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At least 901 records · Page 50

Absorbed Dose Determination Using Experimental and Analytical Predictions of X-Ray Spectra

Electron beam welding in a vacuum is a technology that NASA is investigating as a joining technique for manufacture of space structures. This investigation characterizes the x-ray environment due to operation of an in-vacuum electron beam welding tool and provides recommendations for adequate shielding for astronauts performing the in-vacuum electron beam welding. NASA, in a joint venture with the Russian Space Agency, was scheduled to perform a series of welding in space experiments on board the U.S. Space Shuttle. This series of experiments was named the international space welding experiment (ISWE). The hardware associated with the ISWE was leased to NASA by the Paton Welding Institute (PWI) in Ukraine for ground-based welding experiments in preparation for flight. Two ground tests were scheduled, using the ISWE electron beam welding tool, to characterize the radiation exposure to an astronaut during the operation of the ISWE. These radiation exposure tests used thermoluminescence dosimeters (TLD's) shielded with material currently used by astronauts during extravehicular activities to measure the radiation dose. The TLD's were exposed to x-ray radiation generated by operation of the ISWE in-vacuum electron beam welding tool. This investigation was the first known application of TLD's to measure absorbed dose from x rays of energy less than 10 keV. The ISWE hardware was returned to Ukraine before the issue of adequate shielding for the astronauts was completely verified. Therefore, alternate experimental and analytical methods were developed to measure and predict the x-ray spectral and intensity distribution generated by ISWE electron beam impact with metal. These x-ray spectra were normalized to an equivalent ISWE exposure, then used to calculate the absorbed radiation dose to astronauts. These absorbed dose values were compared to TLD measurements obtained during actual operation of the ISWE in-vacuum electron beam welding tool. The calculated absorbed dose values were found to be in agreement with the measured TLD values.

Edwards, D. L.↗

New high-throughput endstation to accelerate the experimental optimization pipeline for synchrotron X-ray footprinting

Synchrotron X-ray footprinting (XF) is a growing structural biology technique that leverages radiation-induced chemical modifications via X-ray radiolysis of water to produce hydroxyl radicals that probe changes in macromolecular structure and dynamics in solution states of interest. The X-ray Footprinting of Biological Materials (XFP) beamline at the National Synchrotron Light Source II provides the structural biology community with access to instrumentation and expert support in the XF method, and is also a platform for development of new technological capabilities in this field. Hee, the design and implementation of a new high-throughput endstation device based around use of a 96-well PCR plate form factor and supporting diagnostic instrumentation for synchrotron XF is described. This development enables a pipeline for rapid comprehensive screening of the influence of sample chemistry on hydroxyl radical dose using a convenient fluorescent assay, illustrated here with a study of 26 organic compounds. The new high-throughput endstation device and sample evaluation pipeline now available at the XFP beamline provide the worldwide structural biology community with a robust resource for carrying out well optimized synchrotron XF studies of challenging biological systems with complex sample compositions.

38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEA↗

Differences Between ERBE and CERES Tropical Means Fluxes: ENSO, Climate Change of Calibration?

Verner E. Soumi was the father of radiation budget measurements from space. He directed the team at the University of Wisconsin that developed the first radiation budget measurements on the Iota (Explorer VII) coverage) spacecraft in 1959. The first data published was from hand calculations of night-time long-wave fluxes, with absolute accuracy estimated as better than 10 percent, and the data shown as hand drawn maps with lines of equal "long-wave radiation loss, in Langleys per minute X 10(exp -3) (isolangleys)". The first comparisons of the new radiation data with nephanalyses showed that clouds dominated the radiation patterns. Soumi immediately proposed using the radiation fields to help understand the atmospheric heat sources necessary to drive the atmospheric circulation. This early work already pointed to the relationship between the outgoing longwave radiation at the top of the atmosphere and the vertical flux divergence of infrared radiation within the atmosphere. In the next 30 years, global satellite observations of the radiation balance of the planet have advanced both in accuracy, stability, and in their ability to address cause and effect in the climate system. The purpose of the present paper is to examine early results of the new Clouds and the Earth's Radiant Energy System (CERES) data on Tropical Rainfall Measuring System (TRMM) which started data collection in January, 1998. CERES is a direct descendant of the legacy of Soumi's foresight on understanding the global energetics using satellite observations of broadband radiation.

Wielicki, Bruce A.↗

Differences between ERBE and CERES Tropical Mean Fluxes: ENSO, Climate Change or Calibration?

Verner E. Soumi was the father of radiation budget measurements from space. He directed the team at the University of Wisconsin that developed the first radiation budget measurements on the Iota (Explorer VII) coverage) spacecraft in 1959. The first data published was from hand calculations of night-time long-wave fluxes, with absolute accuracy estimated as better than 10 percent, and the data shown as hand drawn maps with lines of equal "long-wave radiation loss, in Langleys per minute X 10(exp -3) (isolangleys)". The first comparisons of the new radiation data with nephanalyses showed that clouds dominated the radiation patterns. Soumi immediately proposed using the radiation fields to help understand the atmospheric heat sources necessary to drive the atmospheric circulation. This early work already pointed to the relationship between the outgoing longwave radiation at the top of the atmosphere and the vertical flux divergence of infrared radiation within the atmosphere. In the next 30 years, global satellite observations of the radiation balance of the planet have advanced both in accuracy, stability, and in their ability to address cause and effect in the climate system. The purpose of the present paper is to examine early results of the new Clouds and the Earth's Radiant Energy System (CERES) data on Tropical Rainfall Measuring System (TRMM) which started data collection in January, 1998. CERES is a direct descendant of the legacy of Soumi's foresight on understanding the global energetics using satellite observations of broadband radiation.

Wielicki, Bruce A.↗

Temporal Variations of Strength and Location of the South Atlantic Anomaly as Measured by RXTE

The evolution of the particle background at an altitude of approx.540km during the time interval between 1996 and 2007 is studied using the particle monitor of the High Energy X-ray Timing Experiment on board NASA's Rossi X-ray Timing Explorer. A special emphasis of this study is the location and strength of the South Atlantic Anomaly (SAA). The size and strength of the SAA are anti-correlated with the the 10.7 cm radio flux of the Sun, which leads the SAA strength by approx.1 year reflecting variations in solar heating of the upper atmosphere. The location of the SAA is also found to drift westwards with an average drift rate of about 0.3deg/yr following the drift of the geomagnetic field configuration. Superimposed to this drift rate are irregularities, where the SAA suddenly moves eastwards and where furthermore the speed of the drift changes. The most prominent of these irregularities is found in the second quarter of 2003 and another event took place in 1999. We suggest that these events are previously unrecognized manifestations of the geomagnetic jerks of the Earth's magnetic field. Key words: space radiation environment, South Atlantic Anomaly, radiation monitors, Rossi X-ray Timing Explorer

Wilms, Jorn↗

X-Raying the Beating Heart of a Newborn Star: Rotational Modulation of High-Energy Radiation from V1647 Ori

We report a periodicity of approx.1 day in the highly elevated X-ray emission from the protostar V1647 Ori during its two recent multiple-year outbursts of mass accretion. This periodicity is indicative of protostellar rotation at near-breakup speed. Modeling of the phased X-ray light curve indicates the high-temperature ( 50 MK), X-ray-emitting plasma, which is most likely heated by accretion-induced magnetic reconnection, resides in dense ( 5 1010 cm.3), pancake-shaped magnetic footprints where the accretion stream feeds the newborn star. The sustained X-ray periodicity of V1647 Ori demonstrates that such protostellar magnetospheric accretion configurations can be stable over timescales of years. Subject headings: stars: formation stars: individual (V1647 Ori) stars: pre-main sequence X-rays: stars

Hamaguchi, Kenji↗

Global Energetics of Several Large Solar Eruptive Events

We have evaluated the energetics of 38 solar eruptive events observed by a variety of spacecraft instruments between February 2002 and December 2006, as accurately as the observations allow. The measured energetic components include: (1) the radiated energy in the GOES 1 { 8 A band; (2) the total energy radiated from the soft X-ray (SXR) emitting plasma; (3) the peak energy in the SXR-emitting plasma; (4) the bolometric radiated energy over the full duration of the event; (5) the energy in are-accelerated electrons above 20 keV and in ions above 1 MeV; (6) the kinetic and potential energies of the coronal mass ejection (CME); (7) the energy in solar energetic particles (SEPs); and (8) the amount of free (nonpotential) magnetic energy estimated to be available in the pertinent active region. Major conclusions include: (1) the energy radiated by the SXR-emitting plasma exceeds, by about half an order of magnitude, the peak energy content of the thermal plasma that produces this radiation; (2) the energy content in are-accelerated electrons and ions is sufficient to supply the bolometric energy radiated across all wavelengths throughout the event; (3) the energy contents of are-accelerated electrons and ions are comparable; (4) the energy in SEPs is typically a few percent of the CME kinetic energy (measured in the rest frame of the solar wind); and (5) the available magnetic energy is sufficient to power the CME, the are-accelerated particles, and the hot thermal plasma.

Emslie, A. G.↗

A variable X-ray chopper system for phase-sensitive detection in synchrotron X-ray scanning tunneling microscopy

An ultra-high-vacuum compatible X-ray chopper system has been designed, constructed and integrated into the XTIP beamline at the Advanced Photon Source at Argonne National Laboratory. The XTIP beamline can operate at soft X-ray energies from 400 eV to 1900 eV while providing a focused beam down to about 10 µm × 10 µm into the synchrotron X-ray scanning tunneling microscopy (SX-STM) endstation instrument. The X-ray chopper is a critical component for separating topographic information from chemical information in SX-STM through phase-sensitive current detection. Depending on the experimental needs, the modulation frequency can be controlled from 100 Hz to 10 kHz. In addition, the chopper system is fully bakeable and can achieve a base pressure of 10 -10 mbar. Facilities for active water cooling have been designed, but passive cooling through copper braids has been shown to be sufficient at standard chopping frequencies. Using an Fe/Al 2 O 3 /CoAl(111) sample, the separation of the SX-STM current into a chemical component and a stable feedback signal is demonstrated.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

Soft X-ray production by photon scattering in pulsating binary neutron star sources

A new mechanism is proposed as a source of soft (less than 1 keV) radiation in binary pulsating X-ray sources, in the form of photon scattering which leaves the electron in an excited Landau level. In a plasma with parameters typical of such sources, the low-energy X-ray emissivity of this mechanism far exceeds that of bremsstrahlung. This copious source of soft photons is quite adequate to provide the seed photons needed to explain the power-law hard X-ray spectrum by inverse Comptonization on the hot electrons at the base of the accretion column.

Bussard, R. W.↗

The shadow wind in high-mass X-ray binaries

We present hydrodynamic simulations of the most X-ray luminous high-mass X-ray binary systems, such as Cen X-3 and SMC X-1. These models illustrate the presence of both a normal radiatively driven wind confined to the X-ray shadow of the primary star -- a shadow wind -- and a thermally driven wind excited by the X-ray heating of the primary's stellar surface -- an X-ray-excited wind. The X-ray flux in these systems is sufficiently intense that any circumstellar gas exposed to the X-ray source will be highly photoionized. These extreme ionization conditions prevent the formation of a normal radiatively driven wind from the irradiated surface of the primary, but such a wind can still form on the shadowed side of the primary. Orbital rotation can then bring this shadow wind into the line of sight toward the X-ray source, enhancing the column density of the wind seen near eclipse egress. Furthermore, such a high X-ray flux can also excite a thermal wind from the irradiated surface of the primary. Again, orbital rotation tends to deflect the wind, this time leading to an enhanced column density near eclipse ingress.

Blondin, John M.↗

Mapping 3D grain and precipitate structure during in situ mechanical testing of open-cell metal foam using micro-computed tomography and high-energy X-ray diffraction microscopy

Open-cell metal foams are ultra-low-density cellular metals with complex hierarchical structures that span bulk, cell, ligament, and sub-ligament scales and give rise to desirable properties such as high strength-to-weight ratio and excellent energy absorption. Although literature suggests that intrinsic material structures at sub-ligament length scales (e.g., grains and precipitates) play an important role in mechanical behavior of open-cell metal foams, there are very few experimental measurements of such structures in three dimensions and for meaningful volumes of foam. This study seeks to map and track the three-dimensional (3D) grain and precipitate structures of an intact volume of open-cell aluminum foam by advancing microstructural characterization techniques that leverage X-ray micro-computed tomography (μCT) and far-field high-energy X-ray diffraction microscopy (FF-HEDM). A 6%-relative-density aluminum foam sample was mechanically tested in compression while μCT and FF-HEDM measurements were collected at interrupted loading states at beamline 1-ID of the Advanced Photon Source. Further, a new scanning strategy and reconstruction algorithm were established to enable characterization of a foam volume with diameter approximately four times wider than the nominal width of the X-ray beam. The result is a set of maps that detail both the 3D grain and precipitate structures throughout the foam volume at successive strain steps. A novel grain tracking procedure was developed to track individual grains within the foam volume by accounting for the large rigid-body motions that individual ligaments can undergo during mechanical loading. The ability to track grains and precipitate structures in three dimensions throughout large bulk deformation of ultra-low-density polycrystalline materials enables new possibilities for validating numerical models and investigating local failure mechanisms. Furthermore, the methods and procedures developed in this study could be applied to other ultra-low-density structures, such as additively manufactured lattices.

36 MATERIALS SCIENCE↗

Role of Small-Scale Impulsive Events in Heating the X-Ray Bright Points of the Quiet Sun

Small-scale impulsive events, known as nanoflares, are thought to be one of the prime candidates that can keep the solar corona hot at its multimillion-Kelvin temperature. Individual nanoflares are difficult to detect with the current generation of instruments; however, their presence can be inferred through indirect techniques such as Differential Emission Measure (DEM) analysis. Here, we employ this technique to investigate the possibility of nanoflare heating of the quiet corona during the minimum of solar cycle 24. We estimate the DEM of disk-integrated quiet Sun and X-ray bright points (XBP) using the observations from XSM on board the Chandrayaan-2 orbiter and AIA on board the Solar Dynamic Observatory. XBPs are found to be the dominant contributor to disk-integrated X-rays, with a radiative flux of ∼2 × 10 5 erg cm −2 s −1 . XBPs consist of small-scale loops associated with bipolar magnetic fields. We simulate such XBP loops using the EBTEL hydrodynamic code. The lengths and magnetic field strengths of these loops are obtained through a potential field extrapolation of the photospheric magnetogram. Each loop is assumed to be heated by random nanoflares having an energy that depends on the loop properties. The composite nanoflare energy distribution for all the loops has a power-law slope close to −2.5. The simulation output is then used to obtain the integrated DEM. It agrees remarkably well with the observed DEM at temperatures above 1 MK, suggesting that the nanoflare distribution, as predicted by our model, can explain the XBP heating.

Solar coronal heating↗

Dark field X-ray microscopy below liquid-helium temperature: The case of NaMnO 2

Dark field X-ray microscopy (DFXM) is an experimental technique employed to investigate material properties by probing their ‘mesoscale,’ or microscale structures, in a bulk-sensitive manner using hard X-rays at synchrotron radiation sources. However, challenges remain when it comes to applications of this technique to examine low-temperature phenomena in quantum materials, which exhibit complex phase transitions at cryogenic temperatures. One such material is NaMnO 2 , which hosts an antiferromagnetic transition at 45 K that is suspected to coincide with local structural transitions from its majority monoclinic phase to nanoscale triclinic domains. Direct observation of local heterogeneities and this effect at low temperatures in NaMnO 2 is an important step in understanding this material and serves as an ideal candidate study for expanding the DFXM experimental design space. This paper details a foundational high-resolution DFXM study, down to liquid-helium temperature and below, conducted to explore phase transitions in NaMnO 2 . In conclusion, the outlined experiment ushers in the evaluation of other functional materials at low temperatures using this technique.

36 MATERIALS SCIENCE↗

Emergence of complex-regular eutectic patterns in Al–Ge: Observations from correlative nano-imaging

Eutectic solidification exemplifies nonequilibrium pattern formation, making it a well-studied moving boundary problem. Yet the mechanisms behind the formation of complex-regular microstructures – particularly in highly anisotropic systems with a significant volume fraction of a faceted phase – remain poorly understood. Our understanding of such systems is made complicated by the nonlinear interface kinetics and unique growth dynamics characteristic of faceted phases. To address these challenges, we investigate a model Al–Ge eutectic system, where the faceted Ge phase constitutes a substantial volume fraction (~0.35) and where the two solid phases arrange into so-called “fishbone” or “feather” complex-regular patterns. Using synchrotron-based x-ray nano-imaging and nanotomography with high spatial resolution (22 nm per pixel), we capture in real-time the evolution of the solid–liquid interfaces and the resulting three-dimensional microstructures in this faceted/non-faceted eutectic system. By integrating these observations with electron backscattered diffraction, we elucidate the crystallographic biases on the solidification process and the mechanisms driving the formation of such complex-regular microstructures. These findings inform a new growth model for irregular eutectics in (near-)symmetrical phase diagrams, offering insight on advanced microstructural design and processing strategies. More broadly, we demonstrate how interfacial curvature is generated in irregular eutectic alloys and how it depends on the volume fraction of the faceted phase.

36 MATERIALS SCIENCE↗

NuSTAR Measurement of the Cosmic X-ray Background in the 3–20 keV Energy Band

We present measurements of the intensity of the cosmic X-ray background (CXB) with the Nuclear Spectroscopic Telescope Array (NuSTAR) telescope in the 3–20 keV energy range. Our method uses spatial modulation of the CXB signal on the NuSTAR detectors through the telescope’s side aperture. Based on the NuSTAR observations of selected extragalactic fields with a total exposure of 7 Ms, we have estimated the CXB 3–20 keV flux to be 2.8×10−11erg s−1cm−2deg−2, which is∼8 per cent higher than that measured withHEAO-1and consistent with the INTEGRAL measurement. The inferred CXB spectral shape in the3–20 keV energy band is consistent with the canonical model of Gruber et al. We demonstrate that the spatially modulated CXB signal measured by NuSTAR is not contaminated by systematic noise and is limited by photon statistics. The measured relative scatter of the CXB intensity between different sky directions is compatible with cosmic variance, which opens new possibilities for studying CXB anisotropy over the whole sky with NuSTAR.

Detectors↗

Solid State Studies of the Radiation Histosy of Lunar Samples

Particle track densities up to greater than 3 x 10(exp 9) per square centimeter have been measured in different samples. Rocks 17, 47, 57, and 58 have VH (Z greater than 22) galactic cosmic ray ages of 11, 14, 28, and 13 x 10(exp 6) years, respectively. Rock 57 has a calculated erosion rate of approximately less than 10(exp -7) centimeter per year. Near-surface track versus depth data in rock 17 can be fit with solar flare particles that have a differential energy spectrum alpha E(exp -s); lunar samples can be used to study the history of solar activity. The uranium in the crystalline rocks occurs principally in small regions less than 10 to approximately equal to 100 micrometers in size. The (low) thermoluminescence of the fines increases with depth in core 10004. With one possible exception, x-ray studies have not shown pronounced radiation damage effects. The total energy release upon heating is small up to 900 C and occurs in three broad regions.

Crozaz, G.↗

The 18–19 March 2022 Series of 3He-Rich Events Observed By Solar Orbiter at 0.36 Au Compared With EUV, X-Ray, and Radio Observations

Context. During the first close perihelion pass of Solar Orbiter, a series of impulsive 3He-rich solar particle events was observed on 18–19 March 2022 from a distance of 0.36 au. In addition to the energetic particle, radio, and X-ray data from Solar Orbiter, the events were observed in radio and/or extreme ultraviolet by STEREO-A, SDO, Wind, and Parker Solar Probe. Aims. Observations of the event series along with remote sensing of flaring and radio emission with only small timing delays due to the close distance allow the association with energetic particles to be determined with much higher accuracy than previously possible from 1 au. Methods. By comparing the onsets of type-III bursts with the arrival of electrons of tens of keV at Solar Orbiter only a few minutes later, it can be seen that, overall, each of the more intense type-III bursts was associated with an electron and ion injection. Extreme ultraviolet data show that the times of the type-III bursts coincide with emission from a small (approximately Earth-sized) loop to the west of a nearby active region. Results. The energetic particle spectra and abundances show typical properties of impulsive 3He-rich flares and, when combined with the remote sensing observations, establish that the particle-accelerating mechanism in this series of events operates near the solar surface in association with magnetic loops, and in the absence of other phenomena such as jets and small coronal mass ejections.

acceleration of particles↗