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All sources NASA NTRS DOE OSTI

DOE OSTI2021

Influence of dissolved salts and impurities on seawater on heat transfer and fluid flow through fuel channels and debris bed

This project aims to better understand this mechanism and its effect on heat transfer. Specifically, experimental research was conducted to investigate the long term coolability issues in scaled test setups. Advanced diagnostic and measurement techniques were investigated and incorporated into an annular test facility and a debris bed test facility. The diagnostic techniques investigated included: radioactively tagged salt solution, Frisch collar radiation detector array, neutron and x-ray imaging systems, and a Rayleigh backscatter-based fiber-optic temperature system. Models were checked against the in-situ experimental data and recommendations were made for modeling purposes.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗

NASA NTRS1976

Status of NASA aircraft engine emission reduction and upper atmosphere measurement programs

Advanced emission reduction techniques for five existing aircraft gas turbine engines are evaluated. Progress made toward meeting the 1979 EPA standards in rig tests of combustors for the five engines is reported. Results of fundamental combustion studies suggest the possibility of a new generation of jet engine combustor technology that would reduce oxides-of-nitrogen (NOx) emissions far below levels currently demonstrated in the engine-related programs. The Global Air Sampling Program (GAS) is now in full operation and is providing data on constituent measurements of ozone and other minor upper-atmosphere species related to aircraft emissions.

Rudey, R. A.↗

NASA NTRS2000

WSTF Pyrovalve Test Program Status: 2000

Extensive propulsion and pyrotechnic testing has been in progress at NASA/JSC White Sands Test Facility (WSTF) since 1995, starting with the Mars Observer Propulsion and Pyrotechnics Corrective Action Test Program (MOCATP). The MOCATP has been concluded, but extensive pyrovalve testing plus research and development continues at WSTF. Our capability to accurately characterize pyrovalve combustion product blow-by into propellant systems, evaluate hydrazine and monomethylhydrazine (MMH) thermal decomposition initiated by blow-by, and characterize valve actuation operation, continues to be used and refined. Data from this and several low blow-by pyrovalves manufactured by Conax and other corporations continues to be evaluated as a potential corrective measure for blow-by induced propellant explosions. Additionally, new measurement techniques are being developed, advanced pyrovalve development is under-way, and nondestructive examination (NDE) methods are being developed to help ensure pyrovalve safety. Starting in 2000 these data are being formatted into a pyrovalve application and testing handbook. Near-term testing includes evaluation of 3/8-in. Conax pyrovalves and other commercially available valves; development of advanced pyrovalve subcomponent technology; investigation of NDE techniques to evaluate pyrovalve ram seals and real-time measurement of housing deformation; and investigation of pyrotechnically induced explosive hydrazine decomposition both through testing and modeling. Evaluation of 3/8-in. Conax valves is to include operational margin testing to be accomplished at the NASA Langley Research Center.

Saulsberry, Regor L.↗

NASA NTRS1985

The investigation of advanced remote sensing, radiative transfer and inversion techniques for the measurement of atmospheric constituents

The research program is documented for developing space and ground-based remote sensing techniques performed during the period from December 15, 1977 to March 15, 1985. The program involved the application of sophisticated radiative transfer codes and inversion methods to various advanced remote sensing concepts for determining atmospheric constituents, particularly aerosols. It covers detailed discussions of the solar aureole technique for monitoring columnar aerosol size distribution, and the multispectral limb scattered radiance and limb attenuated radiance (solar occultation) techniques, as well as the upwelling scattered solar radiance method for determining the aerosol and gaseous characteristics. In addition, analytical models of aerosol size distribution and simulation studies of the limb solar aureole radiance technique and the variability of ozone at high altitudes during satellite sunrise/sunset events are also described in detail.

Deepak, Adarsh↗

NASA NTRS1996

Frequency Response of Pressure Sensitive Paints

An experimental method for measuring the frequency response of Pressure Sensitive Paints (PSP) is presented. These results lead to the development of a dynamic correction technique for PSP measurements which is of great importance to the advancement of PSP as a measurement technique. The ability to design such a dynamic corrector is most easily formed from the frequency response of the given system. An example of this correction technique is shown. In addition to the experimental data, an analytical model for the frequency response is developed from the one dimensional mass diffusion equation.

Winslow, Neal A.↗

DOE OSTI2025

Application of Raman Spectroscopy to Determine Uranium Content in ADUN Solution

The work presented in this report is part of the ongoing efforts to address the nuclear material control and accounting needs for advanced reactor fuel fabrication facilities. This work was supported by the Materials Protection, Accounting, and Control Technologies (MPACT) program under the US Department of Energy Office of Nuclear Energy‘s Nuclear Fuel Cycle and Supply Chain program. The activities and engagements under the MPACT program are designed to support a robust US civilian nuclear energy enterprise. In the work described in this report, we supported MPACT objectives by developing measurement techniques that could be used for material accounting and process monitoring and by working with industry partners to identify existing gaps and areas for improvement. Oak Ridge National Laboratory has been working with commercial tristructural isotropic (TRISO) fuel fabricators such as Standard Nuclear to develop technology for rapid and cost-effective uranium content assessment. This work has focused on demonstrating advanced measurement techniques (e.g., Raman spectroscopy) that can be used for rapid, reliable, and cost-effective routine measurements of uranium content in feed solutions and liquid waste streams as well as for monitoring in-line process measurements and product streams. Specifically, this report explores techniques for accurately determining uranium content in acid-deficient uranyl nitrate (ADUN) solutions and detecting low uranium concentrations in ammonia solutions. Developing such measurement techniques will benefit TRISO fuel fabrication facilities, facilities involved in other parts of the fuel cycle that require online monitoring of aqueous solutions, and potentially molten salt fuel reactors. This work supports developing Raman spectroscopy procedures to determine uranium concentrations in ADUN solutions, which are used as feedstock in the sol–gel process for creating TRISO fuel. Some additional benefits of using Raman spectroscopy for uranium quantification in fabrication facilities include enabling online monitoring of the chemical process, which would provide near real-time feedback; eliminating the need for sample transfers, preparation, or dilution; providing nondestructive measurements; and user friendliness. In this fiscal year, FY25, we determined the identity of the unknown Raman band at approximately 853 cm−1 that was discovered in ADUN Raman spectra in FY24, created calibration curves and determined uranium concentrations of two ADUN solutions, and compared the Raman results to results obtained from inductively coupled plasma mass spectrometry and Davies–Gray titration. Furthermore, we have identified focus areas for experimentation in future fiscal years. A key result is that the accuracy of using Raman can provide accuracy comparable to destructive analysist techniques, With a well-developed calibration curve, using standards and a large number of samples (more than five samples), uncertainty on the order of 1%–3% is achievable. Given that the uncertainties achieved by Raman spectroscopy were on the order of the uncertainties achieved using ICP-MS, we conclude that with a well-developed procedure Raman spectroscopy can be used to determine uranium concentrations in ADUN solutions for NMC&A applications. The benefits of such an approach are that the time and effort will be less than that of comparable destructive analysis techniques, with approximately the same level of technical expertise. This will be attractive to operators of fuel fabrication facilities as it will lower costs and improve efficiencies.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

NASA NTRSDate not supplied

Seeding Mechanism for High-Pressure Nozzles

NASA tests new launch and entry vehicle configurations in wind tunnels, where flow visualizations and quantitative flow field measurements are often desired. Some of these vehicles have rocket motors for propulsion, retro-propulsion, or reaction control. Unseeded,high-pressure air is often used to simulate these rocket motor plumes. However, it is difficult to make off-body measurements in these regions, for several reasons. First, the plumes themselves are usually unseeded and at such low pressures that the flow velocity cannot currently be measured. Second, the plumes displace seeded tunnel air, preventing measurements such as laser sheet visualizations. Third, they force shock waves ahead of the vehicle, which melts the ice crystal fog commonly used for many visualization and measurement techniques. The Virginia Tech Advanced Propulsion and Power Lab has designed and tested a novel method for seeding the flow in these small-scale, high-pressure nozzles to allow quantitative measurement with a particle-based measurement such as particle image velocimetry (PIV). The method involves a Venturi contraction to draw the seed liquid out of a reservoir and into the nozzle channel, wherein shearing forces atomize the seed into particles. The concept was tested with a laser sheet visualization, which showed the nozzle spray pattern and the controllability of the seeding flow rate. This relatively inexpensive and simple technique may prove useful in wind tunnel experiments involving particle-based laser diagnostics and small, high-pressure nozzles.

particle image velocimetry↗

NASA NTRS2019

Characterizing the System Impulse Response Function from Photon-Counting LiDAR Data

NASA's Multiple Altimeter Beam Experimental LiDAR (MABEL) is an aircraft-based photon-counting laser altimeter designed as a simulator to test measurement techniques and algorithms for Advanced Topographic Laser Altimeter System (ATLAS), the sole instrument on NASA's Ice, Cloud, and land Elevation Satellite-2 (ICESat-2) mission. By measuring the time of flight, pointing angle, and absolute position for individual photons, ICESat-2 provides detailed elevation measurements of earth's surface. Calculating accurate and precise elevations requires an understanding of how photons interact with surfaces, and characterization of the photon distribution after returning from surfaces. Neither MABEL nor ATLAS records the transmitted laser pulse shape, relying instead on aggregating several pulses worth of photons, often using histograms, to characterize the pulse shape. In this paper, we assess the limitations of using histograms and propose a more robust method to describe MABEL's system impulse-response function using an exponentially modified Gaussian distribution. We also provide standard error estimates for the arithmetic mean and standard deviation calculations, and for exponentially modified Gaussian parameters using a Monte Carlo sensitivity analysis. We apply this method to photon returns from a sea ice lead and from a dry salt lake bed as case studies for estimating the standard error associated with sample size for the arithmetic mean and standard deviation, and for the exponentially modified Gaussian parameters. We use these standard errors to calculate the minimum number of photons required to find both Gaussian and exponentially modified Gaussian distribution parameters within 3 cm of their parent population values.

photoncounting↗

NASA NTRS1980

The measuring and growing of advanced gas turbines

Advances in the gas turbine technology level and the corresponding advances in measurement instruments and technique are reviewed for each of the past decades, starting with the forties. The review provides a picture of the gradual development from the earlier, relatively simple systems, to the present sophisticated machines. A look in the future indicates that continued advances in gas turbine technology will be needed, used, and supported and that substantial changes are underway as to how these advances will be achieved. Some projections of the type of advances and in technology and measurements to be expected in the decade of the eighties are presented.

Hartmann, M. J.↗

NASA NTRS2015

Advanced Intensity-Modulation Continuous-Wave Lidar Techniques for ASCENDS O2 Column Measurements

Global atmospheric carbon dioxide (CO2) measurements for the NASA Active Sensing of CO2 Emissions over Nights, Days, and Seasons (ASCENDS) space mission are critical for improving our understanding of global CO2 sources and sinks. Advanced Intensity- Modulated Continuous-Wave (IM-CW) lidar techniques are investigated as a means of facilitating CO2 measurements from space to meet the ASCENDS measurement requirements. In recent numerical, laboratory and flight experiments we have successfully used the Binary Phase Shift Keying (BPSK) modulation technique to uniquely discriminate surface lidar returns from intermediate aerosol and cloud contamination. We demonstrate the utility of BPSK to eliminate sidelobes in the range profile as a means of making Integrated Path Differential Absorption (IPDA) column CO2 measurements in the presence of optically thin clouds, thereby eliminating the need to correct for sidelobe bias errors caused by the clouds. Furthermore, high accuracy and precision ranging to the surface as well as to the top of intermediate cloud layers, which is a requirement for the inversion of column CO2 number density measurements to column CO2 mixing ratios, has been demonstrated using new hyperfine interpolation techniques that takes advantage of the periodicity of the modulation waveforms. This approach works well for both BPSK and linear swept-frequency modulation techniques. The BPSK technique under investigation has excellent auto-correlation properties while possessing a finite bandwidth. A comparison of BPSK and linear swept-frequency is also discussed in this paper. These results are extended to include Richardson-Lucy deconvolution techniques to extend the resolution of the lidar beyond that implied by limit of the bandwidth of the modulation, where it is shown useful for making tree canopy measurements.

Campbell, Joel F.↗

NASA NTRS1980

Concepts and techniques for ultrasonic evaluation of material mechanical properties

Ultrasonic methods that can be used for material strength are reviewed. Emergency technology involving advanced ultrasonic techniques and associated measurements is described. It is shown that ultrasonic NDE is particularly useful in this area because it involves mechanical elastic waves that are strongly modulated by morphological factors that govern mechanical strength and also dynamic failure modes. These aspects of ultrasonic NDE are described in conjunction with advanced approaches and theoretical concepts for signal acquisition and analysis for materials characterization. It is emphasized that the technology is in its infancy and that much effort is still required before the techniques and concepts can be transferred from laboratory to field conditions.

Vary, A.↗

NASA NTRS1983

An evaluation of the accuracy of some radar wind profiling techniques

Major advances in Doppler radar measurement in optically clear air have made it feasible to monitor radial velocities in the troposphere and lower stratosphere. For most applications the three dimensional wind vector is monitored rather than the radial velocity. Measurement of the wind vector with a single radar can be made assuming a spatially linear, time invariant wind field. The components and derivatives of the wind are estimated by the parameters of a linear regression of the radial velocities on functions of their spatial locations. The accuracy of the wind measurement thus depends on the locations of the radial velocities. The suitability is evaluated of some of the common retrieval techniques for simultaneous measurement of both the vertical and horizontal wind components. The techniques considered for study are fixed beam, azimuthal scanning (VAD) and elevation scanning (VED).

Koscielny, A. J.↗

DOE OSTI2025

High‐Speed Embedded Ink Writing of Anatomic‐Size Organ Constructs

Embedded ink writing (EIW) is an emerging 3D printing technique that fabricates complex 3D structures from various biomaterial inks but is limited to a printing speed of ∼10 mm s −1 due to suboptimal rheological properties of particulate-dominated yield-stress fluids when used as liquid baths. In this work, a particle-hydrogel interactive system to design advanced baths with enhanced yield stress and extended thixotropic response time for realizing high-speed EIW is developed. In this system, the interactions between particle additive and three representative polymeric hydrogels enable the resulting nanocomposites to demonstrate different rheological behaviors. Accordingly, the interaction models for the nanocomposites are established, which are subsequently validated by macroscale rheological measurements and advanced microstructure characterization techniques. Filament formation mechanisms in the particle-hydrogel interactive baths are comprehensively investigated at high printing speeds. To demonstrate the effectiveness of the proposed high-speed EIW method, an anatomic-size human kidney construct is successfully printed at 110 mm s −1 , which only takes ∼4 h. This work breaks the printing speed barrier in current EIW and propels the maximum printing speed by at least 10 times, providing an efficient and promising solution for organ reconstruction in the future.

36 MATERIALS SCIENCE↗

NASA NTRS2013

Advanced Ceramics Property Measurements

Mechanical and physical properties of ceramic bodies can be difficult to measure correctly unless the proper techniques are used. The Advanced Ceramics Committee of ASTM, C-28, has developed dozens of consensus test standards and practices to measure various properties of a ceramic monolith, composite, or coating. The standards give the "what, how, how not, and why" for measurement of many mechanical, physical, thermal, and performance properties. Using these standards will provide accurate, reliable, and complete data for rigorous comparisons with other test results from your test lab, or another. The C-28 Committee has involved academics, producers, and users of ceramics to write and continually update more than 45 standards since the committee's inception in 1986. Included in this poster is a pictogram of the C-28 standards and information on how to obtain individual copies with full details or the complete collection of standards in one volume.

Salem, Jonathan↗

DOE OSTI2022

Development of an MC&A toolbox for liquid-fueled molten salt reactors with online reprocessing (Final Report)

A critical barrier to the deployment of MSRs is the absence of a well-defined nuclear material control and accounting (MC&A) approach, a vital prerequisite to meet NRC licensing requirements as well as facilitating future international exports. Liquid-fueled MSR variants (especially those incorporating online refueling or reprocessing) present a unique set of challenges to traditional nuclear material control and accountancy. Unlike solid-fueled light-water reactors, traditional item-counting methods cannot be applied as an accountancy strategy. Rather, MC&A approaches to MSR variants (including both uranium and thorium fueled designs) are more analogous to bulk material handling facilities (e.g., enrichment and reprocessing); yet further complicating matters is the fact that fuel medium is also highly radioactive. Meanwhile, the space of MSRs covers a broad range of design parameters, including thermal and fast spectra designs; operation in actinide breeder or burner modes, choice of actinide fuel used (e.g., 235 U, 232 Th / 233 U, denatured 233 U, etc.), pool or loop-type configuration, and even different salt chemistry. Each of these design choices introduce significant challenges to MC&A approaches within MSR facilities. We propose to bridge this gap for liquid-fueled MSRs by developing a modular, component-based test framework for evaluating viable process monitoring and MC&A techniques specifically suited to liquid-fueled MSR system variants employing online refueling or reprocessing. This test platform will consist of a toolbox of independent process modules representing discrete physical units (such as the reactor core, off-gas processing, decay tanks, and actinide separation units), each with its own self-contained physics responsive to the input mass flow, along with appropriate measurement models that can be coupled to key flow points. These dynamic physical signatures thus afford the ability to test the viability and efficacy of potential accountancy techniques under the full range of reactor operating conditions. As process modules are connected via mass flows, the result is a reconfigurable, generic MSR mass flow model capable of serving as an MC&A test platform for a broad spectrum of possible MSR configurations. The resulting MSR MC&A toolbox will enable robust assessment of accountancy strategies for this unique facility type, including analysis of physical feedbacks arising both from depletion of the fuel over time as well as from potential off-normal events, including those introduced by equipment failures (e.g., a pump failure) as well as by malicious action (i.e., attempts to divert material). The proposed toolbox both addresses a critical needs area for the MPACT analysis toolkit while leveraging existing MPACT-sponsored tools, especially with respect to simulation of measurement and accountancy techniques for advanced fuel cycle facilities. Beyond enabling new analysis capabilities for MSR systems, the design of this toolbox will be to such to maximize compatibility with existing MPACT tools, such to enhance existing facility MC&A analysis capabilities.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

DOE OSTI2023

Production of Precursor Materials for the Development of Iron-Based Superconductor (IBS) Wire

The objective of the activities under this Annex is to address the extrinsic Jc limitations uncovered in pioneering work. In order to engineer the defects pinning landscape charged particle irradiations experiments on bulk samples, different doping and chemical additions will be performed at different National facilities (Test Beam Facility at Fermilab; Linac Isotope Producer at Brookhaven National Laboratory; Integrated Biology Laboratory at University of Wisconsin-Madison; Facility for Rare Isotope Beams at Michigan State University). The samples will be produced at ENEA by different techniques. Magnetization and advanced microscopy measures will be performed at Fermilab. After irradiation, depending on the level of radioactivity, the samples will be tested at Fermilab or where it is possible to measure radioactive materials as University of Wisconsin-Madison.

43 PARTICLE ACCELERATORS↗

DOE OSTI2023

Production of Precursor Materials for the Development of Iron-Based Superconductor (IBS) Wire

The objective of the activities under this Annex is to address the extrinsic Jc limitations uncovered in pioneering work. In order to engineer the defects pinning landscape charged particle irradiations experiments on bulk samples with different doping and chemical additions will be performed at different National facilities (Test Beam Facility at Fermilab; Linac Isotope Producer at Brookhaven National Laboratory; Integrated Biology Laboratory at University of Wisconsin-Madison; Facility for Rare Isotope Beams at Michigan State University). The samples will be produced at TUAT by different synthesis techniques. Magnetization and advanced microscopy measures will be performed at Fermilab. After irradiation, depending on the level of radioactivity, the samples will be tested at Fermilab or where it is possible to measure radioactive materials as University of Wisconsin-Madison. In parallel, the precursor materials produced by TUAT will be used for IBS-wire fabrication at Fermi

43 PARTICLE ACCELERATORS↗

NASA NTRS1994

Preliminary solutions for the lunar gravity field from analysis of lunar orbiter tracking data

Knowledge of the gravitation field, in combination with surface topography, provides one of the principal means of inferring the internal structure of a planetary body. Previous analyses of the lunar gravitational field have been based on data from the Lunar Orbiters, the Apollo subsatellites, and the low altitude passes of the Apollo spacecraft. Recently, Konopliv et al. have reanalyzed all available Lunar Orbiter and Apollo subsatellite tracking data, producing a 60th degree and order solution. In preparation for the Clementine Mission to the Moon, we have also initiated a reanalysis of the Lunar Orbiter and Apollo subsatellite data. Our reanalysis takes advantage of advanced force and measurement modeling techniques as well as modern computational facilities. We applied the least squares collocation technique which stabilizes the behavior of the solution and high degree and order. The extension of the size of the field reduces the aliasing coming from the omitted portion of the gravitational field. This is especially important for the analysis of the tracking data from the Lunar Orbiters, as the periapse heights frequently ranged from 50 to 100 km.

Lemoine, F. G.↗