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Aluminum-clad Spent Nuclear Fuel Engineering Scale Drying Experiment Design

The purpose of this document is to provide the technical specifications for the Engineering Scale Design for the drying tests of aluminum-clad spent nuclear fuel (ASNF). The engineering scale design is to accommodate both forced helium drying (FHD) as well as vacuum drying. The experiments will employ mock ASNF assemblies with a limited number of chemically treated aluminum plates to simulate the aluminum hydroxides found on ASNF. The goal here is to understand the transformation that may occur in plates including the loss of chemisorbed water and changes in morphology. Physiosorbed and bulk water found in experiments will be dried in the process and the effect on drying operations noted. Decay heat will be simulated in one assembly using a custom designed resistance heating element. A typical radial arrangement of assemblies will be employed using a modified Type 1A Basket design. For the chamber/canister, a single assembly layer with full radial dimension will be employed. Modifications to the standard canister design and configuration include the addition of a siphon tube to enable recirculation of hot gas for forced helium drying. A ring of ports/flanges are added near the top of the chamber to accommodate the feedthroughs for instrumentation and power needed for the experiment and data collection. Four viewports are added to the main section of the chamber with two in line with one of the fuel assembly and siphon tube. The other two viewports are on the opposite side of the chamber. The purpose here is to provide the option of thermal imaging in addition to the nearly four dozen thermocouples available inside the chamber. Modeling of the chamber, basket, and mock ASNF assemblies was conducted to estimate temperature distributions throughout the chamber during forced helium drying and over the anticipated drying period. This modeling was used as input to decisions on the Engineering Scale Design. Work on modeling continues in the period during setup and testing to develop preliminary drying models. Analysis of experimental results will later be used to validate these and subsequent models.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

AGR-1, AGR-2 and AGR-3/4 Release-to-Birth Ratio Data Analysis

A series of Advanced Gas Reactor (AGR) irradiation tests is being conducted in the Advanced Test Reactor at Idaho National Laboratory in support of development and qualification of tristructural isotropic (TRISO) low enriched fuel used in the High Temperature Gas-cooled Reactor (HTGR). Each AGR test consists of multiple independently controlled and monitored capsules containing fuel compacts placed in a graphite cylinder shrouded by a steel shell. These capsules are instrumented with thermocouples embedded in the graphite enabling temperature control. AGR configuration and irradiation conditions are based on prismatic HTGR technology distinguished primarily by the use of helium coolant, a low-power-density ceramic core capable of withstanding very high temperatures, and TRISO coated particle fuel. Thus, these tests provide valuable irradiation performance data to support fuel process development, qualify fuel for normal operating conditions, and support development and validation of fuel performance and fission product transport models and codes. The release-rate-to-birth-rate ratio (R/B) for each of fission product isotopes (i.e., krypton and xenon) is calculated from release rates in the sweep gas flow measured by the germanium detectors used in the AGR Fission Product Monitoring (FPM) System installed downstream from each irradiated capsule. Birth rates are calculated based on the fission power in the experiment and fission product generation models. Thus, this R/B is a measure of the ability of fuel kernel, particle coating layers, and compact matrix to retain fission gas atoms preventing their release into the sweep gas flow, especially in the event of particle coating failures that occurred during AGR-2 and AGR-3/4 irradiations. The major factors that govern gaseous radioactive decay, diffusion, and release processes are found to be material diffusion coefficient, temperature, and isotopic decay constant. For each of all AGR capsules, ABAQUS-based three-dimensional finite-element thermal models are created to predict daily averages of fuel compact temperatures for the entire irradiation period, which are used in establishing the R/B correlation with temperature and decay constant. This correlation can be used by reactor designers to estimate fission gas release from postulated failed fuel particles in HTGR cores, which is the key safety factor for fuel performance assessment.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Technical Evaluation Report for the NDMAS AGR-5/6/7 TRISO Irradiation Monitoring System

The Nuclear Data Management and Analysis System (NDMAS) manages irradiation experiment data collected under the Advanced Gas Reactor (AGR) Fuel Development and Qualification program within the Advanced Reactor Technologies Technology Development Office. The AGR-5/6/7 irradiation experiment combines the fifth, sixth, and seventh planned irradiation campaigns of the U.S. Department of Energy AGR Fuel Development and Qualification Program. These combined irradiation tests will consist of fuel qualification tests (AGR-5/6) and a margin test (AGR-7) for the industrially produced uranium oxycarbide (UCO) tristructural isotropic (TRISO) coated particle fuel developed by the AGR program. The objective of the AGR-5/6/7 irradiation experiment is to establish the performance of UCO TRISO fuel fabricated using engineering-scale equipment in a production environment under and beyond normal operating conditions (PNL-5245). Experimental irradiation measurements for this experiment (i.e., thermocouple temperature, gas flow rate, fission product release rate, gross gamma count, and Advanced Test Reactor (ATR) operational parameters) are captured automatically to the NDMAS database. Data derived from numerical simulation or other mathematical analyses (i.e., fast fluence, burnup, temperature, and fission product release to birth ratio) are captured to the database when provided by the researchers. The NDMAS database is a relational database accessed via structured query language and managed with Microsoft SQL Server. While select users can directly access the database, that is not the most convenient way to interact with the data. The NDMAS team constructs numerous tables that combine related datasets, and delivers those data to researchers via graphs and spreadsheets on a Microsoft SharePoint-based website. For the AGR-5/6/7 experimental data, a new subsite has been developed, along with a set of web pages. These pages will be used by members of fuel irradiation team for monitoring irradiation conditions according to specification (SPC-1749), by the physics modelers to access necessary model inputs, and by the nuclear engineering community to view and access data such as fuel temperatures, fission product release from capsules, and ATR operational parameters. The deliverable represented in this document is a SharePoint website containing tables of the AGR-5/6/7 measured and calculated data, graphs displaying the data, and links to source documents and references.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Certification and User Manual for A 5kW Heat Exchanger Test Loop at Low Temperatures and High-Pressures

Yankee Scientific has designed and built a custom heat exchanger test stand (HXTS), for Oak Ridge National Laboratory, to support a program to develop advanced heat exchangers (HX) for geothermal Organic Rankine Cycle (ORC) power plants under Subcontract Number 40000141544 with ORNL. The test stand was designed to measure the performance of laboratory scale sub-sections of these advanced heat exchangers. Provisions have been made to facilitate testing the advanced heat exchanger as a primary refrigerant vaporizer and as a recuperator and as the system condenser. The test loop was operated with a controller and was instrumented with 11 thermocouples, 5 pressure gauges, 2 pressure transducers, 2 differential pressure transducers, and 3 flow meters.

15 GEOTHERMAL ENERGY↗

Optical Fiber Sensor Technology Development and Field Validation for Distribution Transformer and Other Grid Asset Health Monitoring

Power transformers are critical pieces of infrastructure in the electric grid that are both extremely expensive and difficult to replace. These transformers often have long lead times for replacement, and failures can create long service disruptions. This project has developed a new suite of sensors designed to give early warning of the impending failure of these important power transformers before it is too late and a major failure occurs. By using novel fiber optic sensors instead of conventional existing technologies, we are able to measure transformer characteristics indicative of impending failures in ways that were not previously possible. These new optical fiber-based sensors are completely immune to the strong magnetic fields present in power transformers, as well as being capable of using distributed measurement techniques. Distributed measurement techniques enable the fiber to return information all along its length as opposed to only collecting data at a single point; as would a thermocouple or standard pressure sensor.

24 POWER TRANSMISSION AND DISTRIBUTION↗

Non-visual analysis of miniaturized melt wire arrays for in-pile measurement of peak irradiation temperature

As a part of the in-pile instrumentation program, the Idaho National Laboratory (INL) has established in-house capabilities to fabricate and test new advanced manufactured printed sensors for measurement of peak temperature inside the harsh environment of a nuclear test reactor. Although nuclear test reactors may use standard methods that can provide real-time temperature information, such as thermocouples, the need for feedthroughs for real-time measurements greatly increases the cost of the experiment. Some experiments also present the problem of limited space available for instrumentation. To address this need, INL is working to improve temperature detection options for such applications. The lab is developing advanced manufactured melt wire arrays to determine peak temperatures in experiments with limited space. Furthermore, capabilities to print multiple melt wires with different melting properties on a single miniaturized unit is being established. Recent results and knowledge from this ongoing work have made it possible to develop unique temperature sensors that can accomplish user specific temperature ranges inside the harsh environments experienced during radiation testing.

36 MATERIALS SCIENCE↗

Demonstrate embedding of sensors in a relevant microreactor component

This report describes the first successful embedding of sensors in stainless steel pipe specimens and a miniature hex block to support structural health monitoring of microreactor components during electrically heated testing in non-nuclear testbed facilities. Sensors were embedded with an ultrasonic additive manufacturing process that uses a combination of downward pressure and an ultrasonic scrubbing motion to bond stainless steel foils to underlying materials. After placing sensors within cavities that have been machined to the size of the sensors, the ultrasonic bonding process fills the gaps around the sensors and embeds them within the part. Both Type K thermocouples and spatially distributed fiber-optic strain sensors were successfully embedded within two pipe specimens and a miniature hex block. After the fiber-optic sensors were embedded, they were interrogated and found to have minimal signal attenuation within the embedded region—a significant improvement compared to previous trials. This is likely because of the low-bend-loss fiber that was used, which greatly reduces microbending losses that occur after the embedding process. In addition to showing minimal signal attention, the fibers also showed adequate compressive strain, which is a strong indication that the sensors are physically embedded in the parts as opposed to simply being loosely contained inside the machined cavities. The embedded fibers were able to capture the strain induced in one of the pipe specimens while the pipe was actively heated with a moving heat source.

42 ENGINEERING↗

One-Step Ahead Prediction of Thermal Mixing Tee Sensors with Long Short Term Memory (LSTM) Neural Networks

High-temperature advanced reactors under development, such as sodium fast reactors (SFR) and molten salt cooled reactors (MSCR), are expected to offer lower levelized cost of energy (LCOE) compared to existing light water reactor (LWR’s). In the existing light water reactors (LWR’s), operation and maintenance (O&M) expenses constitute the largest fraction of the total operating cost. Some of the O&M costs are related maintenance of sensors which can fail due to exposure to harsh environment in a reactor. The O&M costs of Advanced Reactor (AR)’s are expected to constitute a significant fraction of the total cost as well, because of high temperature and radiation level in AR are likely to cause material fatigue and premature failure of sensors and components. The O&M costs in AR’s could be reduced through integration of advanced informatics of performance-related sensors into a digital twin designed for reactor monitoring. For example, machine learning (ML) could be employed for real-time validation and correction of performance-related sensors, and reducing the number of performance-related physical sensor units through virtual sensing. As part of the effort, we investigate real-time validation of thermal hydraulic sensors through one-step ahead forecasting of sensor values using long short-term memory (LSTM) recurrent neural networks (RNN). The sensors are installed in a flow loop containing a thermal mixing tee, which is a common experimental model to study thermal fatigue in a thermal hydraulic loop. In addition, nonlinear transients generated in a thermal mixing tee constitute a good challenge data set for training and validation of ML algorithms. Sensors in this study include thermocouples, flow meters, and optical fibers for distributed temperature sensing. In one experiment, measurement data sets were obtained for a loop was filled with water, and in another experiment, measurements were performed on a loop filled with liquid metal Galinstan. We have also conducted preliminary investigation of one-step ahead prediction of fiber optics-based distributed temperature sensing with LSTM networks. In predicting fiber-based temperature measurements, we treated each gauge pitch of the fiber as an independent sensor. Accuracy of one-step ahead forecasting was estimated by calculating root mean square error (RMSE) for the test segment of time series of each sensor. RMSE’s for temperature sensors in water loop were, for the most part, lower than for the same sensors in Galinstan loop. The RMSE’s for flow meters were similar for both loops. The RMSE’s for distributed temperature measured with the fiber optic sensor were similar to those of the point sensors. Results of this study demonstrated the capability of LSTM one-step ahead forecasting with RMSE comparable to uncertainty in sensor measurements.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗

Transient Thermal Analysis of Calorimeters Used in Characterization of the ACRR Radiation Environments

Silicon calorimeters have been used for active radiation dosimetry in the central cavity of the Annular Core Research Reactor (ACRR) for over a decade. Recently, there has been interest in using other materials for calorimetry to accurately measure the prompt gamma-ray energy deposition in the mixed neutron and gamma-ray environment. The calorimeters used in the ACRR use a thermocouple (TC) to measure the change in temperature of specific materials in the radiation environment. The temperature change is related to the instantaneous dose received by the material in a pulse-transient operation. SOLIDWORKS Simulation and ANSYS Mechanical were used to model the calorimeter and analyze the thermal behavior under pulse-transient conditions. This report compares the results from modeling to experimental results for selected calorimeter materials and radiation environments. These materials include bismuth, tin, zirconium, and silicon. Calorimeters assembled with each material were irradiated in the ACRR central cavity in the free- field, LB44, CdPoly, and PLG radiation environments. The neutronics code Monte-Carlo N- Particle (MCNP) was used to calculate the neutron and gamma-ray response of the calorimeter materials at the experimental locations in the central cavity. Different response tallies were used and found to give different results for the gamma-ray energy deposition. It was determined that performing the neutron/gamma-ray/electron transport in MCNP using the *F8 electron tally gave the overall best agreement with the experimental results. The *F8 tally, however, is much more computationally intensive than the neutron/gamma-ray transport calculations. Also, this report contains parametric analyses that examine the ways to improve the current design of the calorimeters. One finding from the parametric analysis was that the TC should be placed closer to the outer radius of the disks to obtain a measurement closer to the maximum temperature of the disk. Also, the parametric analysis showed that the most dominant mechanism of heat loss in the calorimeters is conduction through the alumina posts. In future designs, the conduction should be minimized to reduce the effect of heat loss on the measurements.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

Wireless Instrumented RB Experiment Preliminary Design and Analysis

The ability to deploy new nuclear fuels for current or future reactor concepts requires carefully designed experiments to generate data to support fuel qualification. Ideally these experiments would include state of-the-art sensing to maximize the amount of in situ data that can be collected during operation. Furthermore, advanced reactor systems can take advantage of integrated in-core sensing technologies to maximize fuel utilization, reduce unnecessary conservativism in design margins, and improve operator’s understanding of limiting peaking factors. Before any novel sensing technologies can be readily adopted for nuclear applications, they must first demonstrate acceptable performance in test reactors. This report summarizes the preliminary design and analysis of the most highly instrumented irradiation experiment ever performed in the removable beryllium (RB) positions of the High Flux Isotope Reactor (HFIR) at Oak Ridge National Laboratory (ORNL). The Wireless Instrumented RB Experiment 2021 (WIRE-21) will test a wide range of sensors including wireless sensors being developed by Westinghouse Electric Company (WEC) that could provide in situ measurements of peak fuel temperatures and fuel rod pressurization due to fission gas release. The ability to wirelessly transmit a signal through the fuel rod’s cladding is critical to improving fuel monitoring capabilities without requiring signal penetrations through the cladding pressure boundary, which would significantly impact fuel fabrication, handling, and operation. Other sensors that will be tested in WIRE-21 include an array of thermocouples, self-powered neutron detectors (SPNDs), and spatially distributed fiber-optic temperature sensors. More generally, WIRE-21 will establish a flexible irradiation vehicle design to allow accelerated, economical testing of advanced sensor technologies while leveraging the extremely high neutron flux that is available in HFIR. This report summarizes the mechanical design for WIRE-21, the experimental test matrix, initial neutronic and thermal design analyses, and the active monitoring and control system enhancements necessary to support testing of advanced sensor technologies. The containment for WIRE-21 is similar to previous RB irradiation vehicles but includes a few modifications, most notably the use of integrated compression seals to pass a larger number of sensor leads through the experiment’s pressure boundary. In addition to the sensor leads, inert gas lines are passed into the experiment to enable active temperature control and the ability to pneumatically actuate a bellows-driven pressure sensor. WIRE-21 is targeting temperatures (300–350°C) and neutron fluence levels (~10 22 n/cm 2 ) relevant to light water reactors (LWRs), but the flexible design of the experiment vehicle allows much higher operating temperatures (>1,100°C). Neutronic calculations determine the neutron flux conditions as well as the nuclear heating within the experiments. These results are used as inputs to detailed thermal finite element calculations, which are required to evaluate the complex, three-dimensional heat transfer that occurs within WEC’s wireless sensor enclosures. Initial results show that the temperatures of the sensors’ enclosures and the metal bellows can be operated near the temperature range of LWR coolants and cladding while simultaneously increasing the temperature of a surrogate fuel material to values in the range of 800–1200°C to simulate centerline fuel temperatures during LWR operation.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Simulations of SITI Cookoff Experiments Carried Out with Different Lots of PBX 9502

A pressure dependent cookoff model for PBX 9502 was developed by Hobbs’ et. al. PBX 9502 is composed of 95% by mass triaminotrinitrobenzene (TATB) and a 5% by mass chlorotrifluoroethylene/vinylidine fluoride binder. The objective in this study is to implement this cookoff model in Aria to simulate Sandia Instrumented Thermal Ignition (SITI) experiments that were carried out with different manufacturing lots of PBX 9502. The SITI design consists of solid cylinders (1" diameter × 1" height) of insensitive high explosive (IHE) confined by a cylindrical aluminum case. An electric heater is wrapped around the lateral surface of the case. This heater produces a temperature heating ramp on the outer surface of the case. Internal thermocouples measure the IHE temperature rise from the center to locations close to the IHE-aluminum interface. The energetic material is heated until thermal ignition occurs. Pressure is measured with a static pressure transducer installed on top of the confinement case. Two–dimensional axisymmetric heat conduction finite element models were implemented to simulate these experiments using four options of the PBX 9502 cookoff model. In addition, the predictive ability of this thermal decomposition model is evaluated using Latin Hypercube Sampling (LHS) techniques.

42 ENGINEERING↗

Data and Insights for the KRUSTY Nuclear-Powered Tests

This document, and the associated files, describe all of the data from the KRUSTY warm criticals and the KRUSTY nuclear system test. The warm criticals were a group of tests where fission power heated the core and the feedback response was studied. There were 3 experiments, the 15-cent run (which was a true “free run”), followed by 30-cent and 60-cent runs, where reactivity was added to heat the core to higher temperatures. The nuclear system test (often referred to as the full-run or the final-run), engaged the power conversion system and evaluated system performance. These experiments are described in a pair of NUCLEAR TECHNOLOGY papers, which includes plots of the data that this document-set includes. Note that a lot of information in this document is based on my interpretation and could be wrong, but I’ve included it to potentially save some people a lot of time and headaches by trying to figure out which instrumentation to believe, but beware treating anything I say as fact. I’ve also included several post-irradiation photos, to show some thermocouple locations and indicate possible changes in emissivity and/or geometry (although no changes in geometry were indicated).

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

Brine Availability Test in Salt (BATS) FY21 Update

This report summarizes the 2021 fiscal year (FY21) status of ongoing borehole heater tests in salt funded by the disposal research and development (R&D) program of the Office of Spent Fuel & Waste Science and Technology (SFWST) of the US Department of Energy’s Office of Nuclear Energy’s (DOE-NE) Office of Spent Fuel and Waste Disposition (SFWD). This report satisfies SFWST milestone M2SF- 21SN010303052 by summarizing test activities and data collected during FY21. The Brine Availability Test in Salt (BATS) is fielded in a pair of similar arrays of horizontal boreholes in an experimental area at the Waste Isolation Pilot Plant (WIPP). One array is heated, the other unheated. Each array consists of 14 boreholes, including a central borehole with gas circulation to measure water production, a cement seal exposure test, thermocouples to measure temperature, electrodes to infer resistivity, a packer-isolated borehole to add tracers, fiber optics to measure temperature and strain, and piezoelectric transducers to measure acoustic emissions. The key new data collected during FY21 include a series of gas tracer tests (BATS phase 1b), a pair of liquid tracer tests (BATS phase 1c), and data collected under ambient conditions (including a period with limited access due to the ongoing pandemic) since BATS phase 1a in 2020. A comparison of heated and unheated gas tracer test results clearly shows a decrease in permeability of the salt upon heating (i.e., thermal expansion closes fractures, which reduces permeability).

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

SPHERE Assembly and Operation Demonstration

The objective of the current scope was to complete single primary heat extraction and removal emulator (SPHERE) assembly and demonstrate the operation of the SPHERE facility. The initial testing consisted of vacuum operation of a sodium heat pipe. The temperature was measured at 10 evenly spaced points along the heat pipe. Additional exterior thermocouple measurements were also taken on the exterior of the heat pipe to confirm the similarity of thermowell temperatures to exterior heat pipe temperature measurements. The initial test was successfully completed and results measured at INL are consistent with the data from the manufacturer.

42 ENGINEERING↗

Design Optimization for Printed Melt Wire Arrays Encapsulation

As part of the Nuclear Energy Enabling Technology (NEET) Advanced Sensor and Instrumentation (ASI) Program, Idaho National Laboratory (INL) has recently established in-house capabilities to fabricate and test new advanced-manufactured sensors for measuring peak irradiation temperature within a nuclear test reactor. Although methods of real-time temperature monitoring, such as thermocouples, may be used, the complexity of feedthroughs and attachments to collect real-time measurements greatly increases the cost of the experiment. Instead, passive monitoring techniques may be used for peak- temperature measurement that exploit the melting point of well-characterized materials (standard melt wires) to infer peak reactor temperatures. However, limited available space for instrumentation during experiments introduces an additional challenge. To accommodate this, INL has expanded its temperature- detection instrumentation capabilities to include advanced manufactured (AM) melt wires for peak irradiation temperature measurements. These melt wires can determine peak temperatures while also accommodate space limitations in irradiation experiments. In an effort to improve performance reliability of AM meltwire capabilities, a process was developed and tested to identify the significance of entrapping a high purity inert atmosphere within the packaging of printed melt wire arrays. The materials used in this study were aluminum, zinc, and tin encapsulated in high purity helium within a stainless steel (SS) 316 container. Tin, with a low melting point of approximately 230°C, Zn with a mid-melting point of approximately 420°C, and Al with a high melting point of approximately 660°C. This report describes the design, fabrication process, furnace testing and X-ray Computed Tomography (XCT) evaluation. Results show a successful outcome in creating an inert gas encapsulation and high-resolution evaluation methods.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Initial Temperature Testing of Advanced Manufactured Melt Wire Package

As a part of the In-Pile Instrumentation Program, The Idaho National Laboratory (INL) has recently established in-house capabilities to fabricate and test new advanced manufactured sensors for measuring the peak irradiation temperature inside a nuclear test reactor. Although nuclear test reactors can use standard methods of real-time temperature monitoring, such as thermocouples, the complexity of feedthroughs and attachment complications to collect real-time measurements greatly increases the cost of the experiment. Passive monitoring techniques may be utilized that exploit the melting point of well characterized material (standard melt wires), however, the limited space available for instrumentation during experiments is also a challenge. To accommodate the challenge, INL has expanded its temperature detection instrumentation capabilities paired with the advancement of in-house advanced manufacturing options to include printed melt wires for peak irradiation temperature measurement. The advanced manufactured melt wire package can determine peak temperatures in experiments that can fit the challenging space available during irradiation. Recent results and knowledge from this ongoing work have made it possible to develop unique temperature sensors that can accomplish user specific temperature ranges inside the harsh environments experienced during radiation testing. This report summarizes the initial temperature testing using fabricated melt wires with two different melting temperatures, silver (melting temperature of ~960 °C) and solder (melting temperature of ~160 °C), that were initially tested for their relative melting points using non-standard method of furnace and hot plate testing under normal air conditions. Future work will include more controlled way of testing printed melt wires under inert gas with multiple temperature measurements followed by comparison of standard melt wire package performance for baseline characterization.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Computational and Experimental Validation of Fractal-Fin, Dimpled Solar Heat Collector

A 3 foot x 3 foot x 3 foot aluminum solar collector was manufactured using computer numerical control. The interior of the device included six triangular dimpled fins for enhanced heat transfer. The interior vertical wall on the south side was also dimpled. The solar collector working fluid was based on water, and the collector consisted solely of passive heat transfer mechanisms (no moving parts), making it ideal for off-the-grid and rural applications. Two types of heat transfer experiments were conducted. One experiment had external flat heaters attached on the top and the front side, while the other four sides were insulated. Except for the bottom surface, the second experiment had all its exterior surfaces sprayed with black solar paint to collect as much solar heat as possible. Temperature data as a function of time was collected using 14 thermocouples spread strategically throughout the solar collector. In addition, computational fluid dynamics (CFD) simulations were conducted using the dynamic Smagorinsky large eddy simulation turbulence model. The first simulation considered that both the top and front surfaces were exposed to a fixed temperature of 313.7 K (105 °F), while the remaining four surfaces were insulated. For the second simulation, all conditions were the same, except that the temperature for both heated surfaces was raised to 350 K (170.3 °F). The two temperatures are expected to bound the solar collector operational temperature during the late- Spring, Summer, and early-Fall months. The solar collector design, experimental data, CFD output, and a discussion of five manufacturing approaches and costs are documented in this report.

14 SOLAR ENERGY↗

AOI [1]: Passive Wireless Sensor Systems Fabricated by Direct-Writing for Temperature and Health Monitoring of Energy Systems in Harsh-Environments (Final Report)

Researchers at West Virginia University (WVU) propose to demonstrate a wireless, high-temperature sensor system for monitoring the temperature and health of energy-system components. The active sensor and electronics for wireless communication will be composed entirely of an electroceramic materials (conductive ceramics) which are capable of withstanding the harsh-environments required for fossil energy-based technologies. This work will focus primarily on the fabrication and testing of temperature (thermocouples and thermistors) and health (strain/stress and crack propagation sensors) that function at extreme temperatures (up to 700-1700ºC). The electronics will accompany the high-temperature sensor, which will include a passive wireless communication circuit that allows the transmission of the data based on the LCR resonance principle to a near-by reader antenna. This passive transmission of data will reduce the need for interconnect wires near the active, and possibly rotating, energy-system component. The research will include process development to permit the 2D/3D direct-writing of the entire sensor and communication circuit onto the energy-system component. The direct-writing will be facilitated by using silicon-based polymer-derived precursors to form the high-temperature, stable electroceramic compositions. In addition, methods for direct-writing the circuit onto a fugitive carrier substrate will be completed, which will permit a “peel-and-stick”-like transfer of the sensor circuit to the energy-system component. This feature will allow the economical and precise placement of the sensor circuit onto components of various shapes and locations, without altering the geometry and active features of the manufactured component, or the removal (or decommissioning) of the component for installation. The proposed work will be directed at the following areas: 1) Investigation of phase formation, sintering/grain growth, and electrical properties of polymer-derived electroceramic composites; 2) Definition of processes to direct-write through ink-jet and robo-casting the polymer-derived electroceramic composites onto oxide and polymer surfaces; 3) Development of methods to form monolithic "peel-and-stick" preforms that will efficiently transfer the sensor circuit to ceramic surfaces after thermal treatment; 4) Design of passive wireless LCR circuits and receiver (reader) antennas for communication and testing at high temperatures; 5) Investigation of the passive wireless sensor system developed (and method of transferring sensor system) for temperature and stress/strain measurements on a SOFC repeat unit and a singular gas turbine blade prototype as example applications.

01 COAL, LIGNITE, AND PEAT↗