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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 91 records · Page 5
All sourcesNASA NTRSDOE OSTI
DOE OSTI2022

Nano-FTIR Investigation of the CM Chondrite Allan Hills 83100

Mid-infrared (MIR) spectroscopy has been used with great success to quantitatively determine the mineralogy of geologic samples. It has been employed in a variety of contexts from determining bulk composition of powdered samples to spectroscopic imaging of rock thin sections via micro-Fourier transform infrared (micro-FTIR) imaging spectroscopy. Recent advances allow for IR measurements at the nanoscale. Near field nanoscale infrared imaging and spectroscopy with a broadband source (nano-FTIR) enable understanding of the spatial relationships between compositionally distinct materials within a sample. This will be of particular use when analyzing returned samples from Bennu and Ryugu, which are thought to be compositionally like CI or CM1/2 carbonaceous chondrites. Returned samples will likely contain olivine/pyroxene chondrules that have been transformed into hydrous phyllosilicates, sulfides, carbonates, and other alteration phases. The use of near-field infrared techniques to probe the boundaries between once pristine chondrules and alteration phases at the nanoscale is a novel approach to furthering our understanding of the compositional evolution of carbonaceous asteroids and the processes that drive their evolution. Here we report the results of nano-FTIR spectroscopy and imaging measurements performed on the carbonaceous chondrite Allan Hills (ALH) 83100 (CM1/2). We show with nanoscale resolution that spatially resolved Fe-Mg variations exist within the phyllosilicates around a chondrule rim. We also present effects of crystal orientation on the nano-FTIR spectra to account for the spectral differences between the meteorite and mineral spectra.

58 GEOSCIENCES↗
DOE OSTI2021

Research on Chemically Deuterated Cellulose Macroperformance and Fast Identification

Chemically deuterated cellulose fiber was expected to provide novel applications due to its spectral, biological, and kinetic isotope effect. In this research, the performance of the chemically deuterated cotton fibers, including their mechanical property, enzymatic degradation performance, effect on bacterial treatment, and fast identification (near-infrared modeling) was investigated. The breaking tenacity of the deuterated cotton fibers was slightly lower, which might be attributed to the structural damage during the chemical deuteration. The glucose yield by enzymatic hydrolysis was less than that of the protonic cotton fibers, implying the deuterated fibers are less sensitive to enzymatic degradation. Furthermore, the deuterated fibers could promote the growth of bacteria such as Escherichia. coli, which was associated with the released low-level deuterium content. At last, the near-infrared technique combined with partial least squares regression successfully achieved a fast identification of the protiated and deuterated cotton fibers, which significantly promoted the potential application of deuterated cellulose as anticounterfeiting materials (e.g., special paper).

59 BASIC BIOLOGICAL SCIENCES↗
DOE OSTI2021

Structural, Thermal, and Mechanical Characterization of a Thermally Conductive Polymer Composite for Heat Exchanger Applications

Polymer composites are being considered for numerous thermal applications because of their inherent benefits, such as light weight, corrosion resistance, and reduced cost. In this work, the microstructural, thermal, and mechanical properties of a 3D printed polymer composite with high thermal conductivity are examined using multiple characterization techniques. Infrared spectroscopy and X-ray diffraction reveal that the composite contains a polyphenylene sulfide matrix with graphitic fillers, which is responsible for the high thermal conductivity. Furthermore, differential scanning calorimetry determines that the glass transition and melting point of the composite are 87.6 °C and 285.6 °C, respectively. Thermogravimetric analysis reveals that the composite is thermally stable up to ~400 °C. Creep tests are performed at different isotherms to evaluate the long-term performance of the composite. The creep result indicates that the composite can maintain mechanical integrity when used below its glass transition temperature. Nanoindentation tests reveal that modulus and hardness of the composite is not significantly influenced by heating or creep conditions. These findings indicate that the composite is potentially suitable for heat exchanger applications.

36 MATERIALS SCIENCE↗
NASA NTRS1972

Enhanced Lamb dip for absolute laser frequency stabilization

Enhanced Lamb dip width is 5 MHz and total depth is 10 percent of peak power. Present configuration is useful as frequency standard in near infrared. Technique extends to other lasers, for which low pressure narrow linewidth gain tubes can be constructed.

Siegman, A. E.↗
NASA NTRS1969

Additional line of sight methodology to that presented by John W. Strohbehn in the use of line of sight microwave propagation in remote atmospheric probing

Some additional microwave and infrared techniques are reported which are being tested in line-of-sight tropospheric scattering. Newly measured parameters of the incoherent scattered microwave field are sensitive to wavefront sphericity, to wind speed, and to the eddy wavenumber spectrum. A recommendation for advancing the state of the art is given by a proposed experimental program.

Beard, C. I.↗
NASA NTRS1975

Investigations of lubricant rheology as applied to elastohydrodynamic lubrication

Traction prediction in sliding elastohydrodynamic (EHD) contacts was examined along with an elastohydrodynamic lubrication simulation of the effects of load and speed on temperatures in the EHD contact. An existing shear stress theory and lubricant rheological model were studied and evaluated by applying them to traction prediction. Results obtained using measured film thickness and surface temperature data, were compared with measured traction values. The infrared technique for measuring temperatures in an EHD contact was further developed and ball surface and fluid temperatures are reported for sliding speeds of 0.35 to 5.08 m/s at 0.52 to 2.03 GN/sq m maximum pressure and surface roughnesses of .011 to .381 micrometers c.1.a. The relationship between asperity interaction, as measured by relocation surface profilimetry and high frequency temperature measurements, and the ratio of film thickness to surface roughness was also studied.

Kunz, R. K.↗
NASA NTRS1976

Effects of load, speed, and surface roughness on sliding EHD contact temperatures

An infrared technique has been used to determine the effects of load, speed and surface roughness on temperature in a sliding elastohydrodynamic (EHD) point contact. Ball surface temperatures are reported for sliding speeds of 0.35 to 5.08 m/s at 0.52 to 2.03 GN/per sq m maximum pressure with surface roughness in the range 0.01 to 0.38 micron c.l.a. The relationship between asperity interaction, as measured by relocation surface profilimetry and high frequency temperature measurements, and the ratio of film thickness to surface roughness has also been studied.

Nagaraj, H. S.↗
NASA NTRS1977

A gas filter correlation monitor for CO, CH4, and HCl

A fast response instrument for monitoring the atmospheric constituents CO, CH4, and HCl, using a modified nondispersive infrared technique, was designed, assembled, and tested. This gas filter correlation method uses a sample of gas to provide a selective filter for radiation absorbed in a gas mixture containing the specified gas. Depending on the spectral line broadening, temperature, and optical depth of the gas selected, exceptionally high spectral resolution may be attained. A description of the single beam rotating cell system and its specific application is presented along with the signal processing circuit. Calibrations of the instrument show that the technique can be used to measure CO, CH4, and HCl concentrations as small as 5 ppm-m. A field version was employed to measure diurnal variations of CO and CH4 and the interfering effects of other atmospheric gases were analyzed.

Sebacher, D. I.↗
NASA NTRS1978

A Multi-Band Far-Infrared Survey with a Balloon-Borne Telescope

Nine additional radiation sources, above a 3-sigma confidence level of 1300 Jy, were identified at 100 microns by far infrared photometry of the galactic plane using a 0.4 meter aperture, liquid helium cooled, multichannel far infrared balloon-borne telescope. The instrument is described, including its electronics, pointing and suspension systems, and ground support equipment. Testing procedures and flight staging are discussed along with the reduction and analysis of the data acquired. The history of infrared astronomy is reviewed. General infrared techniques and the concerns of balloon astronomers are explored.

Jacobson, M. R.↗
NASA NTRS1978

The Chesapeake Bay: A challenge to the remote sensing community

The use of remote sensing in studying, monitoring, and understanding the Chesapeake Bay was examined. References to multispectral scanning, laser techniques, infrared microwave, and radar were made. These aspects were then analyzed with multidimensional models, digital analysis, and holographic projections.

James, C. E.↗
NASA NTRS1978

Surface temperature measurements in rolling and sliding EHD contacts

In this study, moving surface temperature measurements in rolling and sliding EHD point contacts were made using an available infrared technique. Film thickness and traction have also been measured. Slide-to-roll ratios of -2 to +2 have been studied. By using a different kinematic configuration, stationary surface temperatures have also been measured. It has been shown that, while surface temperature rises in the low slip region are relatively small, stationary surface temperatures are significantly higher than the moving surface temperatures. Flash temperature theory has been extended to cover the combined rolling and sliding conditions. Correlation between the predicted and the measured values has also been performed.

Nagaraj, H. S.↗
NASA NTRS1978

A gas filter correlation analyzer for methane

A fast-response instrument for monitoring CH4 was designed and tested using a modified nondispersive infrared technique. An analysis of the single-beam rotating-cell system is presented along with the signal processing circuit. A calibration of the instrument shows that the technique can be used to measure CH4 concentrations as small as 5 ppm-m and the effects of interfering gases are analyzed.

Sebacher, D. I.↗
NASA NTRS1980

Review of spectroscopic data for measurement of stratospheric species

The role of various infrared techniques in measurements of trace gases in the stratosphere were surveyed. Particular emphasis was placed on the role of instruments exhibiting ultrahigh resolution (i.e., less than or equal to 0.00/cm) such as laser heterodyne spectrometers.

Goldman, A.↗
NASA NTRS1980

Thermography for estimating near-surface soil moisture under developing crop canopies

Previous investigations of thermal infrared techniques using remote sensors (thermography) for estimating soil water content have been limited primarily to bare soil. Ground-based and aircraft investigations were conducted to evaluate the potential for extending the thermography approach to developing crop canopies. A significant exponential relationship was found between the volumetric soil water content in the 0-4 cm soil layer and the diurnal difference between surface soil temperature measured at 0230 and 1330 LST (satellite overpass times of NASA's Heat Capacity Mapping Mission - HCMM). Surface soil temperatures were estimated using minimum air temperature, percent cover of the canopy and remote measurements of canopy temperature. Results of the investigation demonstrated that thermography can potentially be used to estimate soil temperature and soil moisture throughout a complete growing season for a number of different crops and soils.

Heilman, J. L.↗
NASA NTRS1976

The status of cometary science

The problem of determining the chemical composition and physical structure of comet nuclei are discussed in light of recent analytical improvements. The development of radio and infrared techniques, improved sensing equipment, and the ability to conduct observations in space using satellites or skylabs are highlighted. The studies of two major comets, Kohoutek and West 1975n, are presented as examples of the utilization of these improved analytic tools.

Whipple, F. L.↗
NASA NTRS1983

Fire-Resistant Composites

Resin blend produces high-char-yield, low-smoke composites. Diglycidyl Ether of Bis-(4-Hydroxyphenyl)-Fluorene is prepared by reacting epichlorohydrin and sodium hydroxide with 9,9-bis(hydroxyphenyl) fluorene. End of reaction determined by gas or liquid chromatography, mass spectroscopy or infrared techniques. Used to manufacture printed circuit boards and panels for buildings, ships and aircraft.

Kourtides, D. A.↗