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NASA NTRS1982

Homogeneous and heterogeneous condensation of nitrogen in transonic flow

Onset of both homogeneous and heterogeneous nucleation for nitrogen gas has been measured in the Langley 0.3m Transonic Cryogenic Tunnel. Homogeneous nucleation data have been taken using a DFVLR CAST-10 airfoil and are used to evaluate classical liquid droplet theory and several proposed corrections to it. A correction for differences in translational energy states between the droplet and the bulk liquid due to either Reiss (1977) or Kikuchi (1977) achieves good agreement between the predicted onset of nucleation and the data. Good agreement is also found using a Tolman constant of 0.25 x 10 to the -10th m. Onset of heterogeneous nucleation on pre-existing seed particles in the flow has also been studied, and preliminary estimates of seed size and number are 0.25 x 10 to the -6th m and 3.0 x 10 to the 12th per kilogram of the gas. It is shown that this preexisting seed population is insufficient to influence the observed onset of homogeneous nucleation.

Hall, R. M.↗

NASA NTRS1990

TiCl4 as a source of TiO2 particles for laser anemometry measurements in hot gas

A method of reacting TiCl4 with water saturated gaseous nitrogen (GN2) at the entrance into a high temperature gas flow is described. The TiO2 particles formed are then entrained in the gas flow and used as seed particles for making laser anemometry (LA) measurements of the flow velocity distribution in the hot gas. Scanning electron microscope photographs of the TiO2 particles are shown. Data rate of the LA processor was measured to determine the amount of TiO2 formed. The TiCl4 and mixing gas flow diagram is shown. This work was performed in an open jet burner.

Weikle, Donald H.↗

NASA NTRS1993

Generation of monodisperse droplets by spontaneous condensation of flow in nozzles

Submicron size monodisperse particles are of interest in many industrial and scientific applications. These include the manufacture of ceramic parts using fine ceramic particles, the production of thin films by deposition of ionized clusters, monodisperse seed particles for laser anemometry, and the study of size dependence of cluster chemical and physical properties. An inexpensive and relatively easy way to generate such particles is by utilizing the phenomenon of spontaneous condensation. The phenomenon occurs when the vapor or a mixture of a vapor and a noncondensing gas is expanded at a high expansion rate. The saturation line is crossed with the supercooled vapor behaving like a gas, until all of a sudden at the so called Wilson point, condensation occurs, resulting in a large number of relatively monodisperse droplets. The droplet size is a function of the expansion rate, inlet conditions, mass fraction of vapor, gas properties, etc. Spontaneous condensation of steam and water vapor and air mixture in a one dimensional nozzle was modeled and the resulting equations solved numerically. The droplet size distribution at the exit of various one dimensional nozzles and the flow characteristics such as pressure ratio, mean droplet radius, vapor and droplet temperatures, nucleation flux, supercooling, wetness, etc., along the axial distance were obtained. The numerical results compared very well with the available experimental data. The effect of inlet conditions, nozzle expansion rates, and vapor mass fractions on droplet mean radius, droplet size distribution, and pressure ratio were examined.

Lai, Der-Shaiun↗

NASA NTRS1987

Laser velocimetry in turbulent flow fields - Particle response

Measurements of the particle response in a decelerating flow and a highly turbulent two-phase flow were obtained. Simultaneous measurements of the particle size and velocity served to quantify the particle response to the prevailing flow field. In the case of a flow incident upon a cylinder, the particle lag for a range of size classes was recorded. Results were also obtained in the flow generated by an atomizer operating on the leeward side of a flat disk bluff body in a coflowing air stream. Measurements of the mean axial, mean radial, and rms velocities and angles of trajectories were obtained for representative particle size classes. The air velocity and turbulence intensity were inferred from the seed particles on the order of one micrometer in diameter. Particles 9 micrometers and larger showed significant differences with respect to the gas phase mean velocity and turbulence intensity even at low velocities. In two-phase flows, reliable measurements of the continuous phase velocity and turbulence parameters requires the simultaneous measurement of particle size as a means for rejecting readings from large particles from the velocity pdf's.

Bachalo, W. D.↗

NASA NTRS2001

Three-Dimensional Stereoscopic Tracking Velocimetry and Experimental/Numerical Comparison of Directional Solidification

Measurement of three-dimensional (3-D) three-component velocity fields is of great importance in both ground and space experiments for understanding materials processing and fluid physics. The experiments in these fields most likely inhibit the application of conventional planar probes for observing 3-D phenomena. Here, we present the investigation results of stereoscopic tracking velocimetry (STV) for measuring 3-D velocity fields, which include diagnostic technology development, experimental velocity measurement, and comparison with analytical and numerical computation. STV is advantageous in system simplicity for building compact hardware and in software efficiency for continual near-real-time monitoring. It has great freedom in illuminating and observing volumetric fields from arbitrary directions. STV is based on stereoscopic observation of particles-Seeded in a flow by CCD sensors. In the approach, part of the individual particle images that provide data points is likely to be lost or cause errors when their images overlap and crisscross each other especially under a high particle density. In order to maximize the valid recovery of data points, neural networks are implemented for these two important processes. For the step of particle overlap decomposition, the back propagation neural network is utilized because of its ability in pattern recognition with pertinent particle image feature parameters. For the step of particle tracking, the Hopfield neural network is employed to find appropriate particle tracks based on global optimization. Our investigation indicates that the neural networks are very efficient and useful for stereoscopically tracking particles. As an initial assessment of the diagnostic technology performance, laminar water jets with and without pulsation are measured. The jet tip velocity profiles are in good agreement with analytical predictions. Finally, for testing in material processing applications, a simple directional solidification apparatus is built for experimenting with a metal analog of succinonitrile. Its 3-D velocity field at the liquid phase is then measured to be compared with those from numerical computation. Our theoretical, numerical, and experimental investigations have proven STV to be a viable candidate for reliably measuring 3-D flow velocities. With current activities are focused on further improving the processing efficiency, overall accuracy, and automation, the eventual efforts of broad experimental applications and concurrent numerical modeling validation will be vital to many areas in fluid flow and materials processing.

Lee, David↗

NASA NTRS1991

Digital Image Velocimetry

Digital image velocimetry is technique for extracting two-dimensional (in image planes) velocities of objects from multiple photographs or video images of objects. Devised to overcome disadvantages of particle-image velocimetry and laser-speckle velocimetry, both of which involve use of illuminated seed particles to make flows visible. Directions of velocity vectors determined unambiguously, and dynamic range limited only by speed of camera or, equivalently, by speed of stroboscopic illumination.

Cho, Y.-C.↗

NASA NTRS1980

New methods to detect particle velocity and mass flux in arc-heated ablation/erosion facilities

Arc-heated flow facilities with injected particles are used to simulate the erosive and ablative/erosive environments encountered by spacecraft re-entry through fog, clouds, thermo-nuclear explosions, etc. Two newly developed particle diagnostic techniques used to calibrate these facilities are discussed. One technique measures particle velocity and is based on the detection of thermal radiation and/or chemiluminescence from the hot seed particles in a model ablation/erosion facility. The second technique measures a local particle rate, which is proportional to local particle mass flux, in a dust erosion facility by photodetecting and counting the interruptions of a focused laser beam by individual particles.

Brayton, D. B.↗

NASA NTRS1985

Measurements in the flow field of a cylinder with a laser transit anemometer and a drag rake in the Langley 0.3 m transonic cryogenic tunnel

An experiment was conducted at the 0.3 m Transonic Cryogenic Tunnel using a Laser Transit Anemometer (LTA) to probe the flow field around a 3.05 centimeter-diameter circular cylinder. Measurements were made along the stagnation line and determination of particle size was evaluated by their ability to follow the flow field. The LTA system was also used to scan into the boundary layer near the 45 degree point on the model. Results of these scans are presented in graphic and tabular form. Flow field particle seeding was accomplished by inbleeding dry service air. The residual moisture (5-10 ppm) condensed and formed ice particles which served as Mie scattering centers for the LTA detection system. Comparison of data taken along the stagnation streamline with theory indicated that these particles tracked the velocity gradient of the flow. Tunnel operating conditions for the tests were a Mach number of 0.3, a pressure of 1.93 x 100000 n/m squared, and a temperature of 225 degrees K. Free stream Mach number and pressure were varied for the particle size determination.

Honaker, W. C.↗

NASA NTRS1987

The role of photographic parameters in laser speckle or particle image displacement velocimetry

The parameters involved in obtaining the multiple exposure photographs in the laser speckle velocimetry method (to record the light scattering by the seeding particles) were optimized. The effects of the type, concentration, and dimensions of the tracer, the exposure conditions (time between exposures, exposure time, and number of exposures), and the sensitivity and resolution of the film on the quality of the final results were investigated, photographing an experimental flow behind an impulsively started circular cylinder. The velocity data were acquired by digital processing of Young's fringes, produced by point-by-point scanning of a photographic negative. Using the optimal photographing conditions, the errors involved in the estimation of the fringe angle and spacing were of the order of 1 percent for the spacing and +/1 deg for the fringe orientation. The resulting accuracy in the velocity was of the order of 2-3 percent of the maximum velocity in the field.

Lourenco, L.↗

NASA NTRS1985

Estimation of particle size based on LDV measurements in a de-accelerating flow field

The accuracy of velocity measurements made with a laser velocimeter is strongly dependent upon the response of the seeding particles to the dynamics of the flow field. The smaller the particle the better the response to flow fluctuations and gradients and therefore the more accurate velocity measurement. In direct conflict is the requirement of light scattering efficiency to obtain signals with the laser velocimeter which, in general, is better as the particle size is increased. In low speed flow fields these two requirements on particle size overlap and accurate measurements may be obtained. However in high speed flows, where the velocity gradients may be severe, very small particles are required to maintain sufficient dynamic response characteristics to follow the flow. Therefore if velocity measurements are to be made in these flows, the laser velocimeter must be designed with sufficient sensitivity to obtain signals from these small particles. An insitu determination of the size distribution of kaolin particles (Al2O3, .2 + or - SiO2 . 2H2O) in the 16-foot Transonic Tunnel and the sensitivity characteristics of the laser velocimeter system is described.

Meyers, J. F.↗

NASA NTRS1990

Particle image fields and partial coherence

The accuracy of Young's fringe method for reducing velocity field data is compromized by a spatially incoherent background field which originates in the random locations of the seeding particles. The probability density function for the spatial frequency cutoff of this background is derived as a function of the particle count, the distribution governing the power in each frequency interval is derived, and conditions are found under which the Van Cittert-Zernike theorem applies. The background field resembles the far field of a partially coherent source in the high particle count limit, but departs significantly at low and moderate counts.

Rubinstein, Robert↗

NASA NTRS1992

Full field flow visualization and computer-aided velocity measurements in a bank of cylinders in a wind tunnel

The full field flow tracking (FFFT) method that is presented in this paper uses a laser-generated, mechanically strobed planar sheet of light, a low luminosity TV camera coupled with a long distance microscope, and a computer-controlled video recorder to study nonintrusively and qualitatively the flow structures in a bank of cylinders that are placed in a wind tunnel. This setup simulates an upscale version of the geometry of internal cooling passageways characteristic of small air-cooled radial turbines. The qualitative images supplied by the FFFT system are processed by means of a computer-integrated image quantification (CIIQ) method into quantitative information, trajectories and velocities, that describe the flow upstream of and within the bank of cylinders. The tracking method is Lagrangian in concept, and permits identification and tracking of the same particle, thus facilitating construction of time dependent trajectories and the calculation of true velocities and accelerations. The error analysis evaluates the accuracy with which the seed particles follow the flow and the errors incurred during the quantitative processing of the raw data derived from the FFFT/CIIQ method.

Braun, M. J.↗

NASA NTRS1982

Capacitively-Heated Fluidized Bed

Fluidized-bed chamber in which particles in bed are capacitively heated produces high yields of polycrystalline silicon for semiconductor devices. Deposition of unrecoverable silicon on chamber wall is reduced, and amount of recoverable silicon depositing on seed particles in bed is increased. Particles also have a size and density suitable for direct handling without consolidation, unlike silicon dust produced in heated-wall chambers.

Mchale, E. J.↗

NASA NTRS2010

Optical Characterization of a Multipoint Lean Direct Injector for Gas Turbine Combustors: Velocity and Fuel Drop Size Measurements

Performance of a multipoint, lean direct injection (MP-LDI) strategy for low emission aero-propulsion systems has been tested in a Jet-A fueled, lean flame tube combustion rig. Operating conditions for the series of tests included inlet air temperatures between 672 and 828 K, pressures between 1034 and 1379 kPa and total equivalence ratios between 0.41 and 0.45, resulting in equilibrium flame temperatures approaching 1800 K. Ranges of operation were selected to represent the spectrum of subsonic and supersonic flight conditions projected for the next-generation of commercial aircraft. This document reports laser-based measurements of in situ fuel velocities and fuel drop sizes for the NASA 9-point LDI hardware arranged in a 3 3 square grid configuration. Data obtained represent a region of the flame tube combustor with optical access that extends 38.1-mm downstream of the fuel injection site. All data were obtained within reacting flows, without particle seeding. Two diagnostic methods were employed to evaluate the resulting flow path. Three-component velocity fields have been captured using phase Doppler interferometry (PDI), and two-component velocity distributions using planar particle image velocimetry (PIV). Data from these techniques have also offered insight into fuel drop size and distribution, fuel injector spray angle and pattern, turbulence intensity, degree of vaporization and extent of reaction. This research serves to characterize operation of the baseline NASA 9- point LDI strategy for potential use in future gas-turbine combustor applications. An additional motive is the compilation of a comprehensive database to facilitate understanding of combustor fuel injector aerodynamics and fuel vaporization processes, which in turn may be used to validate computational fluid dynamics codes, such as the National Combustor Code (NCC), among others.

Heath, Christopher M.↗

NASA NTRS1985

Seeding requirements for scanning laser velocimetry

To measure the velocity distributions within time dependent turbulent flow fields, a continuously scanning laser velocimeter system is being developed at Sandia National Laboratories Livermore (SNLL). A prototype of this system has produced results which show that spatial and temporal variations in particle seed distribution seriously compromise the overall performance and operation of this device. To alleviate some of these problems, alternate flow seeding concepts are explored. The most promising appear to be those that actively induce laser sparks within the gas flow, the velocity of which may be measured by a Fourier transformed velocimetry system.

Hackett, C. E.↗

NASA NTRS1981

Fluidized bed heating process and apparatus

Capacitive electrical heating of a fluidized bed enables the individual solid particles within the bed to constitute the hottest portion thereof. This effect is achieved by applying an A. C. voltage potential between dielectric coated electrodes, one of which is advantageously the wall of the fluidized bed rejection zone, sufficient to create electrical currents in said particles so as to dissipate heat therein. In the decomposition of silane or halosilanes in a fluidized bed reaction zone, such heating enhances the desired deposition of silicon product on the surface of the seed particles within the fluidized bed and minimizes undesired coating of silicon on the wall of the reaction zone and the homogeneous formation of fine silicon powder within said zone.

McHale, Edward J.↗

NASA NTRS2012

Multi-Component, Multi-Point Interferometric Rayleigh/Mie Doppler Velocimeter

An interferometric Rayleigh scattering system was developed to enable the measurement of multiple, orthogonal velocity components at several points within very-high-speed or high-temperature flows. The velocity of a gaseous flow can be optically measured by sending laser light into the gas flow, and then measuring the scattered light signal that is returned from matter within the flow. Scattering can arise from either gas molecules within the flow itself, known as Rayleigh scattering, or from particles within the flow, known as Mie scattering. Measuring Mie scattering is the basis of all commercial laser Doppler and particle imaging velocimetry systems, but particle seeding is problematic when measuring high-speed and high-temperature flows. The velocimeter is designed to measure the Doppler shift from only Rayleigh scattering, and does not require, but can also measure, particles within the flow. The system combines a direct-view, large-optic interferometric setup that calculates the Doppler shift from fringe patterns collected with a digital camera, and a subsystem to capture and re-circulate scattered light to maximize signal density. By measuring two orthogonal components of the velocity at multiple positions in the flow volume, the accuracy and usefulness of the flow measurement increase significantly over single or nonorthogonal component approaches.

Danehy, Paul M.↗

NASA NTRS1991

Aerosol reactor production of uniform submicron powders

A method of producing submicron nonagglomerated particles in a single stage reactor includes introducing a reactant or mixture of reactants at one end while varying the temperature along the reactor to initiate reactions at a low rate. As homogeneously small numbers of seed particles generated in the initial section of the reactor progress through the reactor, the reaction is gradually accelerated through programmed increases in temperature along the length of the reactor to promote particle growth by chemical vapor deposition while minimizing agglomerate formation by maintaining a sufficiently low number concentration of particles in the reactor such that coagulation is inhibited within the residence time of particles in the reactor. The maximum temperature and minimum residence time is defined by a combination of temperature and residence time that is necessary to bring the reaction to completion. In one embodiment, electronic grade silane and high purity nitrogen are introduced into the reactor and temperatures of approximately 770.degree. K. to 1550.degree. K. are employed. In another embodiment silane and ammonia are employed at temperatures from 750.degree. K. to 1800.degree. K.

Flagan, Richard C.↗