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At least 91 records · Page 5

Inertial Confinement fusion targets

Inertial confinement fusion (ICF) targets are made as simple flat discs, as hollow shells or as complicated multilayer structures. Many techniques were devised for producing the targets. Glass and metal shells are made by using drop and bubble techniques. Solid hydrogen shells are also produced by adapting old methods to the solution of modern problems. Some of these techniques, problems, and solutions are discussed. In addition, the applications of many of the techniques to fabrication of ICF targets is presented.

Hendricks, C. D.↗

Radiation-Hardened GaN HEMT and Cell Design, Modeling, and Fabrication for Nuclear Instrumentation Applications

Recent advances in nuclear power generation technologies show great promise for efficient, safe generation of carbon-free power in the near future. Consequently, many new generation reactor designs are being pursued by government and industry groups, including both fission- and fusion-based technologies. Radiation- and temperature-tolerant sensor technology continues to advance, yet development of the electronics/instrumentation technologies suitable for these environments have fallen behind. Industry has adequately addressed harsh environment electronics needs for low earth orbit satellites, but the much more extreme conditions associated with electronics placed near or in a reactor core remain unaddressed. This project investigates the use of gallium nitride (GaN) circuit technology to address the unique needs for sensor interface electronics and communications in reactor environments. This report provides a summary of the first year’s project activities related to developing and optimizing devices and circuits for this GaN high electronic mobility transistor (HEMT) process. Activities reported include multiple analog and digital circuit designs simulated using custom Verilog-A models generated from measured GaN devices fabricated in the target process. Digital circuit designs included fundamental logic circuits such as an inverter, NAND, NOR, AND and OR gates, as well as a 5-stage ring oscillator. Each design was simulated using an open-source SPICE simulator, and an integrated circuit layout was produced of each design for use in future fabrication. Analog circuit designs focused on the fundamental building blocks to be used to construct sensor interface and communications circuits. These included current mirrors, matched differential pairs, and a Gilbert cell mixer design, each with an associated integrated circuit layout. Layout tools used for these designs included two open-source packages—KLayout and Magic—which were customized for specific use with the OSU GaN process layers. Design rules and preliminary device extraction capabilities were built for the Magic tool to enable device extraction and subsequent netlist generation for SPICE simulation. Finally, future research directions for year two are summarized. When the year-two directions are implemented, the project will be in position to advance the state of the art in electronics for near- or in-reactor sensor interfacing and communications.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗

Target Optimization Study: Tolerance Sensitivity

A Work Package was initiated to investigate the potential for target optimization. The current design is made up of 82 disks 0.5 mm thick spaced 0.25 mm apart for helium coolant flow. This disk thickness and gap width are a result of continual increases is beam power and hence volumetric heating rate. Thickening the disks would mean higher disk temperatures, but this would be weighed against the prospect of fewer, thicker disks and wider coolant gap spaces, and the relaxed tolerances that would result. Fabrication of the target holder would be easier and less expensive, and target assembly would also be easier.

43 PARTICLE ACCELERATORS↗

Fully Additively Manufactured Wetted Foam Capsules for Inertial Confinement Fusion

In the pursuit of realizing reliable clean energy generation via inertial confinement fusion (ICF), wetted foam (WF) capsule targets have long been coveted due to their potential to simplify the target fielding process and suppress hydrodynamic instabilities and material mixing that limit achievable energy output, yet producing and deploying a WF target has proven challenging. Here, in this work, we demonstrate the design, fabrication, metrology, and testing of fully additively manufactured (AM) foam-lined capsules using two-photon polymerization (2PP) for ICF. We successfully fielded an AM polymeric foam capsule with a 3-mm outer diameter, a nominally 15-µm-thick solid outer layer, a 120-µm-thick inner foam layer, and a 250-µm outer diameter copper fill tube on the National Ignition Facility for a polar direct-drive shot, and we showcase deuterium wetting of the capsule foam layer inside an ignition target proofing station. Our exploration showed that 2PP can produce fieldable targets with complex geometries and potentially shorten the design iteration turnaround time and the overall target fabrication time.

Target↗

Shock Initiation Microscopy with High Time and Space Resolution

In this paper, we describe studies of shock initiation and shock-to-detonation transitions in energetic materials using a tabletop shock compression microscope with nanosecond time resolution and micrometer spatial resolution. Planar input shocks with durations of 4–20 ns are produced using 0–4.5 km/s laser-launched flyer plates. Emphasis is on measurements of temperature, velocities, pressure, and microstructure using photon Doppler velocimetry (PDV), optical pyrometry and high-speed videography. Techniques are discussed for fabricating disposable shock target arrays of tiny plastic-bonded explosives (PBX), liquid and powder explosives, and single-crystal explosives for high-throughput studies. Optical temperature measurements of shocked triaminotrinitrobenzene (TATB) are discussed. Since TATB is yellow, we developed methods to correct for the blue absorption to obtain more accurate temperatures. Hot spots in shocked polymer-encased HMX (octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine) crystals are observed in real-time, showing a hot spot produced in a collapsing void that ignites a deflagration. Despite the small dimensions of our explosive charges (typically 1 mm diameter and 250 μm length), we produced reproducible detonation states in solid and liquid explosives using short-duration shocks near the von Neumann spike (VNS) pressure. We show the VNS pressure is associated with a transition to high-efficiency gas production from the explosives. In studies of NM, prior to detonation, we see reaction originating at hot spots which coalesce to form a superdetonation.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Scalable fabrication of an array-type fixed-target device for automated room temperature X-ray protein crystallography

X-ray crystallography is one of the leading tools to analyze the 3-D structure, and therefore, function of proteins and other biological macromolecules. Traditional methods of mounting individual crystals for X-ray diffraction analysis can be tedious and result in damage to fragile protein crystals. Furthermore, the advent of multi-crystal and serial crystallography methods explicitly require the mounting of larger numbers of crystals. To address this need, we have developed a device that facilitates the straightforward mounting of protein crystals for diffraction analysis, and that can be easily manufactured at scale. Inspired by grid-style devices that have been reported in the literature, we have developed an X-ray compatible microfluidic device that can be used to trap protein crystals in an array configuration, while also providing excellent optical transparency, a low X-ray background, and compatibility with the robotic sample handling and environmental controls used at synchrotron macromolecular crystallography beamlines. At the Stanford Synchrotron Radiation Lightsource (SSRL), these capabilities allow for fully remote-access data collection at controlled humidity conditions. Furthermore, we have demonstrated continuous manufacturing of these devices via roll-to-roll fabrication to enable cost-effective and efficient large-scale production.

chemical engineering↗

Artificial intelligence driven laser parameter search: Inverse design of photonic surfaces using greedy surrogate-based optimization

Photonic surfaces designed with specific optical characteristics are becoming increasingly crucial for novel energy harvesting and storage systems. The design of these surfaces can be achieved by texturing materials using lasers. The optimal adjustment of laser fabrication parameters to achieve target surface optical properties is an open challenge. Thus, we develop a surrogate-based optimization approach. Our framework employs the Random Forest algorithm to model the forward relationship between the laser fabrication parameters and the resulting optical characteristics. During the optimization process, we use a greedy, prediction-based exploration strategy that iteratively selects batches of laser parameters to be used in experimentation by minimizing the predicted discrepancy between the surrogate model’s outputs and the user-defined target optical characteristics. This strategy allows for efficient identification of optimal fabrication parameters without the need to model the error landscape directly. We demonstrate the efficiency and effectiveness of our approach on two synthetic benchmarks and two specific experimental applications of photonic surface inverse design targets. By calculating the average performance of our algorithm compared to other state of the art optimization methods, we show that our algorithm performs, on average, twice as well across all benchmarks. Additionally, a warm starting inverse design technique for changed target optical characteristics enhances the performance of the introduced approach.

97 MATHEMATICS AND COMPUTING↗

Layered Metals Fabrication Technology Development for Support of Lunar Exploration at NASA/MSFC

NASA's human exploration initiative poses great opportunity and risk for missions to the Moon and beyond. In support of these missions, engineers and scientists at the Marshall Space Flight Center are developing technologies for ground-based and in-situ fabrication capabilities utilizing provisioned and locally-refined materials. Development efforts are pushing state-of-the art fabrication technologies to support habitat structure development, tools and mechanical part fabrication, as well as repair and replacement of ground support and space mission hardware such as life support items, launch vehicle components and crew exercise equipment. This paper addresses current fabrication technologies relative to meeting targeted capabilities, near term advancement goals, and process certification of fabrication methods.

Cooper, Kenneth G.↗

Process Improvement For Pu-238 Production at Idaho National Laboratory

Idaho National Laboratory (INL) has supported the production of Pu-238 for future NASA deep space missions since 2017. Over this time, INL has worked to improve the qualification process of Pu-238 production targets as well as improve processes related to the shipping, storage, irradiation, and storage of Pu-238 production targets. Qualification of Pu-238 production targets began with flux measurements and scoping analysis to provide fundamental data to confirm the impacts on the operation of the Advanced Test Reactor (ATR), Fig1. Later, initial production targets were irradiated in ATR’s I-7 position, and then the South Flux Trap (SFT). A modified target design was then implemented which would use the full length of the ATR core and increase Pu-238 production. While working to improve and streamline the qualification of the Pu-238 production targets, INL worked to improve multiple operational aspects of the Pu-238 production process. These changes include updating procedures to streamline operations, supporting modification of shipping containers to contain five rather than one production target, reviewing target receipt procedures and changing work flow to provide flexibility in target receipt, and designing and fabricating support equipment for the storage and internal transfer of production targets

07 ISOTOPE AND RADIATION SOURCES↗

Process Improvements For Pu-238 Production at Idaho National Laboratory

Idaho National Laboratory (INL) has supported the production of Pu-238 for future NASA deep space missions since 2017. Over this time, INL has worked to improve the qualification process of Pu-238 production targets as well as improve processes related to the shipping, storage, irradiation, and storage of Pu-238 production targets. Qualification of Pu-238 production targets began with flux measurements and scoping analysis to provide fundamental data to confirm the impacts on the operation of the Advanced Test Reactor (ATR), Fig1. Later, initial production targets were irradiated in ATR’s I-7 position, and then the South Flux Trap (SFT). A modified target design was then implemented which would use the full length of the ATR core and increase Pu-238 production. While working to improve and streamline the qualification of the Pu-238 production targets, INL worked to improve multiple operational aspects of the Pu-238 production process. These changes include updating procedures to streamline operations, supporting modification of shipping containers to contain five rather than one production target, reviewing target receipt procedures and changing work flow to provide flexibility in target receipt, and designing and fabricating support equipment for the storage and internal transfer of production targets.

07 ISOTOPE AND RADIATION SOURCES↗

Mini-99 Experiment Design and Target Assembly

Qualification of nuclear fuels requires an understanding of a myriad of fuel performance variables, which requires time-consuming irradiations in test reactors. Accelerating burnup accumulation to reduce the irradiation time has historically been accomplished by increasing the 235 U enrichment in integral fuel tests, which inherently couples the fuel’s temperature and fission heat generation. Separate effects irradiation testing of nuclear fuel, using the MiniFuel target in the Oak Ridge National Laboratory’s (ORNL’s) High Flux Isotope Reactor (HFIR), offers an approach for decoupling fuel temperature and fission rate by reducing the quantity of the fuel and relying primarily on gamma heating in the surrounding components to drive fuel temperatures. However, if the fission rate is high enough, the fuel temperature will still vary over time as the fission heating changes, primarily due to poor heat conduction between the fuel and the surrounding components. This work details the design, analysis, and fabrication of a MiniFuel target which utilizes sodium bonding to improve the heat rejection from the fuel specimen, enabling the testing of higher 235 U enrichments (~8wt.%) to further accelerate burnup accumulation without prohibitively large temperature variations throughout the course of the irradiation.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Design Principles to Govern Electrode Fabrication for the Lithium Trivanadate Cathode

A full depth of discharge mathematical model for the lithium trivanadate cathode, considering lithiation of the layered α-phase, phase change, and lithiation of the rock-salt like β-phase at lower potentials, is developed. The coupled electrode-scale and crystal-scale model is fit to electrochemical data, and additionally validated with operando EDXRD. There is good agreement between the simulated and measured spatial variation of the volume fraction of the β-phase. This mathematical model is used to guide electrode fabrication, accounting for both ionic and electronic transport effects. Values of three design parameters—electrode thickness, porosity, and volume fraction of conductor—are identified, and the sensitivity of the energy density to these design parameters is quantified. The model is also used to investigate electrode design to create electrodes that deliver the maximum achievable energy density under the constraint that the α to β-phase transition is avoided, since phase change has been demonstrated to reduce cycle life. The energy density sacrificed to avoid phase change decreases at higher discharge rates, but the target values for electrode fabrication remain the same as those when optimizing the electrode for the full depth of discharge.

25 ENERGY STORAGE↗

Tether deployment monitoring system, phase 2

An operational Tether Deployment Monitoring System (TEDEMS) was constructed that would show system functionality in a terrestrial environment. The principle function of the TEDEMS system is the launching and attachment of reflective targets onto the tether during its deployment. These targets would be tracked with a radar antenna that was pointed towards the targets by a positioning system. A spring powered launcher for the targets was designed and fabricated. An instrumentation platform and launcher were also developed. These modules are relatively heavy and will influence tether deployment scenarios, unless they are released with a velocity and trajectory closely matching that of the tether. Owing to the tracking range limitations encountered during field trails of the Radar system, final TEDEMS system integration was not completed. The major module not finished was the system control computer. The lack of this device prevented any subsystem testing or field trials to be conducted. Other items only partially complete were the instrumentation platform launcher and modules and the radar target launcher. The work completed and the tests performed suggest that the proposed system continues to be a feasible approach to tether monitoring, although additional effort is still necessary to increase the range at which modules can be detected. The equipment completed and tested, to the extent stated, is available to NASA for use on any future program that requires tether tracking capability.

Source record↗

An engineering perspective on evaluating mechanisms governing ductility in pure molybdenum

The United States lacks a stable domestic supply of 99 mTc, a critical medical imaging isotope generated from 99 Mo. Accelerator-based production using 100 Mo targets (aMo) introduces mechanical concerns due to the ductile-to-brittle transition temperature inherent to refractory metals like Mo. This study evaluates the tensile behavior of aMo targets from 25 to 1000 °C, compared to powder-metallurgy-processed natural Mo (PMo) and cast-and-rolled Mo (RMo), both as-received and after 5 ppm O 2 exposure in flowing He. RMo showed superior ductility (7.3% at 25 °C, 48% at 1000 °C) and strength, attributed to its fine, elongated grains and high geometrically necessary dislocation density. PMo exhibited variable ductility (up to 33%), while aMo remained brittle, with a maximum elongation of 10.4% at 600 °C. EBSD analysis revealed weak texture in PMo and aMo, but high defect density in aMo limited dislocation mobility. This work links processing, microstructure, and deformation mechanisms to guide fabrication of ductile refractory targets.

Hyer, Holden C. [Oak Ridge National Laboratory (OR↗

Understanding Reproducibility of Sputter‐Deposited Metastable Ferroelectric Wurtzite Al 0.6 Sc 0.4 N Films Using In Situ Optical Emission Spectrometry

High‐Sc Al 1– x Sc x N thin films are of tremendous interest because of their attractive piezoelectric and ferroelectric properties, but overall film quality and reproducibility are widely reported to suffer as x increases. In this study, structural and electrical properties of metastable Al 0.6 Sc 0.4 N films are connected with plasma changes during film growth, identified via glow discharge optical emission spectroscopy (GD‐OES), and linked to the target mode changes. This in situ GD‐OES technique uses changes in the N 2 (I) intensity, correlated with DC bias hysteresis behavior of a Al 0.6 Sc 0.4 target in metallic and poisoned modes, to identify films that subsequently exhibit unacceptable structural and electrical performance. Two representative samples deposited under identical conditions but possessing distinct properties related to phases present in the films are focused on. Films sputtered under a poisoned target mode produce pure wurtzite ferroelectric Al 0.6 Sc 0.4 N with a reversible 80 μC cm −1 polarization and 3.1 MV cm −1 coercive field. When identical chamber settings are used but the process starts in metallic mode, a mixed wurtzite/rocksalt film is deposited which exhibits nanometer‐scale changes to the film microstructure and a nonferroelectric response. These results illustrate the utility of optical emission spectroscopy for tracking target mode fluctuations when fabricating metastable materials such as high‐Sc Al 1– x Sc x N films.

36 MATERIALS SCIENCE↗