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At least 883 records · Page 49

Structural phase purification of bulk HfO 2 :Y through pressure cycling

We combine synchrotron-based infrared absorption and Raman scattering spectroscopies with diamond anvil cell techniques and first-principles calculations to explore the properties of hafnia under compression. We find that pressure drives HfO 2 :7%Y from the mixed monoclinic ( P 2 1 / c ) + antipolar orthorhombic ( Pbca ) phase to pure antipolar orthorhombic ( Pbca ) phase at approximately 6.3 GPa. This transformation is irreversible, meaning that upon release, the material is kinetically trapped in the Pbca metastable state at 300 K. Compression also drives polar orthorhombic ( P c a 2 1 ) hafnia into the tetragonal ( P 4 2 / n m c ) phase, although the latter is not metastable upon release. These results are unified by an analysis of the energy landscape. The fact that pressure allows us to stabilize targeted metastable structures with less Y stabilizer is important to preserving the flat phonon band physics of pure HfO 2 .

36 MATERIALS SCIENCE↗

Inversion technique to obtain local ion temperature profiles for an axisymmetric plasma with toroidal and radial velocities

A matrix inversion technique is derived to calculate local ion temperature from line-integrated measurements of an extended emission source in an axisymmetric plasma which exactly corrects for both toroidal velocity and radial velocity components. Local emissivity and toroidal velocity can be directly recovered from line-integrated spectroscopic measurements, but an independent measurement of the radial velocity is necessary to complete the temperature inversion. The extension of this technique to handle the radial velocity is relevant for magnetic reconnection and merging compression devices where temperature inversion from spectroscopic measurements is desired. A simulation demonstrates the effects of radial velocity on the determination of ion temperature.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

$S$ Hmax orientation in the Alpine region from observations of stress-induced anisotropy of nonlinear elasticity

The orientation of $S$ Hmax is commonly estimated from in situ borehole breakouts and earthquake focal mechanisms. Borehole measurements are expensive, and therefore sparse, and earthquake measurements can only be made in regions with many well-characterized earthquakes. Here, we derive the stress-field orientation using stress-induced anisotropy in nonlinear elasticity. In this method, we measure the strain derivative of velocity as a function of azimuth. We use a natural pump-probe (NPP) approach which consists of measuring elastic wave speed using empirical Green’s functions (probe) at different points of the earth tidal strain cycle (pump). The approach is validated using a larger data set in the Northern Alpine Foreland region where the orientation of maximum horizontal compressive stress is known from borehole breakouts and drilling-induced fractures. The technique resolves NNW-SSW to N-S directed $S$ Hmax which is in good agreement with conventional methods and the recent crustal stress model. We confirm that the NPP method can be applied to dense large-scale seismic arrays. The technique is then applied to the Southern Alps to understand the contemporary stress pattern associated with the ongoing deformation due to counterclockwise rotation of the Adriatic plate with respect to the European plate. Our results explain why the two major faults in Northeastern Italy, the Giudicarie Fault and the Periadriatic Line (Pustertal–Gailtal Fault) are currently inactive, while the currently acting stress field allows faults in Slovenia to deform actively. We have demonstrated that the pump-probe method has the potential to fill in the measurement gap left by conventional approaches, both in terms of regional coverage and in depth.

58 GEOSCIENCES↗

Dynamic compression of [100] MgF 2 single crystals: Shock-induced polymorphism to highly coordinated structures

AX 2 -type compounds exhibit a rich and complex series of phase transitions under compression. The high-pressure polymorphism of rutile-type AX 2 difluorides can be characterized by a typical sequence from rutile type → Ca Cl 2 type → HP – Pd F 2 type → cotunnite type . Relative to dioxides, the reduced valence and ionic radius of the F – anion in rutile-type MgF 2 (sellaite) results in lowered transition pressures, making it a useful analog for SiO 2 and other dioxides. In this work, MgF 2 single crystals were shock-compressed along the [100] direction to 24 to 120 GPa using plate impact techniques, and wave profiles were measured using laser interferometry. At low stresses (24 to 44 GPa), we observe features consistent with an elastic–inelastic response, followed by a phase transformation. Peak stress-density states in this stress range are consistent with those expected for the modified fluorite-type (HP- PdF 2 ) phase or a related structure. At higher stresses (69 to 91 GPa), we observe a two-wave structure with peak stress-density states consistent with transformation to a denser and likely more highly coordinated phase such as the cotunnite-type structure. Furthermore, at 120 GPa, only a single wave structure is observed, indicating that the wave profile features observed at lower stresses are overdriven.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Inversion technique to obtain local ion temperature profiles for an axisymmetric plasma with toroidal and radial velocities

A matrix inversion technique is derived to calculate local ion temperature from line-integrated measurements of an extended emission source in an axisymmetric plasma which exactly corrects for both toroidal velocity and radial velocity components. Local emissivity and toroidal velocity can be directly recovered from line-integrated spectroscopic measurements, but an independent measurement of the radial velocity is necessary to complete the temperature inversion. The extension of this technique to handle the radial velocity is relevant for magnetic reconnection and merging compression devices where temperature inversion from spectroscopic measurements is desired. A simulation demonstrates the effects of radial velocity on the determination of ion temperature.

ion temperature↗

LA-R43S6-L1 Postshot Report [Slides]

The Ranchero LA-R43S6-L1 test (formerly referred to as LA-43S-L1. The R specifically designates it is a Ranchero device and the 6 indicates a 6” high explosive charge diameter in anticipation of using larger diameters in the future.) was conducted on 3/8/17 with good success. The experiment was the first test of a “Swooped” Ranchero flux compression generator (FCG), and the load for the test was an aluminum imploding liner. In addition to the swoop, the stator was anodized to provide an insulating layer instead of one or more layers of polyethylene as had been the case for all earlier Ranchero tests. Using the Firing point TA-39-88 capacitor bank, 3.5 MA was delivered to the FCG for the initial magnetic field, and 36.4 MA were delivered to the load having an initial inductance of 2.5 nH. Implosion speeds over 1.1 cm/us were recorded, which exceeds previous LANL solid liner experimental results. The test was diagnosed with 18 PDV channels, 12 of which recorded liner implosion data, and the other 6 of which tracked the FCG armature during flux compression. These armature expansion data recorded during flux compression are the first of their kind, and it was previously unknown, due to unknown effects of the SF 6 in the flux compression volume, whether or not the expansion could be recorded using the PDV technique. Post shot 2D MHD calculations employed a complete external circuit model, and an improved flux diffusion model not available prior to the test. Results from these simulations show very good agreement with the experimental result. Four PDV channels recorded the liner implosion viewed radially outward from the center of the liner. All four of these probes recorded implosion velocities greater that 1 cm/µs, with the cylindrical center displaced by ~2 mm from actual center. Four PDV channels looked at +10° angles from the CMU wall, and four looked at -10° angles. A glide plane interaction is shown moving toward the center of the liner in MHD calculations, and PDV probes provide confirmation. The high explosive (HE) in the LA-R43S6-L1 test was PBX 9501 which had to be glued together in many pieces, and the test was preceded by a camera test to verify that the PBX 9501 could be assembled with acceptable tolerance in glue joints to prevent severing the armature during expansion. The camera test verified an acceptable armature performance, and results are given in complete detail in a post shot report LA-UR-19-20124, and summarized here. This report provides complete detail of the considerable body of data obtained on the test and in the post shot calculations. It is prepared in Power Point for ease of preparation and future review. Shot documentation available in the LANL on-line library are included as references, and non-referenceable documents will be cited and stored in an LA- R43S6-L1 post shot folder stored on an M-6 shared drive. Fabrication drawings are also maintained in an M-6 shared drive and paper files are available from M-6 personnel. This report will be maintained as a PowerPoint document on the shared drive, as well, since included movies will play and graphs from Excel files retain information in the PowerPoint versions. PDF versions are required for clearance and are not to large to send by e-mail.

42 ENGINEERING↗

Applications of dynamic measurement techniques to wind-tunnel testing

The uses of laser Doppler velocimeter, hot wire, and surface hot film techniques in the study of turbulent flows are described, and data obtained in compressible flows are discussed. Applications are illustrated with measurements of wind tunnel freestream turbulence characteristics and with data obtained in transitional, turbulent, and separated shear flows. A new method which was developed for the study of time dependent and unsteady turbulent flows is also presented.

Owen, F. K.↗

A composite velocity procedure for the compressible Navier-Stokes equations

A new boundary-layer relaxation procedure is presented. In the spirit of the theory of matched asymptotic expansions, a multiplicative composite of the appropriate velocity representations for the inviscid and viscous regions is prescribed. The resulting equations are structured so that far from the surface of the body the momentum equations lead to the Bernoulli relation for the pressure, while the continuity equation reduces to the familiar compressible potential equation. Close to the body surface, the governing equations and solution techniques are characteristic of those describing interacting boundary-layers; although, the full Navier-Stokes equations are considered here. Laminar flow calculations for the subsonic flow over an axisymmetric boattail simulator geometry are presented for a variety of Reynolds and Mach numbers. A strongly implicit solution method is applied for the coupled velocity components.

Khosla, P. K.↗

Unsteady transonic heat transfer in a transient facility

A facility for making heat transfer measurements on solid surfaces using transient techniques is constructed. The facility being constructed is a Ludweig tube with isentropic compression heating (LICH tube). The work completed is detailed as is the work remaining in order to complete the facility and make useful heat transfer measurements. The scope of the project is briefly discussed along with an overall appraisal of the progress.

Lagraff, J. E.↗

Measure of displacement around holes in composite plates subjected to quasi-static compression

Contour maps of thickness changes were obtained for three quasi-isotropic graphite-epoxy plates with central holes, loaded in compression. Thickness changes were determined for six load increments from nearly zero to within a few percent of the failure load. The largest change of thickness occurred near the hole but not at the boundary of the hole. Below 90 percent of the failure load, the thickness changes were nearly proportional to load. Irregularities of thickness changes occurred in zones of compressive stresses and they were attributed to localized fiber buckling. A new optical technique was developed to measure thickness changes with high sensitivity. It utilizes a comparatively simple means of holographic interferometry on both sides of the specimen, followed by additive moire to obtain thickness changes as the sum of the out-of-plane displacements. Sensitivity was 12.5 x 10 to the -6 power in. per fringe order. The fringe patterns represent thickness changes uniquely, even when specimen warpage and consequent out-of-plane displacements are very large.

Duke, J. C., Jr.↗

AOTV bluff body flow - Relaxation algorithm

Preliminary investigations have led to the consideration of two classes of energy efficient aeroassisted orbital transfer vehicle (AOTV) concepts, with high and low L/D. The AOTV represent reentry space vehicles which are to fly hypersonically in the continuum upper reaches of the atmosphere. Problems arise in connection with convective and nonequilibrium radiative heating. As the possibilities for obtaining needed information by experimentation are limited, reliance must be placed on computational techniques to simulate testing of design concepts. A new relaxation algorithm for the compressible Navier-Stokes equations has been developed in the context of recent work with a conservative flux difference eigenvector split implicit upwind scheme CSCM (conservative supracharacteristics method). Attention is given to the CSCM implicit method, and early results for axisymmetric bluff body flow including complete forebody and base flow for a free flight range model drag brake AOTV.

Lombard, C. K.↗

Summary of investigations of engine response to distorted inlet conditions

A survey is presented of experimental and analytical experience of the NASA Lewis Research Center in engine response to inlet temperature and pressure distortions. Results of experimental investigations and analytical modeling are reviewed together with a description of the hardware and the techniques employed. Distortion devices successfully simulated inlet distortion, and knowledge was gained on compression system response to different types of distortion. A list of NASA research references is included.

Biesiadny, Thomas J.↗

Investigation of chemically reacting and radiating supersonic internal flows

The two-dimensional spatially elliptic Navier-Stokes equations are used to investigate the chemically reacting and radiating supersonic flow of the hydrogen-air system between two parallel plates and in a channel with a ten degree compression-expansion ramp at the lower boundary. The explicit unsplit finite-difference technique of MacCormack is used to advance the governing equations in time until convergence is achieved. The chemistry source term in the species equation is treated implicitly to alleviate the stiffness associated with fast reactions. The tangent slab approximation is employed in the radiative flux formation. Both pseudo-gray and nongray models are used to represent the absorption characteristics of the participating species. Results obtained for specific conditions indicate that the radiative interaction can have a significant influence on the flow field.

Mani, M.↗

Numerical solutions of chemically reacting and radiating flows

The two-dimensional spatially elliptic Navier-Stokes equations are used to investigate the chemically reacting and radiating supersonic flow of the hydrogen-air system between two parallel plates and in a channel with a ten-degree compression-expansion ramp at the lower boundary. The explicit unsplit finite-difference technique of MacCormack is used to advance the governing equations in time until convergence is achieved. The chemistry source term in the species equation is treated implicitly to alleviate the stiffness associated with fast reactions. The tangent slab approximation is employed in the radiative flux formulation. Both pseudo-gray and nongray models are used to represent the absorption-emission characteristics of the participating species. Results obtained for specific conditions indicate that the radiative interaction can have a significant influence on the flow field.

Mani, M.↗

Development and calibration of buried wire gages for wall shear stress measurements in fluid flow

Special methods were developed to arrange 'Buried Wire Gage' inserts flush to the contoured flow surfaces of instrument plugs of a boundary-layer flow apparatus. The fabrication process was aimed at producing proper bonding of the sensor wire to the substrate surface, without causing excessive surface waviness. A large number of gages were built and first calibrated for the resistance-temperature characteristics. The gages were then installed in a flow calibration apparatus and operated from a constant temperature anemometer system for a series of flow settings to derive the calibration constants of each of the gages. The flow settings included a range of subsonic freestream Mach numbers in order to help establish the gage calibration characteristics for compressible flow fields. This paper provides a description of the buried wire gage technique, an explanation of the method evolved for making proper gages, the procedure for calibrating the gages and the results of measurements performed for determining the calibration constants.

Murthy, Sreedhara V.↗

Quantitative characterization of a nonreacting, supersonic combustor flowfield using unified, laser-induced iodine fluorescence

A calibrated, nonintrusive optical technique, laser-induced iodine fluorescence (LIIF) was used to quantify the steady, compressible flowfield of a nonreacting, supersonic combustor. The combustor was configured with single and staged, transverse-air injection into a supersonic-air freestream behind a rearward-facing step. Pressure, temperature, two-velocity components, and injectant mole fraction were measured with high spatial resolution in the three-dimensional flowfields. These experimental results provide a benchmark set of data for validation of computational fluid dynamic (CFD) codes being developed to model supersonic combustor flowfields.

Fletcher, D. G.↗

Modeling of turbulent shear flows

The current progress is documented in the research and development of modeling techniques for turbulent shear flows. These include a two-scale model for compressible turbulent flows and a new energy transfer model. The former represents the status of the efforts to identify compressibility effects in turbulence. The energy transfer model refines a weakly nonlinear wave model developed earlier, which models directly the turbulent large structures. The objective of these activities is to develop second-order closures for compressible turbulent flows.

Liou, William W.↗

Nearly incompressible fluids. II - Magnetohydrodynamics, turbulence, and waves

The theory of nearly incompressible (NI) fluid dynamics developed previously for hydrodynamics is extended to magnetohydrodynamics (MHD). Based on a singular expansion technique, modified systems of fluid equations are obtained for which the effects of compressibility are admitted only weakly in terms of the different possible incompressible solutions. NI MHD represents the interface between the compressible and incompressible magnetofluid descriptions in the subsonic regime. It is shown that three distinct NI descriptions exist corresponding to each of the three possible plasma beta regimes. The detailed theory of weakly compressible corrections to the various incompressible MHD descriptions is presented, and the implications for the solar wind are discussed.

Zank, G. P.↗