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At least 91 records · Page 5

Development of an electronically-scanned pressure module for operation at cryogenic temperatures

Pressure and temperature characteristics were measured for a number of multichannel electronically scanned pressure sensors. The tests were made on commercially available units designed to operate in a controlled temperature environment. Measurements of zero shift, sensitivity, and nonlinearity for each transducer were taken over a temperature range from 100 K to 340 K using a computer controlled data acquisition system. The units tested failed to meet accuracy specifications over the complete temperature range, which was expected. However, the sensors showed acceptable and predictable behavior over the temperature range from approximately -40 C (233 K) to 70 C (343 K). It was determined that a combination of local heating and accurate temperature monitoring can result in a device that can be compensated for temperature as well as its other physical properties. The design of a prototype for operation in a cryogenic environment is proposed, and a method for compensation is developed.

Johnson, Preston B.↗

Optimizing ensemble NV − spin properties of fluorescent diamond microparticles by systematic low pressure high temperature annealing

Low pressure high temperature annealing is a means for driving nitrogen and defect diffusion in diamond to reduce internal lattice damage without the need for technically complicated high-pressure cells. Herein, we perform a systematic time (5, 15, and 30 min) and temperature (1200 °C–1800 °C) study of effects of low-pressure high temperature annealing on photoluminescence, spin concentrations, and spin relaxation properties of NV centers in ca. 3 μm synthetic type 1b diamond particles. Annealing in the temperature range of ca. 1400 °C–1700 °C for even 5 min leads to a higher optically detected magnetic resonance contrast as compared to standard annealing at 900 °C for 2 h. Particles annealed at 1700 °C for 5 min exhibit a contrast close to about 13% as compared to about 9% for those annealed at 900 °C for 2 h. A reduction in the zero-field splitting strain parameter from E ≈ 4.5 MHz to ≈ 2.5 MHz and spectral linewidth from Δν ≈ 7 MHz to ≈ 4 MHz are observed even after 5 min annealing at 1700 °C. Improvements in these spectral parameters resulted in a roughly 2-fold reduction in the noise level of temperature monitoring experiment utilizing an ensemble of NV centers in the particles. Annealing in the temperature range of 1600 °C for 15 or 30 min or 1700 °C for 5 min resulted in NV T 1 relaxation times approaching ca. 5 ms typically observed for bulk diamond. Quantitative electron paramagnetic resonance (EPR) allowed for estimations of thermal activation energies of paramagnetic center annihilation. Monitoring the primary defect concentration (P1 and other defects with half integer spins) and utilizing second order kinetic modeling, an activation energy of 3.63 ± 0.28 eV was estimated. Alternatively, using the NV half field EPR signal and first order kinetic modeling, a similar activation energy 3.89 ± 0.29 eV was estimated.

NV centers↗

Rocket temperature soundings

The purpose was to provide rocket-borne measurements of temperature and wind. These data are used to: obtain a better understanding of the processes that control the chemical and dynamic behavior of the stratospheric region; monitor temperature trends and detect changes; verify and monitor remote measurements (ground- and satellite-based); and provide density measurements for large space vehicle operations.

Schmidlin, Francis J.↗

Precision and Radiosonde Validation of Satellite Gridpoint Temperature Anomalies. Part I; MSU Channel 2: MSU Channel 2 - Pt. 1

In Part 1 of this study, monthly 2.5 deg. gridpoint anomalies in the TIROS-N (Television and Infrared Operational Satellite-N) series Microwave Sounding Unit (MSU) channel 2 brightness temperatures during 1979-88 are evaluated with multiple satellites and radiosonde data for their climate temperature monitoring capability. The MSU anomalies we computed about a 10-year mean annual cycle at each grid point, with the MSUs intercalibrated to a common arbitrary level. The intercalibrations remove relative biases between instruments of up to several tenths of a degree celsius. The monthly gridpoint anomaly agreement between concurrently operating satellites reveals single-satellite precision on generally better than 0.07 C in the tropics and better than 0.15 C at higher latitudes. Monthly anomalies in radiosonde channel 2 brightness temperatures computed with the radiative transfer equation compare very closely to the MSU measured anomalies in all climate zones, with correlations generally from 0.94 to 0.98 and standard errors of 0.15 C in the tropics to 0.30 C at high latitudes. Simplification of these radiative transfer calculations to a static weighting profile applied to the radiosonde temperature profile leads to an average degradation of only 0.02 deg. in the monthly skill. In terms of a more traditionally measured quantity, the MSU channel 2 anomalies match best with either the radiosonde 100-20-kPa or 100-15-kPa layer anomalies. No significant spurious trends were found in the 10-yr satellite dataset compared to the radiosondes that would indicate a calibration drift in either system. Thus, sequentially launched, overlapping passive microwave radiometers provide a useful system for monitoring intraseasonal to interannual climate anomalies and offer hope for monitoring of interdecadal trends from space. The Appendix includes previously unpublished details of the MSU gridpoint anomaly dataset construction. Part II of this study addresses the removal from channel 2 of the temperature influence above the 30-kPa level, providing a sharper and thus potentially more useful weighting function for monitoring lower tropospheric temperatures.

Spencer, Roy W.↗

Passive Wireless Sensors for Realtime Temperature and Corrosion Monitoring of Coal Boiler Components Under Flexible Operation (Final Technical Report)

Researchers at West Virginia University (WVU) propose to demonstrate inexpensive wireless, high-temperature sensors for real-time monitoring of the temperature and corrosion of metal components, which are commonly used in coal-fired boilers. This study presents the development of cost-effective wireless high-temperature sensors for real-time temperature and corrosion monitoring in coal-fired boilers' metal components. The focus is on fabricating and evaluating chipless radio-frequency identification (RFID) sensors capable of operating between 25-1300 ºC. Efforts were directed towards designing passive RFID sensor and interrogator antenna with a broad frequency range, optimizing a microstrip patch antenna sensor integrated into a "peel-and-stick" format for efficient application to various metal specimens without altering their geometry. Additionally, this research aimed to assess the sensor responses under accelerated high-temperature conditions, correlating corrosion and cracking mechanisms with sensor data. An investigation of through-wall data acquisition techniques was also planned, facilitating unobtrusive monitoring of sensor responses housed within metal enclosures. Ultimately, this work sought to establish a robust passive wireless sensor system for the continuous health monitoring of metal components in operational settings, thereby contributing to enhanced safety and efficiency in coal-fired power plants.

20 FOSSIL-FUELED POWER PLANTS↗

Development of an ERT‐Based Framework for Bentonite Buffers Monitoring From Laboratory Tests: 1. Characterizing Thermal–Hydrological–Mechanical Processes

Abstract Bentonite clay is widely used in engineered barrier systems for the permanent disposal of high‐level radioactive waste due to its low permeability, high swelling capacity, and thermal stability. However, the complex thermal‐hydrological‐mechanical (THM) processes induced by heating from decaying radioactive waste and hydration from surrounding rock can lead to heterogeneous changes that are difficult to measure and predict. This study develops an Electrical Resistivity Tomography (ERT)‐based framework for monitoring THM processes, progressing from sample‐scale to bench‐scale tests, to inform field‐scale applications. Sample‐scale tests analyzed small bentonite samples under controlled variations in water content, temperature, and porosity to establish fundamental resistivity relationships. Bench‐scale tests involved larger bentonite columns subjected to heating (up to 200°C) and hydration under controlled pressure, simulating repository conditions. ERT measurements, complemented by X‐ray CT imaging, temperature monitoring, and tracing sensors, revealed coupled THM processes, such as hydration‐induced compression, swelling, and thermal gradients, leading to complex resistivity patterns. The results demonstrate the potential of ERT for capturing THM‐induced resistivity changes, though challenges remain in upscaling and quantitative analysis. This study evaluates laboratory test capabilities and proposes future improvements for understanding THM‐induced resistivity responses. A conceptual framework for ERT implementation in field‐scale monitoring is presented, synthesizing findings from both scales and exploring how ERT data can inform long‐term modeling and reduce prediction uncertainties. Overall, this ERT‐based framework offers a robust method for monitoring bentonite buffers, aiding in early issue detection and supporting the safe long‐term disposal of radioactive waste in geological repositories, while highlighting the need for future development. Plain Language Summary Bentonite clay is crucial in engineered barrier systems (EBS) for containing high‐level radioactive waste due to its ability to absorb water, swell, seal and remain stable under high temperatures. When bentonite absorbs water and heats up from radioactive decay, it experiences complex changes in its physical and mechanical properties. Understanding these changes is important for ensuring the long‐term safety and effectiveness of EBS. This study used Electrical Resistivity Tomography (ERT), a non‐invasive method that measures electrical conductivity to monitor these changes during laboratory experiments. The ERT data revealed significant variations in resistivity corresponding to changes in water content, temperature, and density, providing detailed spatial and temporal insights into the behavior of bentonite. These findings enhance our ability to predict the long‐term performance of bentonite barriers, ensuring the safe containment of radioactive waste. By improving our understanding of bentonite's behavior, this research supports the development of more reliable and effective barrier systems for radioactive waste disposal, protecting the environment and public health. Key Points ERT monitoring was employed to capture resistivity changes in bentonite during controlled heating and hydration experiments, providing insights into THM processes ERT data reveal significant resistivity changes correlated with water content, temperature, and mechanical effects, enhancing the understanding of THM dynamics in bentonite This study explores the potential of the framework for application in field‐scale EBS monitoring, emphasizing the need for integrating additional geophysical methods for comprehensive subsurface imaging

Chen, Hang↗

Comparison of Summer and Winter California Central Valley Aerosol Distributions from Lidar and MODIS Measurements

Aerosol distributions from two aircraft lidar campaigns conducted in the California Central Valley are compared in order to identify seasonal variations. Aircraft lidar flights were conducted in June 2003 and February 2007. While the ground PM(sub 2.5) concentration is highest in the winter, the aerosol optical depth measured from MODIS is highest in the summer. A seasonal comparison shows that PM(sub 2.5) in the winter can exceed summer PM(sub 2.5) by 55%, while summer AOD exceeds winter AOD by 43%. Higher temperatures and wildfires in the summer produce elevated aerosol layers that are detected by satellite measurements, but not surface particulate matter monitors. Temperature inversions, especially during the winter, contribute to higher PM(sub 2.5) measurements at the surface. Measurements of the boundary layer height from lidar instruments provide valuable information need to understand the relationship between satellite measurements of optical depth and in-situ measurements of PM(sub 2.5).

Lewis, Jasper↗

Optical Diagnostics for Thermal Barrier Coatings

The translucent nature of ceramic oxide thermal barrier coatings (TBCs) provides an opportunity to employ optical probes to monitor temperature gradients and buried damage propagation within the coating. An important advantage of noncontact optical diagnostics is that they are amendable to health monitoring of TBCs in service. In this paper, two optical diagnostic approaches, operating in different wavelength regimes, are discussed. The first approach is the use of mid-infrared reflectance (MIR) to monitor the progression of TBC delamination produced by thermal cycling. This approach takes advantage of the maximum transparency of the TBCs at mid-infrared wavelengths, in particular, between 3 and 5 microns. Recent progress in extending the MIR method to a more practical visual inspection tool will be presented. A second approach, using visible wavelengths, is the embedding of thermographic phosphors within the TBC to add sensing functions to the coating that can provide depth-selective information about temperature gradients and TBC integrity. Emphasis will be given to the use of fluorescence decay time measurements to provide temperature readings from a thermographic phosphor layer residing beneath the TBC.

Eldridge, J. I.↗

Ash Fouling Free Regenerative Air Preheater for Deep Cyclic Operation

The University of Kentucky (UKy) project titled “Ash Fouling Free Regenerative Air Preheater for Deep Cyclic Operation”, DE-FE0031757, was conducted from 8/15/2019 to 8/14/2024 in two Budget Periods. Other participants included PPL Corporation and Black Dragon Double Boiler. The overall goal was to investigate the proposed self-cleaning technology to achieve ash fouling free air preheater operation in a coal-fired power plant, especially during deep cycling. All project deliverables, milestones, and success criteria were met. UKy obtained the following scientific findings. • Temporary and periodic high temperature of heating elements (450 ~ 500 °F) can prevent ash accumulation and maintain air preheater free of clogging. • The ash samples analysis and unit operation provide solid evidence of ABS formed during low load with SCR ammonia slip being the major cause of ash accumulation, and air preheater clogging can be prevented by raising the heating element temperature up to 450 °F~ 500 °F at which ABS is decomposed. • In-situ self-cleaning can be controlled by monitoring temperature and/or presetting fixed number of cleanings per day. Both approaches in pilot testing show positive results for maintaining an ash free state for the air preheater. • Temperature criteria (cold end or gas outlet temperature) for entering self-cleaning service is critical to balance the number of cleaning cycles with maintaining the ash level. • Temperature criteria (cold end or gas outlet temperature) for exiting self-cleaning service is critical to balance the duration of the cleaning cycles with maintaining the ash level.

01 COAL, LIGNITE, AND PEAT↗

Controlled-Temperature Hot-Air Gun

Materials that find applications in wind tunnels first tested in laboratory. Hot-Air Gun differs from commercial units in that flow rate and temperature monitored and controlled. With typical compressed-airsupply pressure of 25 to 38 psi (170 to 260 kPa), flow rate and maximum temperature are 34 stdft3/min (0.96 stdm3/min) and 1,090 degrees F (590 degrees C), respectively. Resembling elaborate but carefully regulated hot-air gun, setup used to apply blasts of air temperatures above 1,500 degrees F (815 degrees C) to test specimens.

Munoz, M. C.↗

Performance Test of Mini LVDT - ELVIS

The Institute for Energy (IFE) Technology has been a pioneer in the development of Linear Variable Differential Transformers (LVDTs) for in-pile testing, deploying over 2,200 units in various reactor environments with less than a 10% failure rate after five years of operation. This report focuses on the performance testing of IFE’s Mini LVDT, a compact sensor ideal for material test reactor experiments. The Mini LVDT, with a limited range of +/- 1.5 mm, offers excellent performance comparable to larger LVDTs, making it valuable in space-constrained applications. The development of an Enhanced Linear Variable Intrinsic Sensor (ELVIS) with internal temperature monitoring capabilities represents a significant advancement, addressing the critical need for real-time, accurate measurements in high-radiation and high-temperature environments. Two ELVIS prototypes were evaluated in terms of both temperature and displacement, showcasing promising results, though challenges with noise during temperature measurements were identified. This report summarizes the rigorous testing performed at Idaho National Laboratory (INL) and highlights the potential applications of Mini LVDTs and ELVIS in nuclear and other high-precision industries.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Microwave sensing from orbit

Microwave sensors, used in conjunction with the traditional sensors of visible and infrared light to extend present capabilities of global weather forecasts and local storm watches, are discussed. The great advantage of these sensors is that they can penetrate or 'see' through cloud formations to monitor temperature, humidity and wind fields below the clouds. Other uses are that they can penetrate the earth deeper than optical and IR systems; they can control their own angle of incidence; they can detect oil spills; and they can enhance the studies of the upper atmosphere through measurement of temperature, water vapor and other gaseous species. Two types of microwave sensors, active and passive, are examined. Special attention is given to the study of the microwave radiometer and the corresponding temperature resolution as detected by the antenna. It is determined that not only will the microwave remote sensors save lives by allowing close monitoring of developing storms, but also save approximately $172 million/year.

Kritikos, H. N.↗

Synthesis and application of thermally responsive nanofiber coatings for overtemperature monitoring

This study presents a one-pot synthesis route to organometallic nanofibers based on copper thiolate, exhibiting distinctive chemical and physical characteristics. Electron microscopy analysis of morphology and composition revealed 2-10 μm-long, 50-90 nm-diameter hollow and non-hollow fibers composed of copper, sulfur, oxygen, hydrocarbon, and chlorine. Thermogravimetric analysis showed a pronounced mass loss within 120°C-135°C. To elucidate the thermal responsive pathways, the nanofibers were characterized before and after heating. X-ray photoelectron spectroscopy indicates that an initially mixed Cu(I)/Cu(II) oxidation states transition to predominantly Cu(I) upon heating. A layer of nanofiber was coated on battery pouch foil and evaluated as a candidate thermally sensitive coating. At elevated temperature (100-130°C), nanofiber coating released volatile organic compounds, sulfide and sulfur dioxide as detected using multiple gas sensors. This thermally responsive gas release/sensing approach provides a potential large-area temperature monitoring strategy, which is particularly relevant where direct temperature measurements of individual batteries is impractical. The results established proof of concept for nanofiber-coated battery pouch foil as overtemperature warning platform that can provide alerts when surface temperatures exceed a critical threshold. More broadly, the ability to form interconnected fiber networks positions copper thiolate nanofiber coatings as promising materials for advanced applications.

Ihala Gamaralalage, Chanaka [ORNL] (ORCID:00000002↗

Effects of rotation on impingement cooling of turbine blades

The effects of rotation on impingement cooling of turbine blades were studied experimentally as a specialized facility at M.I.T. A foil heated resistively was cooled by a jet flow on one side and temperature monitored on the other. Rotating the blade limits the heat transfer path to conduction through the support structure and radiation. IR radiometry furnishes the temperature distributions on the chamber wall, permitting the internal heat transfer coefficient to be measured. The heat transfer efficiency has been found to fall as much as 30 percent as rotational speed increases. The conditions observed confirm the significance of rotational effects, particularly with regard to potential early blade failure.

Kreatsoulas, J. C.↗

Nimbus-7 Stratospheric and Mesospheric Sounder (SAMS) experiment data user's guide

The Stratospheric and Mesospheric Sounder (SAMS) aboard Nimbus-7 observes infrared radiation from the atmospheric limb. Global upper atmosphere temperature profiles and vertical concentrations of H2O, NO, N2O, CH4 and CO2 are derived from these measurements. The status of all channels was carefully monitored. Temperature and composition were retrieved from the measurements by linearizing the direct equation about an a priori profile and using an optimum statistical estimator to find the most likely solution. The derived temperature and composition profiles are archived on two tape products whose file structure and record formats are described in detail. The gridded retrieved temperature tape (GRID-T) contains daily day and night average temperatures at 62 pressure levels in a 2.5 degree latitude by 10 degree longitude grid extending from 67.5 degrees N to 50 degrees S. The zonal mean methane and nitrous oxide composition tape (ZMT-G) contains zonal mean day and night average CH4 and N2O mixing ratios at 31 pressure levels for 2.5 degrees latitude zones extending from 67.5 degrees N to 50 degrees S.

Taylor, F. W.↗

DACS II - A distributed thermal/mechanical loads data acquisition and control system

A distributed data acquisition and control system has been developed for the NASA Flight Loads Research Facility. The DACS II system is composed of seven computer systems and four array processors configured as a main computer system, three satellite computer systems, and 13 analog input/output systems interconnected through three independent data networks. Up to three independent heating and loading tests can be run concurrently on different test articles or the entire system can be used on a single large test such as a full scale hypersonic aircraft. Thermal tests can include up to 512 independent adaptive closed loop control channels. The control system can apply up to 20 MW of heating to a test specimen while simultaneously applying independent mechanical loads. Each thermal control loop is capable of heating a structure at rates of up to 150 F per second over a temperature range of -300 to +2500 F. Up to 64 independent mechanical load profiles can be commanded along with thermal control. Up to 1280 analog inputs monitor temperature, load, displacement and strain on the test specimens with real time data displayed on up to 15 terminals as color plots and tabular data displays. System setup and operation is accomplished with interactive menu-driver displays with extensive facilities to assist the users in all phases of system operation.

Zamanzadeh, Behzad↗