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At least 883 records · Page 49

All sources NASA NTRS DOE OSTI

DOE OSTI2023

Exploring the interfacial structure and crystallinity for direct growth of Mn 3 Sn(0001) on sapphire (0001) by molecular beam epitaxy

The Kagome antiferromagnet Mn 3 Sn has garnered a lot of attention due to the presence of interesting properties such as anomalous Hall effects and Nernst effects. Until now, few papers have been reported to grow using molecular beam epitaxy with a buffer layer or on other substrates. In this paper, we discuss the synthesis of crystalline Mn 3 Sn layers, prepared on Al 2 O 3 (0001) without a buffer layer using molecular beam epitaxy. The growth is monitored in-situ using reflection high energy electron diffraction and measured ex-situ using X-ray diffraction, Rutherford back-scattering, and cross-sectional scanning transmission electron microscopy. The samples were deposited at 524 ± 5 °C, with an Mn: Sn atomic flux ratio of 3.2:1 for 90 minutes. Orientation relationships between the Mn 3 Sn films and the sapphire substrates are determined from in-plane and out-of-plane measurements. Our analysis indicates that the resulting film is predominantly c−plane oriented. Lastly, the samples prepared in this way were found to be discontiguous, showing a 3-dimensional morphology. According to first-principles calculations, the Mn 3 Sn exhibits a displaced Kagome structure in the very first stages of growth, for 2ML and 4ML growth on Al 2 O 3 (0001). This result is corroborated by calculating the surface formation energies and explains the observed RHEED patterns.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

NASA NTRS1981

DC calibration of the strain sensitivity of a single mode optical fiber interferometer

The strain sensitivity of an optical fiber interferometer developed for the detection of pulsed ultrasonic waves in solids has been calibrated. The optical paths in both signal and reference arms of the interferometer are through similar 2 m lengths of ITT-110 single mode fibers mode stripped by index matching at both ends and attached to opposite sides of a 30 cm plexiglas bar 0.3 cm thick. Light from the output ends of both fibers was superimposed to form an interference fringe pattern that was interrogated in the far field to give a signal proportional to the differential optical fiber path length. Strain sensitivity was determined by comparing data obtained by clamping and bending the bar at different lengths to simple cantilever beam theory. Calibration indicates a minimum theoretical detectable strain of less than 10 to the -10.

Claus, R. O.↗

NASA NTRS1981

DC calibration of the strain sensitivity of a single mode optical fiber interferometer

The strain sensitivity of an optical fiber interferometer developed for the detection of pulsed ultrasonic waves in solids was calibrated. Light from the output ends of both fibers was superimposed to form an interference fringe pattern that was interrogated in the far field to give a signal proportional to the differential optical fiber path length. Strain sensitivity is determined by comparing data obtained by clamping and bending the bar at different lengths to simple cantilever beam theory. A minimum theoretical detectable strain of less than 10 to the minus 10th power is indicated.

Claus, R. O.↗

DOE OSTI2021

Nanofabrication of silicon surfaces for reduced virus adhesion

Nanofabrication is a remarkably effective technique to create desirable nanoscale patterns. Here, the effect of surface nanofabrication on altering virus adhesion to the substrates was examined. Arrays of nanoholes, 50 nm in diameter, 22 nm deep, and 100 nm in pitch distance, were created on silicon (Si) wafers by electron-beam lithography and reactive ion etching. MS2 coliphage, which is 26 ± 2 nm in diameter and is frequently used as a surrogate for human viruses, was applied to investigate the interaction between the virions and smooth or nanostructured Si surfaces. Scanning electron microscopy and atomic force microscopy along with surface wettability analyses revealed that the nanofabrication had the effect of reducing not only the number of viruses attached but also the strength of virus adhesion. These effects were ascribed to the presence of nanoholes, which were inaccessible to the virions due to the unique surface topographical parameters and the surface chemistry, resulting in the decrease of the overall solid contact area for MS2 attachment. The periodic spacing of the nanoholes also limited the unit landing area for MS2 particles, restricting the formation of MS2 aggregates and leading to the reduced amount of MS2 attachment. We anticipate that smart design of a surface’s chemical composition and nanostructure will offer a feasible solution to improve mitigations for controlling viral adhesion and transmission to and from food contact surfaces.

36 MATERIALS SCIENCE↗

NASA NTRS1985

Optical Mounts for Cryogenic Beam Splitters

Spring-loaded optical mounts maintain flatness and alinement of rigid, framed, or pellicle beam splitters over wide temperature range, despite differences in thermal expansion amoung materials. Mounts permit optical adjustments at ambient temperature even though optical system operated subsequently within few degrees of absolute zero. Mounts useful as holders for integrated-circuit master patterns, survey targets, vibrating membranes, noise- or pressure-sensing membranes, osmosis filters, and fuel-cell elements.

Rudman, A. A.↗

DOE OSTI2025

Azimuthal and axial structures in 3D particle-in-cell simulation of Penning discharge

We report the results of a 3D particle-in-cell simulation of cylindrical Penning discharge with the axial magnetic field in the so-called reflex configuration, where the cathode and anti-cathode are biased to the same negative potential. The discharge is supported by thermal electron emission from the cathode. Electron and ion collisions, including ionization, are fully accounted for. The emphasis is on a specific regime in which the plasma potential at the center of the discharge is positive with respect to the chamber walls, serving as an anode. Spatial and temporal scales of the observed azimuthal and axial fluctuations and structures are characterized. It is suggested that azimuthal structures are caused by the dissipative gradient-drift instability. We find that the axial fluctuations related to the plasma-beam instabilities are weakly correlated with the azimuthal perturbations of the density, so that the azimuthal modes rotate as a whole and do not show any axial shear. The behavior of the electric potential is more involved, demonstrating intermittent standing wave and propagating structures in the axial direction that modulate the electron transport, producing the standing wave pattern (along the z-direction) in the radial electron flux.

3D PIC simulation of discharge↗

NASA NTRS2010

Study of Fabry-Perot Etalon Stability and Tuning for Spectroscopic Rayleigh Scattering

The Fabry-Perot interferometer is a commonly employed instrument for resolving the spectrum of molecular Rayleigh scattered light for the purpose of evaluating flow properties such as gas velocity and temperature. Rayleigh scattered light from a focused laser beam can be directly imaged through a solid Fabry-Perot etalon onto a CCD detector to provide the spectral content of the scattered light. The spatial resolution of the measurements is governed by the locations of interference fringes. The location of the fringes can be changed by altering the etalon?s physical characteristics, such as thickness and index of refraction. For a fused silica solid etalon the physical properties can be adjusted by changing the etalon temperature; hence changing the order of the interference pattern and the physical fringe locations. Controlling the temperature of the etalon can provide for a slow time-response spatial scanning method for this type of etalon system. A custom designed liquid crystal Fabry-Perot (LCFP) can provide for a fast time-response method of scanning the etalon system. Voltage applied to the liquid crystal interface sets the etalon?s properties allowing Rayleigh measurements to be acquired at varying spatial locations across the image of the laser beam over a very short time period. A standard fused silica etalon and a tunable LCFP etalon are characterized to select the system that is best suited for Rayleigh scattering measurements in subsonic and supersonic flow regimes. A frequency-stabilized laser is used to investigate the apparent frequency stability and temperature sensitivity of the etalon systems. Frequency stability and temperature sensitivity data of the fused silica and LCFP etalon systems are presented in this paper, along with measurements of the LCFP etalon?s tuning capabilities. Rayleigh scattering velocity measurements with both etalon systems are presented, in an effort to determine which etalon is better suited to provide optical flow measurements of velocity, temperature, and density.

Clem, Michelle M.↗

DOE OSTI2021

Statistical Correlation Between Quantum Entanglement and Spin–Orbit Coupling in Crossed Beam Molecular Dynamics

Non-classical features like interference are already being harnessed to control the output of chemical reactions. However, quantum entanglement which is an equally enigmatic many-body quantum correlation can also be used as a powerful resource yet has eluded explicit attention. In this report, an experimental scheme under the crossed beam molecular dynamical setup, with the F + HD reaction, is proposed aiming to study the possible influence of entanglement within reactant pairs on the angular features of the product distribution. The aforesaid reaction has garnered interest recently, as an unusual horseshoe shape pattern in the product (HF) distribution was observed, which has been attributed to the coupling of spin and orbital degrees of freedom. An experimental scheme is proposed aiming to study the possible influence of entanglement on the necessity for the inclusion of such spin–orbit characteristics, under circumstances wherein the existence of entanglement and spin–orbit interaction is simultaneously detectable. The attainable results are further numerically simulated highlighting specific patterns corresponding to various possibilities. Finally, such studies if extended can provide unforeseen mechanistic insight into analogous reactions, too, from the lens of quantum information.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

DOE OSTI2022

Infrared nanospectroscopy characterization of metal oxide photoresists

Implementation of extreme ultraviolet (EUV) lithography in high-volume semiconductor manufacturing requires a reliable and scalable EUV resist platform. A mechanistic understanding of the pros and cons of different EUV resist materials is critically important. However, most material characterization methods with nanometer resolution use an x-ray photon or electron beam as the probe, which often cause damage to the photoresist film during measurement. Here, we illustrated the use of non-destructive infrared nanospectroscopy [or nano-Fourier-Transform infrared spectroscopy (nano-FTIR)] to obtain spatially resolved composition information in patterned photoresist films. Further, clear evidence of exposure-induced chemical modification was observed at a spatial resolution down to 40 nm, well below the diffraction limit of infrared light. With improvements, such a nano-FTIR technique with nanoscale spatial resolution, chemical sensitivity, and minimal radiation damage can be a promising candidate for the fundamental study of material properties relevant to EUV lithography.

36 MATERIALS SCIENCE↗

DOE OSTI2024

Undulator radiation of single electrons: coherence length and quantum-optical properties

The aims of the CLARA experiment at the Fermilab Integrable Optics Test Accelerator (IOTA) were to directly measure the coherence length of undulator radiation emitted by a single electron and to test whether the radiation is in a pure classical Glauber coherent state or in a quantum mixture of coherent and Fock states. We used a Mach-Zehnder interferometer (MZI) to study visible radiation generated by 150-MeV electrons circulating in the ring. The relative delay between the two arms of the MZI was adjusted by varying the length of one of them with a resolution of 10 nm. The intensity of the circulating beam spanned several orders of magnitude, down to single electrons. A pair of single-photon avalanche diodes (SPADs) was placed at the output of the MZI arms to detect photocounts with high efficiency and timing resolution. We describe the observed interference patterns and photocount rates as a function of interferometer delay and discuss their implications.

43 PARTICLE ACCELERATORS↗

DOE OSTI2024

Undulator Radiation of Single Electrons: Coherence Length and Quantum-Optical Properties

43 PARTICLE ACCELERATORS↗

DOE OSTI2024

Track vs Shower Discrimination in the Event Reconstruction of the ICARUS Experiment

The ICARUS collaboration has employed the 760-ton T600 liquid argon TPC detector in a successful three-year physics run at the underground LNGS laboratory, performing a sensitive search for LSND-like anomalous appearance in the CERN Neutrino to Gran Sasso beam, which contributed to the constraints on the allowed neutrino oscillation parameters to a narrow region around 1 eV. After a significant overhaul at CERN, the T600 detector has been installed at Fermilab. The detector commissioning phase lasted until June 2022, then ICARUS moved to data taking for neutrino oscillation physics collecting events from the Booster Neutrino Beam (BNB) and the Neutrinos at the Main Injector (NuMI) beam off-axis. The initial experiment goals are to either confirm or refute the claim by Neutrino-4 short-baseline reactor experiment, perform measurements of neutrino cross sections with the NuMI beam and several Beyond Standard Model searches. Then, ICARUS will jointly search for evidence of sterile neutrinos with the Short-Baseline Near Detector (SBND). In this contribution, we discuss recent changes to the standard TPC event reconstruction that uses Pandora, a pattern recognition software common to liquid argon-based detectors. In particular, we performed a new training of the Boosted Decision Tree (BDT) employed to separate track-like and shower-like reconstructed particles using Monte Carlo simulations of neutrino events from BNB in ICARUS. We compare the discrimination capabilities of the old and new BDT training and discuss further improvements of this algorithm.

43 PARTICLE ACCELERATORS↗

NASA NTRS1973

Integrated circuit package with lead structure and method of preparing the same

A beam-lead integrated circuit package assembly including a beam-lead integrated circuit chip, a lead frame array bonded to projecting fingers of the chip, a rubber potting compound disposed around the chip, and an encapsulating molded plastic is described. The lead frame array is prepared by photographically printing a lead pattern on a base metal sheet, selectively etching to remove metal between leads, and plating with gold. Joining of the chip to the lead frame array is carried out by thermocompression bonding of mating goldplated surfaces. A small amount of silicone rubber is then applied to cover the chip and bonded joints, and the package is encapsulated with epoxy resin, applied by molding.

Kennedy, B. W.↗

NASA NTRS1980

Some effects of motion and plane reflecting surfaces on the radiation from acoustic sources

The effects of translatory and rotational motion and of the proximity of ground surface on the radiation from acoustic monopole and dipole sources are discussed together with the key equations. It is shown that interference patterns are produced by reflection and absorption at a plane surface and that consequently, the far-field directivity of an acoustic source near the ground can be substantially altered from its free-field value. The kinematic effects discussed include the beaming of sound in the direction of source motion and the shifting of the observer source frequency in a directionally dependent manner. The effects are illustrated by experimental data.

Lansing, D. L.↗

NASA NTRS1986

Observations of mesoscale vertical velocities around frontal zones

Vertical velocity and reflectivity data obtained with a VHF Doppler radar over a 15-day period in October and November of 1981 are analyzed. Standard radiosonde data and surface observations were used to locate two occluded fronts, two warm fronts, and a cold front that passed the radar site. These fronts are also evident in the radar reflectivity data. Most studies of the vertical circulation patterns associated with mososcale systems have used precipitation and cloud formations as tracers. Unlike other observational techniques, the VHF radar permits the continuous measurement of the three-dimensional air velocity vector in time and height from a fixed location. With the beam in a vertically pointing position, signals are scattered from turbulent variations in the refractive index with half the scale of the radar wavelength and by regions with sudden changes in the refractive index associated with horizontally stratified layers. Generally, the strongest echoes occur at the maximum in the vertical gradient of refractivity, usually at the base of a temperature inversion, such as the tropopause. VHF radars can also be used to locate atmospheric fronts, which are characterized by static stability, large horizontal temperature gradients, large vorticities, and vertical wind shears. These radars can provide the velocity field data needed to study wave motions associated with fronts and compare the actual vertical circulation to theoretical predictions.

Dennis, T. S.↗

NASA NTRS1991

Megawatt Square Microwave Feed Horn

Prototype multiflare square horn antenna designed to combine phased 8.51-GHz outputs of four 250-kW amplifiers into single 1-MW continuous-wave beam. Main lobe and side lobes reasonably below main lobe obtained by choosing tapers of multiflare horn to couple power from TE(Sub10) mode into three other modes. Intended to illuminate subreflector of 70-m-diameter radar antenna. Nearly duplicates radiation pattern of corrugated round feed horn.

Hoppe, Daniel J.↗

NASA NTRS1999

Electronically conducting polymers with silver grains

The present invention provides electronically conducting polymer films formed from photosensitive formulations of pyrrole and an electron acceptor that have been selectively exposed to UV light, laser light, or electron beams. The formulations may include photoinitiators, flexibilizers, solvents and the like. These solutions can be used in applications including printed circuit boards and through-hole plating and enable direct metallization processes on non-conducting substrates. After forming the conductive polymer patterns, a printed wiring board can be formed by sensitizing the polymer with palladium and electrolytically depositing copper.

Murphy, Oliver J.↗

NASA NTRS2001

Method of forming electronically conducting polymers on conducting and nonconducting substrates

Murphy, Oliver J.↗