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NASA NTRS1973

A local eddy viscosity model for turbulent shear flow

In the model described, the eddy viscosity is assumed to be a fluid property dependent on the state of the fluid locally, namely the local density, turbulent kinetic energy, turbulence scale, and Mach number. An empirical law was found which related eddy viscosity to these properties satisfactorily for free jets. This law is used without modification for a set of test cases in free shear layers, free-jet decay, coaxial mixing, and wakes. The scale of turbulence is taken as a constant at any axial location equal to the width of the shear layer. By utilizing the boundary-layer order-of-magnitude analysis, a coupled set of fluid dynamic equations is formulated, which of necessity includes the equation for the production of turbulent kinetic energy.

Ortwerth, P. J.↗
NASA NTRS1979

Lubricant limiting shear stress effect on EHD film thickness

A Grubin-like EHD inlet analysis utilizing a non-linear viscous fluid model with a limiting shear stress is reported. The shear rheological equation requirs only a low shear stress viscosity and the limiting shear stress both functions of pressure. Values employed for these properties are taken from measurements on typical lubricants. Reductions of EHD film thickness are found to be up to 40 percent compared with the standard Grubin prediction for typical operating conditions. Slide-roll ratio, limiting shear stress dependence on pressure, and atmospheric pressure value of limiting shear stress are new variables required to determine film thickness with the first two being more important than the last. The EHD film thickness is reduced by increasing slide-roll ratio and/or decreasing the pressure dependence of the limiting shear stress.

Gecim, B.↗
NASA NTRS2003

Mechanisms for the Crystallization of ZBLAN

The objective of this ground based study is to test the hypothesis that shear thinning (the non-Newtonian response of viscosity to shear rate) is a viable mechanism to explain the observation of enhanced glass formation in numerous low-g experiments. In 1-g, fluid motion results from buoyancy forces and surface tension driven convection. This fluid flow will introduce shear in undercooled liquids in 1-g. In low-g it is known that fluid flows are greatly reduced so that the shear rate in fluids can be extremely low. It is believed that some fluids may have weak structure in the absence of flow. Very small shear rates could cause this structure to collapse in response to shear resulting in a lowering of the viscosity of the fluid. The hypothesis of this research is that: Shear thinning in undercooled liquids decreases the viscosity, increasing the rate of nucleation and crystallization of glass forming melts. Shear in the melt can be reduced in low-g, thus enhancing undercooling and glass formation. The viscosity of a model glass (lithium di-silicate, L2S) often used for crystallization studies has been measured at very low shear rates using a dynamic mechanical thermal analyzer. Our results are consistent with increasing viscosity with a lowering of shear rates. The viscosity of L2S may vary as much as an order of magnitude depending on the shear rate in the temperature region of maximum nucleation and crystal growth. Classical equations for nucleation and crystal growth rates, are inversely related to the viscosity and viscosity to the third power respectively. An order of magnitude variation in viscosity (with shear) at a given temperature would have dramatic effects on glass crystallization Crystallization studies with the heavy metal fluoride glass ZBLAN (ZrF2-BaF2-LaF3-AlF3-NaF) to examine the effect of shear on crystallization are being initiated. Samples are to be melted and quenched under quiescent conditions at different shear rates to determine the effect on crystallization. The results from this study are expected to advance the current scientific understanding of glass formation in low-g and glass crystallization under glass molding conditions and will improve the scientific understanding of technological processes such as fiber pulling, bulk amorphous alloys, and glass fabrication processes.

Ethridge, Edwin C.↗
NASA NTRS1973

Characteristics of a gelled liquid hyprogen polyphenylene oxide (PPO) foam open-cell insulation system, phase 1

A large scale gel production and storage facility and a small scale facility, the latter used for detailed visual examination of the gel/PPO foam interface, were developed. A subcontract was given to investigate techniques for the production of gelled liquid hydrogen, develop a process design for scale-up to a 1.89 cu m (500 gallon) gel production and storage facility, determine gel transfer characteristics, determine the solubility rate of gaseous helium in the gel, and investigate the gross gel/PPO foam interfacial phenomena. An inside-tank process for scaled-up production of gelled liquid hydrogen was selected. No detectable gel structure degradation occurred during repeated shearing. The viscosity of gelled liquid hydrogen at shear rates of 300/sec and higher is 2 to 5-fold greater than that of neat liquid hydrogen. No clogging problems were encountered during the transfer of gelled liquid hydrogen through warmed transfer lines. The solubility rate of helium in liquid hydrogen was significantly reduced by the presence of gel structure. The boil-off rates from gelled liquid hydrogen were reduced from 25 to 50 percent compared to those observed for the neat liquid hydrogen under compatible conditions. The polyphenylene oxide (PPO) foam insulation was found to be compatible with liquid ethane.

Source record↗
NASA NTRS2006

Computer Modeling of Thermal Convection in Melts to Explain Glass Formation in Low Gravity and on Earth

Experiments conducted up to this time on glass forming melts in the low gravity environment of space show that glasses prepared in low-g are more chemically homogeneous and more resistant to crystallization than the comparable glasses prepared at 1-g on Earth. This result is somewhat surprising and opposite to the accepted concept on glass formation for a melt. A hypothesis based on "shear thinning" of a melt, a decrease in viscosity with increasing shear stress, is proposed as an explanation for the observed low-gravity results. This paper describes detailed simulation procedures to test the role of thermal convection in introducing shear stress in glass forming melts, using a lithium disilcate melt as a model. The simulation system in its idealized version consists of a cylinder that is heated at one end and cooled at the other with gravity acting in a transverse direction to the thermal gradient. The side wall of the cylinder is assumed to be insulating. The governing equations of motion and energy are solved using variable properties for viscosity (Arrehenius and non-Arrehenius behaviors) and density (constant and temperature dependent). Other parametric variables in the calculations include gravity level and gravity vector orientation. The shear stress in the system are then computed as a function of gravity from the calculated values of maximum melt velocity, and its effect on melt viscosity (shear thinning) is predicted. Also included and discussed are the modeling efforts related to other potential convective processes in glass forming melts and their possible effects on melt viscosity.

Ray, Chandra S.↗
NASA NTRS1981

Rheological behavior of progressively shear-thickening solutions

The rheological behavior of the recently developed polymer FM-9 in Jet A fuel and JP 8 fuel is reported. In aqueous solution, FM 9 is found to exhibit strong time-dependent shear thickening behavior. Induction time necessary for the onset of thickening is found to depend on shear rate, solvent, concentration, and molecular weight. Altering the nature of the solvent results in effects similar to those obtained by changing the concentration or molecular weight. A critical shear rate is derived, and is inversely proportional to the zero shear rate viscosity of the solution for the temperature and concentrations observed. The onset of shear thickening behavior appears to be related to the onset of viscoelastic response, and thus the time scale follows reduced variable behavior.

Peng, S. T. J.↗
NASA NTRS1985

Measurement and correlation of jet fuel viscosities at low temperatures

Apparatus and procedures were developed to measure jet fuel viscosity for eight current and future jet fuels at temperatures from ambient to near -60 C by shear viscometry. Viscosity data showed good reproducibility even at temperatures a few degrees below the measured freezing point. The viscosity-temperature relationship could be correlated by two linear segments when plotted as a standard log-log type representation (ASTM D 341). At high temperatures, the viscosity-temperature slope is low. At low temperatures, where wax precipitation is significant, the slope is higher. The breakpoint between temperature regions is the filter flow temperature, a fuel characteristic approximated by the freezing point. A generalization of the representation for the eight experimental fuels provided a predictive correlation for low-temperature viscosity, considered sufficiently accurate for many design or performance calculations.

Schruben, D. L.↗
NASA NTRS1978

Surface temperatures and glassy state investigations in tribology, part 1

The research in this report is divided into two categories: (1) lubricant rheological behavior, and (2) thermal behavior of a simulated elastohydrodynamic contact. The studies of the lubricant rheological behavior consists of high pressure, low shear rate viscosity measurements, viscoelastic transition measurements, by volume dilatometry, dielectric transitions at atmospheric pressure and light scattering transitions. Lubricant shear stress-strain behavior in the amorphous glassy state was measured on several fluids. It appears clear from these investigations that many lubricants undergo viscoplastic transitions in typical EHD contacts and that the lubricant has a limiting maximum shear stress it can support which in turn will determine the traction in the contact except in cases of very low slide-roll ratio. Surface temperature measurements were made for a naphthenic mineral oil and a polyphenyl ether. The maximum surface temperature in these experiments was approximately symmetrical about the zero slide-roll ration except for absolute values of slide-roll ratio greater than about 0.9. Additional surface temperature measurements were made in contacts with rough surfaces where the composite surface roughness was approximately equal to the EHD film thickness. A regression analysis was done to obtain a predictive equation for surface temperatures as a function of pressure, sliding speed, and surface roughness. A correction factor for surface roughness effects to the typical flash temperature analysis was found.

Winer, W. O.↗
NASA NTRS1981

Some observations in high pressure rheology of lubricants

Experimental data are presented on viscosity, elastic shear modulus, and limiting shear stress of 12 liquid lubricants. It is shown that transition histories do affect the limiting shear stress of the materials in the form of isothermal compression resulting in a lower density and lower limiting stress than isobaric cooling. The measured limiting shear stress agrees with EHD traction data at slide-to-roll ratios of 0.1 or more. In pressure viscosity measurements of the polymer solutions, it is found that for some temperatures, the pressure viscosity coefficient of the blend is slightly less than that of the base, which results in the crossing of the viscosity-pressure isotherms at high pressures.

Bair, S.↗
NASA NTRS1982

Surface temperatures and glassy state investigations in tribology, part 5

Preliminary measurements of high shear rate viscosity at near atmospheric but variable pressure suggest the importance of low normal stress and cavitation or fluid fracture in the type of stress field existing in elastohydrodynam ic inlets and classical hydrodynamic configurations. An experimental basis is given for three regimes of traction in concentrated contacts: a thin film regime characterized by high traction and determined by lambda ratio, a thick film regime characterized by low traction and determined by the speed parameter, and the elastohydrodynamic regime for which traction is controlled by limiting shear stress. Traction measurements were performed with various liquids, two solid lubricants, and a grease. Film thickness and traction measurements of polymer blends and base oils are compared.

Bair, S.↗
NASA NTRS1983

Particle size effects on viscosity of silver pastes: A manufacturer's view

Particles from a variety of silver powders were investigated by scanning electron microscopy and particle size analyses. Particle size distribution curves and volume population graphs were prepared for these silver powders and for glass powders with optimum, extra fine and coarse particle sizes. The viscosity at a given shear rate and slope of viscosity over a range of shear rates were determined for thick film pastes made with these powders. Because of particle anomalies and variations, the need for flexibility to achieve the best printing qualities for silver pastes was evident. It was established that print quality, dried and fired film density and optimum contact of silver particles with silicon, important for cell electrical output, could be achieved by adjusting the slope of viscosity that fell outside of the range, -0.550 to -0.650. This was accomplished through organic vehicle technology that permitted a change in the slope of viscosity, up or down, while maintaining a constant silver and total solids content.

Provance, J.↗
NASA NTRS1972

Torque on a sphere inside a rotating cylinder.

A circular cylinder of finite dimensions is made to rotate around a sphere fixed in the center of the cylinder. The couple on the sphere is measured over a wide range of rotational speeds for both Newtonian and non-Newtonian fluids. For the Newtonian liquids a comparison of the experimental results is made with Collins' (1955) expansion of the couple as a series in even powers of the angular Reynolds number. For non-Newtonian liquids the apparatus proves to be extremely useful for an accurate determination of the zero shear rate viscosity using only a small amount of fluid.

Mena, B.↗
NASA NTRS1982

Capillary rheometry for thermosets

Capillary rheometry is effectively used with thermosets. Most important is providing a uniform temperature in the barrel. This was successfully accomplished by using a circulating hot oil system. Standard capillary rheometry methods provide the dependence of thermoset apparent viscosity on shear rate, temperature and time. Such information is very useful in evaluating resin processability and in setting preliminary fabrication conditions.

Malguarnera, S. C.↗
NASA NTRS1984

An investigation into the injection molding of PMR-15 polyimide

The chemorheological behavior of the PRM-15 molding compounds were characterized, the range of suitable processing parameters for injection molding in a reciprocating screw injection molding machine was determined, and the effects of the injection molding processing parameters on the mechanical properties of molded PMR-15 parts were studied. The apparatus and procedures for measuring viscosity and for determining the physical response of the material during heating are described. Results show that capillary rheometry can be effectively used with thermosets if the equipment is designed to overcome some of the inherent problems of these materials. A uniform temperature was provided in the barrel by using a circulating hot oil system. Standard capillary rheometry methods can provide the dependence of thermoset apparent viscosity on shear rate, temperature, and time. Process conditions resulting in complete imidization should be carefully defined. Specification of controlled oven temperature is inadequate and can result in incomplete imidization. For completely imidized PMR-15 heat at 15 C/min melt flow without gas evolution occurs in the temperature range of 325 C to 400 C.

Colaluca, M. A.↗
NASA NTRS1989

Three-dimensional application of the Johnson-King turbulence model for a boundary-layer direct method

The Johnson-King turbulence model as extended to three-dimensional flows was evaluated using finite-difference boundary-layer direct method. Calculations were compared against the experimental data of the well-known Berg-Elsenaar incompressible flow over an infinite swept-wing. The Johnson-King model, which includes the nonequilibrium effects in a developing turbulent boundary-layer, was found to significantly improve the predictive quality of a direct boundary-layer method. The improvement was especially visible in the computations with increased three-dimensionality of the mean flow, larger integral parameters, and decreasing eddy-viscosity and shear stress magnitudes in the streamwise direction; all in better agreement with the experiment than simple mixing-length methods.

Kavsaoglu, Mehmet S.↗