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At least 883 records · Page 49

T-1065: Secondary Emitters Study

One possibility to make a fast and radiation resistant shower maximum (SM) detector or preshower detector is to use a secondary emitter (SE) as an active element. This method was proposed in 1990. Micro channel plates (MCP) were used as SE in the SM. The attractive properties of such SM are: 1) a two-dimensional map of energy at the SE location; 2) timing information at few tens of picosecond level, also as transverse shower size and 3) possible separation of electromagnetic and hadronic energy based on the differences of the shower size and timing. An electron-multiplier-based sampling calorimeter requires thin planar detectors at an affordable cost. Large-area photo detectors based on ALD-functionalized 20-cm-square borosilicate glass capillary micro-channel plates (MCPs), currently being developed by the LAPPD Collaboration, are candidates for the active elements. The first results of the new shower maximum detector with the micro channel plate photomultiplier (MCP-PMT) as active elements are described. The current proposal is the next natural step in this direction. The experimenters propose using large-area MCPs assembled without the usual bialkali photocathodes as the active element in sampling calorimeters. LAPPD modules without photocathodes can be economically assembled in a glove box and then pumped and sealed using the process to construct photomultipliers, bypassing the slow and expensive vacuum-transfer process required by bialkali photocathodes. The first use of electron multipliers, in this case MCPs (Fig. 1, left) as an active element in multi-layer sampling calorimeters is described. A chevron of two MCPs in vacuum, was located behind a tungsten plate on which 5 GeV and 26 GeV electrons were incident (Fig. 1, right). The amplitude of the MCP signal (Fig. 2) as a function of the tungsten thickness was measured. The primary electrons produce a shower of secondary particles, including positron-electron pairs and gammas; the response of the MCPs (Fig. 2, left) is proportional to the number of particles in the shower, which is dependent on the initial particle energy. The MCP signal shape is presented in the Fig. 2, right). The FWHM of the signal is 1 ns.

43 PARTICLE ACCELERATORS↗

Secondary-electron emission from hydrogen-terminated diamond

Diamond amplifiers demonstrably are an electron source with the potential to support high-brightness, high-average-current emission into a vacuum. We recently developed a reliable hydrogenation procedure for the diamond amplifier. The systematic study of hydrogenation resulted in the reproducible fabrication of high gain diamond amplifier. Furthermore, we measured the emission probability of diamond amplifier as a function of the external field and modelled the process with resulting changes in the vacuum level due to the Schottky effect. We demonstrated that the decrease in the secondary electrons average emission gain was a function of the pulse width and related this to the trapping of electrons by the effective NEA surface. The findings from the model agree well with our experimental measurements. As an application of the model, the energy spread of secondary electrons inside the diamond was estimated from the measured emission.

43 PARTICLE ACCELERATORS↗

Fabrication of compact electron gun for 6 MeV X-ray source

The 6 MeV X-Ray source for container cargo scanning application has been designed and developed by the Accelerator and Pulse Power Division, BARC, Mumbai. This compact linac has been designed as a mobile system, to be mounted on a moving container. In linac-based cargo-scanning system, to work electron gun on a movable container, it has to be robust. Electron gun is to work at 10{sup -7} mbar vacuum and 2000 degree Celsius temperature. An effort is made to engineer the gun assembly to make it more robust and aligned. The linac acts as the source of X-rays, which fall on the cargo and are then detected by the detector system. Many components are indigenously developed like grid, insulating ring, Tungsten filament and filament guide, which are made from alumina ceramic and Tantalum which is to work at 1500 degree Celsius. Filament connector is made from Invar to reduce heat loss and to make rigid connection. It was CNC machined and wire cut by EDM. Invar and Copper electrode feed through is shrink fitted with the help of liquid Nitrogen. Shrink fit tolerances of 15 micrometer are achieved by jig boring machining processes. Tantalum cup for LaB6 cathode and heat shield are made from die and punch mechanism. For alignment of electron emitter with beam axis this Tantalum cup is a crucial component. Electron gun is assembled and aligned its components with the help of precision jigs. The whole assembly was Helium leak tested by MSLD up to 4 x 10{sup -10} mbar.l/s vacuum, no leak was found. This paper will describe the machining, Tantalum cup forming, ceramic components development, heat shields, ceramic feed through etc of electron gun. (author)

43 PARTICLE ACCELERATORS↗

Control over the Magnetic Properties of Co/Pt-based Multilayered Periodical Structures

The possibility of controlling the magnetic properties of multilayered periodical structures with perpendicular magnetic anisotropy, which are based on cobalt and platinum films, have been studied. The multilayered films composed by layers with a thickness of 0.5–1.0 nm were subjected to two types of actions: vacuum annealing at different temperatures and irradiation by helium ion beams. Transmission electron microscopy has shown that the irradiation by He{sup +} ions with energy of 30 keV leads to material mixing in the layers since at vacuum annealing the layered structure of films is kept. In this case, as a result of thermal annealing, the coercive force of the structure increases significantly, and upon irradiation with helium ions, the coercivity of the films decreases to a change in the type of anisotropy from perpendicular to “easy plane” anisotropy.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Atomic Structure of Submonolayer NaCl Grown on Ag(110) Surface

In this work, we report results on the growth of an NaCl film on Ag(110) under ultrahigh vacuum conditions. At room temperature, low-energy electron diffraction and scanning tunneling microscopy show that the NaCl film forms a (4×1) superstructure. At RT, the film consists of small-sized islands that coalesce into larger islands at 410 K. These large islands preserve the (4×1) superstructure and cover the entire surface. The apparent heights obtained from the STM images show that the initial thickness of the NaCl islands is one atomic layer, and they present a very small height corrugation. The density functional theory calculations, with and without the inclusion of van der Waals effects, confirm the coexistence of two domains in agreement with the observed structure.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Reversible Electron-Beam Patterning of Colloidal Nanoparticles at Fluid Interfaces

The directed self-assembly of colloidal nanoparticles (NPs) using external fields guides the formation of sophisticated hierarchical materials but becomes less effective with decreasing particle size. As an alternative, electron-beam-driven assembly offers a potential avenue for targeted nanoscale manipulation, yet remains poorly controlled due to the variety and complexity of beam interaction mechanisms. Here, we investigate the beam–particle interaction of silica NPs pinned to the fluid–vacuum interface of ionic liquid droplets. In these experiments, scanning electron microscopy of the droplet surface resolves NP trajectories over space and time while simultaneously driving their reorganization. With this platform, we demonstrate the ability to direct particle transport and create transient, reversible colloidal patterns on the droplet surface. By tuning the beam voltage, we achieve precise control over both the strength and sign of the beam–particle interaction, with low voltages repelling particles and high voltages attracting them. This response stems from the formation of well-defined solvent flow fields generated from trace radiolysis of the ionic liquid, as determined through statistical analysis of single-particle trajectories under varying solvent composition. Altogether, electron-beam-guided assembly introduces a versatile strategy for nanoscale colloidal manipulation, offering new possibilities for the design of dynamic, reconfigurable systems with applications in adaptive photonics and catalysis.

36 MATERIALS SCIENCE↗

Effects of Temperature Fluctuations on Surface Mobility of Atomic Steps and Oxidation Dynamics in High-Temperature Alloys

In contrast to the traditional perspective that thermal fluctuations are insignificant in surface dynamics, here we report their influence on surface reaction dynamics. Using real-time low-energy electron microscopy imaging of NiAl(100) under both vacuum and O 2 atmospheres, we demonstrate that transient temperature variations substantially alter the direction of atom diffusion between the surface and bulk, leading to markedly different oxidation outcomes. During heating, substantial outward diffusion of atoms from the bulk to the surface results in step growth. Conversely, cooling induces considerable inward diffusion of adatoms, producing a distinct oxide morphology. In both scenarios, initially formed oxide islands impede local atomic step mobility, thereby increasing step length due to mass transfer between the surface and bulk, with atomic steps acting as adatom sinks during heating and sources during cooling. Furthermore, we show that this pinning effect on atomic step mobility can be mitigated by applying persistent temperature fluctuations. As a result, understanding these nuances is vital for accurately predicting and dynamically manipulating the performance of active materials in various chemical processes under transient thermal conditions.

36 MATERIALS SCIENCE↗

Experimental study of self magnetic pinch diode as flash radiography source at 4 megavolt

The Self Magnetic Pinch (SMP) diode is a potential high-brightness X-ray source for high voltage generators (2–10 MV) that has shown good reliability for flash radiography applications [D. D. Hinchelwood et al., “High power self-pinch diode experiments for radiographic applications” IEEE Trans. Plasma Sci. 35(3), 565–572 (2007)]. We have studied this diode at about 4 MV, driven by the ASTERIX generator operated at the CEA/GRAMAT [G. Raboisson et al., “ASTERIX, a high intensity X-ray generator,” in Proceedings of the 7th IEEE Pulsed Power Conference (1989), pp. 567–570]. This generator, made up of a capacitor bank and a Blumlein line, was initially designed to test the behavior of electronic devices under irradiation. In our experiments, the vacuum diode is modified in order to set up flash radiographic diodes. A previous set of radiographic experiments was carried out on ASTERIX with a Negative Polarity Rod Pinch (NPRP) diode [B. Etchessahar et al., “Study and optimization of negative polarity rod pinch diode as flash radiography source at 4.5 MV,” Phys. Plasmas 19(9), 093104 (2012)]. The SMP diode which is examined in the present study provides an alternative operating point on the same generator and a different radiographic performance: 142 ± 11 rad at 1 m dose (Al) for a 3.46 ± 0.42 mm spot size (1.4× FWHM of the LSF). This performance is obtained in a reproducible and robust nominal configuration. However, several parametric variations were also tested, such as cathode diameter and anode/cathode gap. They showed that an even better performance is accessible after optimization, in particular, a smaller spot size (<3 mm). Numbers of electrical, optical, and X-ray diagnostics have been implemented in order to gain more insight in the diode physics and to optimize it further. For the first time in France, visible and laser imaging of the SMP diode has been realized, from a radial point of view, thus, providing key information on the electrode plasmas evolution, responsible for the gap closure.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Microstructure evolution and magnetic properties of FeB/Pt multilayers and FeBPt composite films

Comparisons of microstructural evolution and magnetic properties were made of a FeB12/Pt10/[FeB1.2/Pt1]{sub 15}/Ta5 nm multilayered structure with a FeB12/Pt10/FeBPt33/Ta5 nm co-deposited structure. The Ta capping layer was used to protect the films from oxidation. Both these samples were sputtered in the same planetary deposition system onto thermally oxidized silicon substrates. They both represent layer-by-layer deposition, with the second type of deposition having atomically fine layers, more than an order of magnitude finer than the first type. The samples were annealed at a range of times, temperatures, and vacuum conditions. X-ray diffraction (XRD), transmission electron microscopy, and alternating gradient magnetometry were employed to characterize the structural and magnetic properties, respectively. Significant differences were observed between the two types of structures. A maximum coercivity of 8.9 kOe was seen for the atomically fine multilayer, about 10% more than that for the coarse multilayer. XRD analysis confirmed that both the coarse and fine multilayers were in the L1{sub 0} phase after annealing. Our results indicate that the co-deposited film, which is really composed of atomically fine multilayers, is superior to the coarse multilayered FeB/Pt for the formation of L1{sub 0}-phase FePt.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

A new Stark decelerator based surface scattering instrument for studying energy transfer at the gas-surface interface

We report on the design and characterization of a new apparatus for performing quantum-state resolved surface scattering experiments. The apparatus combines optical state-specific molecule preparation with a compact hexapole and a Stark decelerator to prepare carrier gas-free pulses of quantum-state pure CO molecules with velocities controllable between 33 and 1000 m/s with extremely narrow velocity distributions. The ultrahigh vacuum surface scattering chamber includes homebuilt ion and electron detectors, a closed-cycle helium cooled single crystal sample mount capable of tuning surface temperature between 19 and 1337 K, a Kelvin probe for non-destructive work function measurements, a precision leak valve manifold for targeted adsorbate deposition, an inexpensive quadrupole mass spectrometer modified to perform high resolution temperature programmed desorption experiments and facilities to clean and characterize the surface.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Demonstration of nitrogen-incorporated ultrananocrystalline diamond photocathodes in a RF gun environment

Quantum efficiency (QE), intrinsic emittance, and robustness are the three most important figures of merit for photocathodes, the first two determine the ultimate achievable brightness of an electron beam, and the third one directly correlates with the complications of a beamline design. Nitrogen-incorporated ultrananocrystalline diamond [(N)UNCD] materials are promising candidates for photocathode applications due to their remarkable electron emission performance as well as the moderate vacuum requirement. Two (N)UNCD photocathodes have been characterized in a realistic RF gun environment with the nicely balanced performance of all three figures of merit. In this work, the QE of the first (N)UNCD cathode (stored in air for two years before the test) was found to be 3.8 x 10 –4 using a 262 nm UV laser and a cathode surface field of 30MV/m. It was found that the QE of the second (N)UNCD sample (grown days before the test) was nearly the same and, therefore, demonstrates the exceptional environmental tolerance of the material. The intrinsic emittance of (N)UNCD was measured to be 1.00 μm/mm.

36 MATERIALS SCIENCE↗

Reaching high laser intensity by a radiating electron

The question of whether an electron radiating its energy away during the interaction with a laser can reach the region of highest intensity with energy high enough to make a number of different phenomena observable is one of the most studied and most important in strong field quantum electrodynamics. Here a simple analytical estimate for an average electron energy evolution is proposed and benchmarked against particle-in-cell simulations. Here, these results are used to estimate the electron and laser pulse properties required to make vacuum Cherenkov emission observable.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Properties of Cu(In,Ga,Al)Se{sub 2} thin films fabricated by magnetron sputtering

Cu(In,Ga,Al)Se{sub 2} (CIGAS) thin films were studied as an alternative absorber layer material to Cu(In{sub x}Ga{sub 1−x})Se{sub 2}. CIGAS thin films with varying Al content were prepared by magnetron sputtering on Si(100) and soda-lime glass substrates at 350 °C, followed by postdeposition annealing at 520 °C for 5 h in vacuum. The film composition was measured by an electron probe microanalyzer while the elemental depth profiles were determined by secondary ion mass spectrometry. X-ray diffraction studies indicated that CIGAS films are single phase with chalcopyrite structure and that the (112) peak clearly shifts to higher 2θ values with increasing Al content. Scanning electron microscopy images revealed dense and well-defined grains, as well as sharp CIGAS/Si(100) interfaces for all films. Atomic force microscopy analysis indicated that the roughness of CIGAS films decreases with increasing Al content. The bandgap of CIGAS films was determined from the optical transmittance and reflectance spectra and was found to increase as Al content increased.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Molecular beam epitaxial growth and scanning tunneling microscopy studies of the gallium rich trench line structure on N-polar w-GaN( 000 1 &#xAF; )

In addition to the usual set of the well-known reconstructions that have been observed on the N-polar GaN surface, namely 1×1, 3×3, 6×6, and c(6×12), an additional structure is occasionally seen at high Ga coverage, which can extend over a large area of the surface. This structure, which is referred to as trench line structure, is partially ordered and consists of parallel-running dark (trench) lines separating wide and narrow strips of atomically ordered regions. There are also randomly placed defects interrupting the ideal ordering. Reflection high energy electron diffraction and scanning tunneling microscopy in ultrahigh vacuum are applied to investigate this trench line structure on samples prepared using molecular beam epitaxy. It is found that the trench line structure results from annealing the Ga-rich c(6×12) at high temperature followed by quenching to room temperature. By careful comparison of the scanning tunneling microscopy images with those from neighboring c(6×12) regions, it is found that the trench line structure can be decomposed into subunits of the c(6×12). Using these subunits, some simple models for the trench line structure are created. It is proposed that the trench line structure is composed of two primary c(6×12) subunits consisting of first and second layer Ga adatoms and that the trench lines are regions devoid of Ga adatoms, going down to the Ga adlayer.

36 MATERIALS SCIENCE↗

High-precision measurement of the W boson mass with the CDF II detector

The mass of the W boson, a mediator of the weak force between elementary particles, is tightly constrained by the symmetries of the standard model of particle physics. The Higgs boson was the last missing component of the model. After observation of the Higgs boson, a measurement of the W boson mass provides a stringent test of the model. We measure the W boson mass, M W , using data corresponding to 8.8 inverse femtobarns of integrated luminosity collected in proton-antiproton collisions at a 1.96 tera–electron volt center-of-mass energy with the CDF II detector at the Fermilab Tevatron collider. A sample of approximately 4 million W boson candidates is used to obtain M W = 80,433.5 ± 6.4 stat ± 6.9 syst = 80,433.5 ± 9.4 MeV/c 2 , the precision of which exceeds that of all previous measurements combined (stat, statistical uncertainty; syst, systematic uncertainty; MeV, mega–electron volts; c, speed of light in a vacuum). This measurement is in significant tension with the standard model expectation.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

LEReC Machine Protection System

The LEReC Machine Protection System (MPS) is designed to alleviate the risk of possible damage to in-vacuum components of the accelerator from high power electron beam.

43 PARTICLE ACCELERATORS↗