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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 91 records · Page 5
All sourcesNASA NTRSDOE OSTI
NASA NTRS1980

Accuracy of trace element determinations in alternate fuels

NASA-Lewis Research Center's work on accurate measurement of trace level of metals in various fuels is presented. The differences between laboratories and between analytical techniques especially for concentrations below 10 ppm, are discussed, detailing the Atomic Absorption Spectrometry (AAS) and DC Arc Emission Spectrometry (dc arc) techniques used by NASA-Lewis. Also presented is the design of an Interlaboratory Study which is considering the following factors: laboratory, analytical technique, fuel type, concentration and ashing additive.

Greenbauer-Seng, L. A.↗
DOE OSTI2026

Shining Light on Halide Perovskites: Teaching Analytical Chemistry Using Flexible, Inquiry-Based Experiments

Two-dimensional (2D) metal halide perovskites are promising next generation semiconducting materials at the forefront of research in solar cells, LEDs, and other devices. Here, we report on an undergraduate intermediate analytical chemistry laboratory experience where students were taught fundamental chemistry concepts, including solubility, complexation, spectroscopy, and microscopy, through the introduction and study of 2D halide perovskite materials. Students explore multiple facets of perovskite synthesis, structure, and properties through a modular set of experiments that students used to form a holistic picture of this material. Importantly, this inquiry-based lab supports students through a guided research process, and students report high interest and learning gains from an end of the semester survey. We further discuss ways to adapt this lab to course, student, equipment, and budget needs. Overall, this laboratory experience teaches and applies the fundamental concepts and tools of analytical chemistry to the contemporary materials research field.

Analytical Chemistry↗
NASA NTRS2004

Compensating for Effects of Humidity on Electronic Noses

A method of compensating for the effects of humidity on the readouts of electronic noses has been devised and tested. The method is especially appropriate for use in environments in which humidity is not or cannot be controlled for example, in the vicinity of a chemical spill, which can be accompanied by large local changes in humidity. Heretofore, it has been common practice to treat water vapor as merely another analyte, the concentration of which is determined, along with that of the other analytes, in a computational process based on deconvolution. This practice works well, but leaves room for improvement: changes in humidity can give rise to large changes in electronic-nose responses. If corrections for humidity are not made, the large humidity-induced responses may swamp smaller responses associated with low concentrations of analytes. The present method offers an improvement. The underlying concept is simple: One augments an electronic nose with a separate humidity and a separate temperature sensor. The outputs of the humidity and temperature sensors are used to generate values that are subtracted from the readings of the other sensors in an electronic nose to correct for the temperature-dependent contributions of humidity to those readings. Hence, in principle, what remains after corrections are the contributions of the analytes only. Laboratory experiments on a first-generation electronic nose have shown that this method is effective and improves the success rate of identification of analyte/ water mixtures. Work on a second-generation device was in progress at the time of reporting the information for this article.

Homer, Margie↗
DOE OSTI2025

C136A and C138A Report of Analysis

In this work the isotopic ratios and weight percentages of 238 Pu, 239 Pu, 240 Pu, 241 Pu and 242 Pu were determined using Isotope Dilution Mass Spectrometry. Two samples of C136A and C138A were sent to the Analytical Research laboratories by the National Nuclear Security Administration Nuclear Reference Material Program. The four samples were dissolved in concentrated hydrochloric acid. From the parent solutions, eight aliquots were taken, diluted, spiked with 244 Pu and submitted to separations. After the samples were separated, they were analyzed using Multicollector Inductively Coupled Plasma Mass Spectrometry. Along with the samples, two C126A Quality Control Samples were analyzed each day. Mass bias standards were also analyzed at the beginning, during and at the end of the analysis. GUM Workbench Pro software Version 2.4.1.406 was used to calculate the isotopic ratios relative to 239 Pu, and total Pu mass and the correlated expanded uncertainties.

37 - INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL C↗
DOE OSTI2025

Quantifying and Optimizing the Energy Benefits of Mass Timber Construction

The International Mass Timber Alliance (IMTA) is a global organization of industry leaders, engineers, scientists, and associations dedicated to advancing mass timber construction. Its mission is to generate and disseminate scientific data supporting the development of standardized construction and energy efficient practices that promote the adoption of mass timber worldwide. IMTA collaborated with Oak Ridge National Laboratory (ORNL) to leverage ORNL’s expertise in building envelope modeling and testing to evaluate how mass timber construction can reduce peak heating and cooling demand, lower overall energy use, and improve resilience during power outages. A previous study of 80 mass timber buildings in Finland found measured energy use up to 50% lower than predicted by simulation. This project aimed to validate and extend those findings for U.S. buildings through analytical modeling, laboratory testing, and full-scale building evaluations. The research focused on the thermal performance of low-embodied-energy wall assemblies, such as cross-laminated timber (CLT) panels and log walls, with particular attention to the effects of thermal inertia on indoor comfort and energy performance. While mass timber’s structural and fire-resistance properties are well documented, its whole-building thermal behavior has received limited attention. Field data, simulation results, and resilience testing from this study will inform future modeling practices, design guidelines, and construction practices by quantifying the unique thermal and demand-flexibility benefits of mass timber construction.

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗
DOE OSTI2026

Analysis Report for Hydrolyzed UF 6 Samples

Under the auspices of the US Department of Energy/National Nuclear Security Agency’s Nuclear Reference Material Program (NRMP), the Material Signatures and Isotopic Standards (MSIS) group of Oak Ridge National Laboratory was tasked with analyzing two UF6 filled hoke tubes for uranium isotopic composition. This report documents the results of the measurements performed by the MSIS group’s International Organization for Standardization/International Electrotechnical Commission 17025:2017 accredited operating procedure CSD-AM-CIMS-IN20, Determination of Uranium and Plutonium Isotopic Composition using Thermal Ionization Mass Spectrometry, and in accordance with the quality assurance plan as described in QAP-X-96-CSD/RML-001, Nuclear Analytical Chemistry Laboratory Section Quality Assurance Plan.

38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEA↗
DOE OSTI2026

ORNL Report for Hydrolyzed UF 6 Samples 439451, 438792, 439144, 439616, and 439617

Under the auspices of the US Department of Energy/National Nuclear Security Agency’s Nuclear Reference Material Program (NRMP), the Material Signatures and Isotopic Standards (MSIS) group of Oak Ridge National Laboratory was tasked with analyzing five UF 6 filled P-10 tubes for uranium isotopic composition. This report documents the results of the measurements performed by the MSIS group’s International Organization for Standardization/International Electrotechnical Commission 17025:2017 accredited operating procedure CSD-AM-CIMS-IN20, Determination of Uranium and Plutonium Isotopic Composition using Thermal Ionization Mass Spectrometry, and in accordance with the quality assurance plan as described in QAP-X-96-CSD/RML-001, Nuclear Analytical Chemistry Laboratory Section Quality Assurance Plan.

38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEA↗
DOE OSTI2026

ORNL Report of Analysis for the Verification of NRMP CRM U030A

In support of the Certified Reference Material (CRM) program managed by the Nuclear Reference Material Program (NRMP), the Material Signatures and Isotopic Standards (MSIS) group of Oak Ridge National Laboratory (ORNL) was asked to prepare a set of CRM U030A units for use as standards for isotopic analysis using multicollector thermal ionization mass spectrometry (TIMS) and inductively coupled plasma mass spectrometry (ICP-MS) instruments. This report documents the results of the verification measurements performed on three randomly selected units by the MSIS group’s ISO/IEC 17025:2017 accredited operating procedure CSD-AM-CIMS-IN20, Determination of Uranium and Plutonium Isotopic Composition using Thermal Ionization Mass Spectrometry [1], and in accordance with the quality assurance plan as described in QAP-X-96-CSD/RML-001, Nuclear Analytical Chemistry Laboratory Section Quality Assurance Plan [2].

Mathew, Kattathu [Oak Ridge National Laboratory (O↗
NASA NTRS1979

Analytical model of an Annular Momentum Control Device (AMCD) laboratory test model magnetic bearing actuator

An analytical model of an Annular Momentum Control Device (AMCD) laboratory test model magnetic bearing actuator with permanent magnet fluxbiasing is presented. An AMCD consists of a spinning annular rim which is suspended by a noncontacting linear electromagnetic spin motor. The actuator is treated as a lumped-parameter electromechanical system in the development of the model.

Groom, N. J.↗
DOE OSTI2024

Rare Earth Elements (REEs) Measurement in Coal and Rock Mineral Matrices

Although critical minerals including rare earth elements (REEs) can be analyzed in laboratory by some established and reliable laboratory based analytical techniques, their in-situ measurements in the field have always been challenging. For identification of REE-rich sites and REEs distribution measurement, portable field applicable technologies are paramount. As Laser-induced breakdown spectroscopy (LIBS) has enormous potential for field measurement, it has been explored for REEs measurements by many research groups. However, most of the studies are still dealing with simulated samples with traditional bench top experiments. In real world, REEs are available in various types of natural complex matrices in low content depending on the geographical locations. Considering this, LIBS has been evaluated for REE measurement in two different complex coal and rock mineral matrices representing some natural REE-rich sites. In addition, multiple samples collected from some natural sites in Wyoming, USA were experimented by using NETL’s bench top as well as miniaturized prototype setups for REE measurements.

Bhatt, Chet R.↗
DOE OSTI2025

Conceptual Design of a Scaled Voloxidation Apparatus for Testing with Used Nuclear Fuel

This report details the conceptual design overview for Department of Energy (DOE) Level 2 milestone M2FT-25IN030101021 titled “Complete conceptual design of a scaled voloxidation apparatus for testing with used nuclear fuel.” Advanced voloxidation uses high temperature nitrogen dioxide (NO2) gas to oxidize uranium dioxide (UO2) material to triuanium octoxide (U3O8) and ultimately to uranium trioxide (UO3). After consideration of multiple available options and inputs, a rotating advanced voloxidation design was determined to be the best fit for the needs of a full-scale apparatus. The system, which will be deployed in hot cell 4 of the Analytical Research Laboratory (ARL), has been designed to meet the space constraints of the facility while still accommodating at least 100g of used nuclear fuel (UNF). The apparatus consists of three main unit operations, including the gas panel, the custom furnace with reaction vessel, and the liquid scrubber.

11 - NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗
NASA NTRS1972

Study of the application of advanced technologies to long-range transport aircraft. Volume 2: Research and development requirements

Investigations were conducted to evaluate the relative benefits attainable through the exploitation of advanced technologies and to identify future research and development efforts required to permit the application of selected technologies to transport aircraft entering commercial operation in 1985. Results show that technology advances, particularly in the areas of composite materials, supercritical aerodynamics, and active control systems, will permit the development of long-range, high-payload commercial transports operating at high-subsonic speeds with direct operating costs lower than those of current aircraft. These advanced transports also achieve lower noise levels and lower engine pollutant emissions than current transports. Research and development efforts, including analytical investigations, laboratory test programs, and flight test programs, are required in essentially all technology areas to achieve the potential technology benefits.

Lange, R. H.↗
NASA NTRS1971

Definition of defect size from ultrasonic inspection.

Attempt to obtain a set of relationships between testing parameters defining the range of defect size that can be associated with a given echo amplitude and defect depth. These relationships allow the user to find the largest defect that will return a signal equal to that from a flat hole of known diameter and depth, and the signal amplitude ratio between worst case and flat hole defects of equal diameter. The variation of the data with defect and testing parameters is shown. The results are obtained analytically, with laboratory corroboration, by calculation of the echo amplitude of the defect shape yielding the smallest return signal, a sphere, and the echo amplitude of the defect shape yielding the largest return signal, a flat hole.

Bennet, S. B.↗
NASA NTRS1972

Quantifying parameters influencing the spacing of geostationary satellites.

Parameters affecting satellite spacing must be investigated to fully exploit the limited capacity of the geostationary orbit. The usefulness of laboratory experiments, analytic methods, and space environment experiments in quantifying these factors is discussed. It is concluded that space environment experiments are required to evaluate the effects of operationally related parameters including antenna gain patterns, polarization, and antenna instabilities. A unique method of measuring the time-variant effects of the earth station antenna characteristics on satellite spacing is described as a possible space environment experiment. The proposed experiment uses a single satellite to obtain the required data.

Henry, V. F.↗
NASA NTRS1975

Flight testing air-to-air missiles for flutter

The philosophy of the design of air-to-air missiles and hence of flight testing them for flutter differs from that of manned aircraft. Primary emphasis is put on analytical and laboratory evaluation of missile susceptibility to aeroelastic and aero-servo-elastic instabilities and uses flight testing for confirmation of the absence of such instabilities. Flight testing for flutter is accomplished by using specially instrumented programmed missiles, air or ground launched with a booster to reach the extreme flight conditions of tactical use, or by using guided missiles with telemetered performance data. The instrumentation and testing techniques are discussed along with the success of recent flight tests.

Kutschinski, C. R.↗
NASA NTRS1976

Propagation of aircraft noise

The major tasks undertaken were (1) analytical and laboratory experiments on the propagation of sound from sources near a flat surface of finite acoustic impedance; (2) laboratory experiments dealing with the reflection of sound from finite sized plane patches; and (3) the diffraction of sound by wedge-and trapezoidal-shape barriers. In addition, a series of measurements were made of the background noise levels for various jet flow conditions in the Anechoic Noise Facility of the Langley Research Center's Acoustic and Noise Reduction Laboratory.

Pierce, A. D.↗
NASA NTRS1978

YF-12 Experiments Symposium, Volume 1

This document is a compilation of papers presented at the YF-12 Experiments Symposium held at the NASA Dryden Flight Research Center, September 13-15, 1978. Papers were presented by personnel from the Dryden Flight Research Center, the Lewis Research Center, and the Ames Research Center. Topics covered propulsion system performance, inlet time varying distortion, structures, aircraft controls, propulsion controls, and aerodynamics. The reports were based on analytical studies, laboratory experiments, wind tunnel tests, and extensive flight research with two YF - 12 airplanes.

YF-12 airplane↗
NASA NTRS1979

Earth orbital teleoperator systems evaluation

The mechanical extension of the human operator to remote and specialized environments poses a series of complex operational questions. A technical and scientific team was organized to investigate these questions through conducting specific laboratory and analytical studies. The intent of the studies was to determine the human operator requirements for remotely manned systems and to determine the particular effects that various system parameters have on human operator performance. In so doing, certain design criteria based on empirically derived data concerning the ultimate control system, the human operator, were added to the Teleoperator Development Program.

Shields, N. L., Jr.↗