of bond strength have been carried out as part of an investigation of roll bonding of 2024 and 7075 aluminum alloys. Shear strengths of the bonded material in the F temper are in the range of 14 to 16 ksi. Corresponding peel strengths are 120 to 130 lb/inch. These values, which are three to five times those reported in the literature for adhesively bonded 2024 and 7075, are a result of the true metallurgical bond achieved. The effects of heat-treating the bonded material are described and the improvements in bond strength discussed relative to the shear strength of the parent material. The significance of the findings for aerospace applications is discussed.

Schwensfeir, R. J., Jr.↗

NASA NTRS1985

Use of Hydration Inhibitors to Improve Bond Durability of Aluminum Adhesive Joints

An investigation is conducted of the mechanisms by which nitrilotris methylene phosphonic acid (NTMP) and related compounds are adsorbed onto oxidized aluminum surfaces to inhibit hydration and increase the durability of adhesive bonds formed with inhibitor-treated panels. P - O - Al bonds are identified as the basis of adsorption, and it is found that water initially adsorbed onto the etched aluminum surfaces is displaced by the NTMP. The hydration of the NTMP-treated surfaces occurs in three stages, namely the reverisble physisorption of water, the slow dissolution of NTMP followed by rapid hydration of the freshly exposed Al2O3 to AlOOH and further hydration of the surface to Al(OH)3. Five properties of an ideal inhibitor are identified.

Davis, G. D.↗

NASA NTRS1985

Evaluation of a high temperature adhesive for fabricating graphite/PMR-15 polyimide structures

Tests are conducted to measure shear strength, shear modulus and flatwise tensile strength of the A7F (amide-imide modified LARC-13) adhesive system. An investigation is also conducted to determine the effect of geometric material parameters, and elevated temperature on the static strength of standard joints. Single-lap and double-lap composite joints, and single, double and step lap composite to metal joints are characterized. A series of advanced joints consisting of preformed adherends, adherends with scalloped edges and joints with hybrid interface plies are tested and compared to baseline single and double-lap designs.

Hill, S. G.↗

NASA NTRS1985

Mixed-mode cyclic debonding of adhesively bonded composite joints

A combined experimental-analytical investigation to characterize the cyclic failure mechanism of a simple composite-to-composite bonded joint is conducted. The cracked lap shear (CLS) specimens of graphite/epoxy adherend bonded with EC-3445 adhesive are tested under combined mode 1 and 2 loading. In all specimens tested, fatigue failure occurs in the form of cyclic debonding. The cyclic debond growth rates are measured. The finite element analysis is employed to compute the mode 1, mode 2, and total strain energy release rates (i.e., GI, GII, and GT). A wide range of mixed-mode loading, i.e., GI/GII ranging from 0.03 to 0.38, is obtained. The total strain energy release rate, G sub T, appeared to be the driving parameter for cyclic debonding in the tested composite bonded system.

Rezaizadeh, M. A.↗

NASA NTRS1986

Method for the production of strongly adhesive films on titanium and titanium alloys with a metallization process

A process for the spray-application of a strongly adhesive, thick antifriction layer on titanium and titanium alloys is proposed. The titanium/titanium alloy component to be coated is first subjected to cleaning in a pickling bath with reducing additives and sand-blasting, then coated with an intermediate layer of nickel, after which the final layer is applied. The formation of TiNi at the interface ensures strong bonding of the antifriction layer.

Hahn, H. J.↗

NASA NTRS1985

Fracto-emission from the peeling of pressure sensitive adhesives

The electron emission, positive ion emission, photon emission, and long wavelength electromagnetic radiation accompanying the peeling of pressure sensitive adhesives in vacuum are examined. These results are interpreted in terms of a previously presented model involving fracture-induced microdischarges which excite the fracture surfaces by particle bombardment.

Dickinson, J. T.↗

NASA NTRS1985

Photon and radiowave emission from peeling pressure sensitive adhesives in air

During separation of an adhesive from a polymer substrate in air, intense bursts of photons ('phE', for photon emission) and long wavelength electromagnetic radiation ('RE', for radiowave emission), similar to those reported earlier by Deryagin, et al. (1978) have been observed. In this paper, careful measurements of the phE time distributions, as well as time correlations between bursts of phE and RE, are reported. These results support the view that patches of electrical charge produced by charge separation between dissimilar materials lead to microdischarges in and near the crack tip. The role of these discharges in producing sustained phE after the discharge has been extinguished is also discussed.

Donaldson, E. E.↗

NASA NTRS1984

Viscoelastic modelling of epoxy-resins for adhesive and composite applications

Nonlinear viscoelastic and thermoelastic characterization procedures were applied to a rubber toughened adhesive that is commercially available as FM-300. Long time (accelerated testing) predictions on the basis of stress-time-superposition and time-temperature-superposition were compared with actual long term data. Good verification was obtained.

Hiel, C.↗

NASA NTRS1984

The application of thermodynamic and spectroscopic techniques to adhesion in the polyimide/Ti 6-4 and polyphenylquinoxaline/Ti 6-4 systems

The results of calorimetric measurements of Ti adherend surfaces are presented. The measurements were carried out after several chemical pretreatments and after fracture of several lap shear samples aged at high temperature. The exact composition of the Ti samples was Ti(6 percent Al-4 percent V). The adhesives used were polyimides and polyphenylquinoxalines (PPQ). Each chemical pretreatment was accompanied by a unique spectroscopic feature which was characterized by XPS, SEM, and specular reflectance infrared spectroscopy. The energetics of the interaction between primer solutions and the Ti adherend were evaluated by microcalorimetry. Changes in the structure of the surface oxide layer upon heating of the adherend were deduced from immersion temperatures of the PI and PPQ solutions. The XPS and SEM data are given is a table.

Dias, S.↗