Engineering Papers⌕ Search

SEARCH · Engineering Papers

Results for “RESIDUES”

Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

Quote a phrase for an exact phrase match. Source license links do not imply unrestricted reuse.

At least 901 records · Page 50
All sourcesNASA NTRSDOE OSTI
DOE OSTI2024

Lignin content of Populus trichocarpa residues after CELF pretreatment and CBP fermentation

Here we present a dataset of lignin content from a woody energy crop (Populus trichocarpa) residues after a series of co-solvent enhanced lignocellulosic fractionation (CELF) pretreatment and consolidated bioprocessing (CBP) process. The natural poplar variant GW-9947 from the Center for Bioenergy Innovation (CBI) was used. The poplar was knife milled and passed through a 1 mm sieve and CELF pretreatment was performed in a Parr autoclave reactor with 7.5 wt % solids loading, 0.5 wt% H2SO4 as catalyst at 150°C with 5, 15, 25 and 30 minutes, respectively. Tetrahydrofuran was added in a 1:1 mass ratio with water as the pretreatment solvent. The residues from CELF pretreatment were then subjected to CBP using the bacterium C. thermocellum DSM 1313. CBP fermentations were performed at 60 °C in a shaker at 50, 75, and 100 grams/L solids loadings. The Klason lignin was measured using a two-step acid hydrolysis process. In brief, the poplar samples were first hydrolyzed by 72 wt% sulfuric acid at 30 oC for an hour. The hydrolysates were then diluted to 4 wt% sulfuric acid using deionized water and subsequently autoclaved at 121 oC for 1 h. Upon the completion of the two-step hydrolysis, the resulting solution was cooled to room temperature and the precipitate was then filtered through a G8 glass fiber filter through a crucible, dried at oven for overnight, and weighed to get the Klason lignin content. The lignin data provides information about lignin content changes after CELF and C. thermocellum CBP process.

Lignin Populus trichocarpa CELF pretreatment CBP f↗
DOE OSTI2022

Using Direct Numerical Simulation of Pore-Level Events to Improve Pore-Network Models for Prediction of Residual Trapping of CO2

Direct numerical simulation and pore-network modeling are common approaches to study the physics of two-phase flow through natural rocks. For assessment of the long-term performance of geological sequestration of CO 2 , it is important to model the full drainage-imbibition cycle to provide an accurate estimate of the trapped CO 2 . While direct numerical simulation using pore geometry from micro-CT rock images accurately models two-phase flow physics, it is computationally prohibitive for large rock volumes. On the other hand, pore-network modeling on networks extracted from micro-CT rock images is computationally efficient but utilizes simplified physics in idealized geometric pore elements. This study uses the lattice-Boltzmann method for direct numerical simulation of CO 2 -brine flow in idealized pore elements to develop a new set of pore-level flow models for the pore-body filling and snap-off events in pore-network modeling of imbibition. Lattice-Boltzmann simulations are conducted on typical idealized pore-network configurations, and the interface evolution and local capillary pressure are evaluated to develop modified equations of local threshold capillary pressure of pore elements as a function of shape factor and other geometrical parameters. The modified equations are then incorporated into a quasi-static pore-network flow solver. The modified model is applied on extracted pore-network of sandstone samples, and saturation of residual trapped CO 2 is computed for a drainage-imbibition cycle. The modified model yields different statistics of pore-level events compared with the original model; in particular, the occurrence of snap-off in pore-throats is reduced resulting in a more frontal displacement pattern along the main injection direction. Compared to the original model, the modified model is in closer agreement with the residual trapped CO 2 obtained from core flow experiments and direct numerical simulation.

Kohanpur, Amir H.↗
DOE OSTI2019

Channelrhodopsin-2 Function is Modulated by Residual Hydrophobic Mismatch with the Surrounding Lipid Environment

Channelrhodopsin-2 (ChR2) is a light-gated ion channel that conducts cations of multiple valencies down the electrochemical gradient. This light-gated property has made ChR2 a popular tool in the field of optogenetics, allowing for the spatial and temporal control of excitable cells with light. A central aspect of protein function is the interaction with the surrounding lipid environment. To further explore these membrane-protein interactions, we demonstrate the role of residual hydrophobic mismatch (RHM) as a mechanistically important component of ChR2 function. We combined computational and functional experiments to understand how RHM between the lipid environment and ChR2 alters the structural and biophysical properties of the channel. Analysis of our results revealed significant RHM at the intracellular/lipid interface of ChR2 from a triad of residues. The resulting energy penalty is substantial and can be lowered via mutagenesis to evaluate the functional effects of this change in lipid-protein interaction energy. The experimental measurement of channel stability, conductance and selectivity resulting from the reduction of the RHM energy penalty showed changes in progressive H+ permeability, kinetics and open-state stability, suggesting how the modulation of ChR2 by the surrounding lipid membrane can play an important biological role and contribute to the design of targeted optogenetic constructs for specific cell types.

Richards, Ryan↗
DOE OSTI2021

In-Situ Calibrated Modeling of Residual Stresses Induced in Machining under Various Cooling and Lubricating Environments

Although many functional characteristics, such as fatigue life and damage resistance depend on residual stresses, there are currently no industrially viable ‘Digital Process Twin’ models (DPTs) capable of efficiently and quickly predicting machining-induced stresses. By leveraging advances in ultra-high-speed in-situ experimental characterization of machining and finishing processes under plane strain (orthogonal/2D) conditions, we have developed a set of physics-based semi-analytical models to predict residual stress evolution in light of the extreme gradients of stress, strain and temperature, which are unique to these thermo-mechanical processes. Initial validation trials of this novel paradigm were carried out in Ti-6Al4V and AISI 4340 alloy steel. A variety dry, cryogenically cooled and oil lubricated conditions were evaluated to determine the model’s ability to capture the tribological changes induced due to lubrication and cooling. The preliminarily calibrated and validated model exhibited an average correlation of better than 20% between the predicted stresses and experimental data, with calculation times of less than a second. Based on such fast-acting DPTs, the authors envision future capabilities in pro-active surface engineering of advanced structural components (e.g., turbine blades).

36 MATERIALS SCIENCE↗
DOE OSTI2020

Robust Learning with Implicit Residual Networks

In this effort, we propose a new deep architecture utilizing residual blocks inspired by implicit discretization schemes. As opposed to the standard feed-forward networks, the outputs of the proposed implicit residual blocks are defined as the fixed points of the appropriately chosen nonlinear transformations. We show that this choice leads to the improved stability of both forward and backward propagations, has a favorable impact on the generalization power, and allows for control the robustness of the network with only a few hyperparameters. In addition, the proposed reformulation of ResNet does not introduce new parameters and can potentially lead to a reduction in the number of required layers due to improved forward stability. Finally, we derive the memory-efficient training algorithm, propose a stochastic regularization technique, and provide numerical results in support of our findings.

Reshniak, Viktor↗
DOE OSTI2014

Beyond the Streetlight Effect: A United Future for Relaxation and Diffraction Methods for Residual Stress Measurement

Residual stress measurement techniques can be categorized as either relaxation or diffraction methods. Practitioners often advocate a particular category and sometimes a specific technique (hole drilling, contour, XRD, neutron, etc) based on their experience or capability rather than using the best technique for the particular application. This paper considers some of the implications from applying this “drunkard’s search” or “streetlight” approach by examining examples where the critical stress could be hidden from both relaxation and diffraction measurements. A better approach to planning residual stress measurements would begin with a detailed consideration of why the stresses should be measured and how the results will be used. Only then can the most appropriate measurement plan be developed. Since a single measurement technique cannot reveal the full state of stress, especially in challenging parts, the use of multiple measurement types often provides the most useful information to customers.

36 MATERIALS SCIENCE↗
DOE OSTI2018

Residual Stresses and Plastic Deformation in Self-Pierce Riveting of Dissimilar Aluminum-to-Magnesium Alloys

In this study, the complex relationship between deformation history and residual stresses in a magnesium-to-aluminum self-pierce riveted (SPR) joint is elucidated using numerical and experimental approaches. Non-linear finite element (FE) simulations incorporating strain rate and temperature effects were performed to model the deformation in the SPR process. In order to accurately capture the deformation, a stress triaxiality-based damage material model was employed to capture the sheet piercing from the rivet. Strong visual comparison between the physical cross-section of the SPR joint and the simulation was achieved. To aid in understanding of the role of deformation in the riveting process and to validate the modeling approach, several experimental measurements were conducted. To quantify the plastic deformation from the piercing of the rivet, micro hardness mapping was performed on a cross-section of the SPR joint. The FE model showed very strong correlation to the experimental hardness mapping results suggesting the nonlinear model captured the plastic deformation with high accuracy. To measure the elastic residual stresses in the SPR joint, neutron and x-ray diffraction mapping techniques were conducted and in general, the FE model correlated well to the trends and magnitudes of the elastic stresses. While some error occurred in between the model and the neutron and x-ray diffraction results, the numerical approach developed in this study shows potential as a tool for understanding SPR behavior as well as optimizing the process parameters.

36 MATERIALS SCIENCE↗
DOE OSTI2016

Development and characterization of an ice-selecting pumped counterflow virtual impactor (IS-PCVI) to study ice crystal residuals

Separation of particles that play a role in cloud activation and ice nucleation from interstitial aerosols has become necessary to further understand aerosol-cloud interactions. The pumped counterflow virtual impactor (PCVI), which uses a vacuum pump to accelerate the particles and increase their momentum, provides an accessible option for dynamic and inertial separation of cloud elements. However, the use of a traditional PCVI to extract large cloud hydrometeors is difficult mainly due to its small cut-size diameters (< 5 µm). Here, for the first time we describe a development of an ice-selecting PCVI (IS-PCVI) to separate ice in controlled mixed-phase cloud system based on the particle inertia with the cut-off diameter ≥ 10 µm. We also present its laboratory application demonstrating the use of the impactor under a wide range of temperature and humidity conditions. The computational fluid dynamics simulations were initially carried out to guide the design of the IS-PCVI. After fabrication, a series of validation laboratory experiments were performed coupled with the Aerosol Interaction and Dynamics in the Atmosphere (AIDA) expansion cloud simulation chamber. In the AIDA chamber, test aerosol particles were exposed to the ice supersaturation conditions (i.e., RH ice > 100 %), where a mixture of droplets and ice crystals was formed during the expansion experiment. In parallel, the flow conditions of the IS-PCVI were actively controlled, such that it separated ice crystals from a mixture of ice crystals and cloud droplets, which were of diameter ≥ 10 µm. These large ice crystals were passed through the heated evaporation section to remove the water content. Afterwards, the residuals were characterized with a suite of online and offline instruments downstream of the IS-PCVI. These results were used to assess the optimized operating parameters of the device in terms of (1) the critical cut-size diameter, (2) the transmission efficiency and (3) the counterflow-to-input flow ratio. Particle losses were characterized by comparing the residual number concentration to the rejected interstitial particle number concentration. Overall results suggest that the IS-PCVI enables inertial separation of particles with a volume-equivalent particle size in the range of ~&thinsp;10–30 µm in diameter with small inadvertent intrusion (~ &thinsp;5 %) of unwanted particles.

54 ENVIRONMENTAL SCIENCES↗
DOE OSTI2018

Electromagnetic zonal flow residual responses

The collisionless axisymmetric zonal flow residual calculation for a tokamak plasma is generalized to include electromagnetic perturbations. We formulate and solve the complete initial value zonal flow problem by retaining the fully self-consistent axisymmetric spatial perturbations in the electric and magnetic fields. Simple expressions for the electromagnetic test of the zonal flow residual in gyrokinetic codes. Unlike the electrostatic potential, the parallel vector potential and the parallel magnetic field perturbations need not relax to flux functions for all possible initial conditions.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
NASA NTRS1969

Apparatus automatically measures soluble residue content of volatile solvents

Solvent Purity Meter /SPM/ automatically measures the soluble residue in volatile solvents used in cleaning or extraction of oils, greases, and other nonvolatile materials. The SPM gives instantaneous and continuous readout of soluble contaminant residues in concentrations as low as one part per million of solution.

Oswalt, F. W.↗
NASA NTRS1971

C-130: Results of center wing residual strength and crack propagation test program

Fourteen C-130 airplane center wings which had experienced from approximately 4,000 to 13,000 hours of flight service and its associated fatigue damage were tested to destruction, seven in upbending and seven in downbending. Six wings were tested directly for static residual strength in the fatigue-damaged condition as received from field service. The other eight wings were tested in crack propagation cyclic testing at a prescribed stress level for a maximum of 10,000 cycles. Then the stress level was reduced and testing was continued up to a maximum of 20,000 total cycles. Cyclic testing was performed with constant-amplitude stresses at a stress ratio of +0.1. Maximum cyclic skin stresses were approximately 18,000 psi. At the conclusion of cyclic testing, a static test to destruction was conducted to determine the residual strength of each fatigue-damaged specimen.

Reeder, F. L.↗
NASA NTRS1972

Analytical and experimental investigation of aircraft metal structures reinforced with filamentary composites. Phase 2: Structural fatigue, thermal cycling, creep, and residual strength

Specimens representative of metal aircraft structural components reinforced with boron filamentary composites were manufactured and tested under cyclic loading, cyclic temperature, or continuously applied loading to evaluate some of the factors that affect structural integrity under cyclic conditions. Bonded, stepped joints were used throughout to provide composite-to-metal transition regions at load introduction points. Honeycomb panels with titanium or aluminum faces reinforced with unidirectional boron composite were fatigue tested at constant amplitude under completely reversed loading. Results indicated that the matrix material was the most fatigue-sensitive part of the design, with debonding initiating in the stepped joints. However, comparisons with equal weight all-metal specimens show a 10 to 50 times improved fatigue life. Fatigue crack propagation and residual strength were studied for several different stiffened panel concepts, and were found to vary considerably depending on the configuration. Composite-reinforced metal specimens were also subjected to creep and thermal cycling tests. Thermal cycling of stepped joint tensile specimens resulted in a ten percent decrease in residual strength after 4000 cycles.

Blichfeldt, B.↗
NASA NTRS1972

Effect of high temperature creep and oxidation on residual room temperature properties for several thin sheet superalloys

Superalloys are being considered for the primary heat shields and supports in the thermal protection system of both hypersonic transport and space shuttle vehicles. Since conservative design philosophy dictates designs based on residual material properties at the end of the service life, material characterization after exposure to the environmental conditions imposed by the flight requirements of these two classes of vehicles is needed on the candidate alloys. An investigation was conducted to provide some of the necessary data, with emphasis placed on oxidation, creep, and residual properties of thin-gage sheet material.

Royster, D. M.↗
NASA NTRS1972

The effect of residual stress on performance of high temperature coatings

Techniques for measurement of residual stress in MoSi2 coatings and the determination of stress in coatings prepared by metalliding, pack and slurry processes are discussed. The stress level can be determined by stress induced deflections or by X-ray techniques. The deflection method is most direct. It is based on the fact that a thin substrate, coated on one side only, is usually curved at room temperature. The radius of curvature is easily measured and readily related to residual stress.

Source record↗
NASA NTRS1973

Experimental masking of RBV images to reduce stationary residual inaccuracies in radiometric correction

Return beam vidicon tube calibration data are used to correct spatially non-uniform radiance response in individual vidicons, during post-acquisition signal processing. However, examination of different ERTS-1 RBV-1, -2, and -3 image scenes showed stationary, repetitive residual inaccuracies in shading correction, large enough to affect qualitative and quantitative image analyses. Photographic masks designed to reduce residual shading were prepared from RBV-1, -2, and -3 images of a relatively cloud-free ocean scene of uniform reflectance. When applied to other RBV scenes, the masks enabled more closely corrected RBV images to be printed. Illustrations are given of RBV-1 image before and after correction, compared with an equivalent MSS spectral image of the same scene.

Ross, D. S.↗
NASA NTRS1973

Residual stress measurement and analysis using ultrasonic techniques.

A technique which utilizes ultrasonic radiation has been developed to measure residual stresses in metals. This technique makes it possible to detect and measure the magnitude of the principle stresses and also to obtain their direction. The velocities of ultrasonic waves in materials are measured as the time to travel a fixed path length, and the change in transit time is related to the applied stress. The linear relationship obtained allows a procedure based on this principle to be used for the measurement of residual stress using surface waves and shear waves. A method for plotting stress profiles through a material using surface waves uses varying frequencies for the ultrasonic wave. A limitation of the shear wave method is considered. The system used for this technique is called the Modified Time of Flight System.

Noronha, P. J.↗
NASA NTRS1974

Texturing and residual stress in metals as a result of sliding

Pole figures of the texturing produced by friction in the alloys Cu - 10 at. % Sn, Cu - 10 at. % Si, 440 C stainless steel, and AISI 52100 bearing steel were obtained with an energy-dispersive X-ray diffractometer. While the texturing behavior of these alloys is generally similar to that of pure metals, the 52100 steel and the Cu5Si phase of Cu - 10 at. % Si show no texturing at the loads and speeds used in this experiment. Photographic methods were used in an attempt to measure the uniform residual stress in the wear tracks produced on some pure metals. The stress in copper and iron was, however, below the limit of detectability - about 4.3 x 10 to the 7th power N/sq m (6000 psi). Line broadening under all test conditions in the case of copper and at high load and speed conditions in iron is attributed, at least in part, to the reduction of crystallite size and, perhaps, to nonuniform residual stress, as well.

Wheeler, D. R.↗
NASA NTRS1974

Effect of throttling on interface behavior and liquid residuals in weightlessness

An experimental investigation was conducted to study liquid-vapor interface behavior and subsequent vapor ingestion in a flat-bottomed cylindrical tank following a single-step throttling in outflow rate in a weightless environment. A throttling process in which the final Weber number was one-tenth of the initial Weber number tended to excite large-amplitude symmetric slosh, with the amplitude generally increasing as initial Weber number increased. As expected, liquid residuals were lower than those obtained without throttling and, for moderate values of initial Weber number, could be adequately predicted by assuming that all draining took place at the final Weber number. At large values of Weber number, residuals tended to be lower than this predicted value.

Symons, E. P.↗