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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 883 records · Page 49
All sourcesNASA NTRSDOE OSTI
DOE OSTI2017

Nuclear magnetic resonance probe head design for precision strain control

Here, we present the design and construction of an NMR probe to investigate single crystals under strain at cryogenic temperatures. The probe head incorporates a piezoelectric-based apparatus from Razorbill Instruments that enables both compressive and tensile strain tuning up to strain values on the order of 0.3% with a precision of 0.001%. 75 As NMR in BaFe 2 As 2 reveals large changes to the electric field gradient and indicates that the strain is homogeneous to within 16% over the volume of the NMR coil.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2018

Variable location channels to improve efficiency and precision for direct ∇ T e measurements and high spatial resolution T e -profile measurements using electron cyclotron emission

Electron cyclotron emission (ECE) diagnostics that use variable location channels based on yttrium iron garnet (YIG) bandpass filters improve the precision and the efficiency of measurements of electron temperature (T e ) profiles and fluctuations (δT e ). These variable frequency filters were substituted for fixed frequency filters in the intermediate frequency section to achieve the required higher resolution over a target radial range, just before the experiment. In this paper, we present the proof-of-principle for high temporal resolution measurement of the electron temperature gradient, via real-time slewing of a YIG filter for relocation of an ECE channel during a long pulse. The key component is the application of YIG tunable filters with their narrow bandwidth and capability for a high slew rate of their center frequency. This application permits fast relocation of the ECE channels for direct measurement of the gradient and close spacing of channels to investigate the magnetic island’s dynamic behavior.

47 OTHER INSTRUMENTATION↗
DOE OSTI2019

Precision Flexure Stages Design for a Compact Multilayer Laue Lens Test Bed for Hard X-ray Nanofocusing

Both the Advanced Photon Source (APS) at Argonne National Laboratory (ANL) and the Beijing Synchrotron Radiation Facility (BSRF) at Institute of High Energy Physics (IHEP) have a keen interest in the development of a compact Multilayer Laue Lens (MLL) test bed for hard x-ray nanofocusing. Recently, collaboration between ANL and IHEP, as a part of the Argonne Strategic Partnership Project (SPP) 85J05, has produced designs of precision flexure stages for a compact MLL test bed for hard x-ray nanofocusing using commercial flexural pivots and Argonne developed laminar nanopositioning flexures. Two sets of the new flexure stages will be built with the new designs, one for R&D activities at the BSRF for the new planned 6 GeV high energy photon source (HEPS) and one for upgrade of the existing MLL test bed at the APS x-ray optics test beamline. Mechanical design and preliminary test for the MLL test bed flexure stages for Argonne SPP project 85J05 are presented in this paper.

nanopositioning flexure stage↗
DOE OSTI2024

Precision-controlled ultrafast electron microscope platforms. A case study: Multiple-order coherent phonon dynamics in 1T-TaSe2 probed at 50 fs–10 fm scales

We report on the first detailed beam tests attesting the fundamental principle behind the development of high-current-efficiency ultrafast electron microscope systems where a radio frequency (RF) cavity is incorporated as a condenser lens in the beam delivery system. To allow for the experiment to be carried out with a sufficient resolution to probe the performance at the emittance floor, a new cascade loop RF controller system is developed to reduce the RF noise floor. Temporal resolution at 50 fs in full-width-at-half-maximum and detection sensitivity better than 1% are demonstrated on exfoliated 1T-TaSe2 system under a moderate repetition rate. To benchmark the performance, multi-terahertz edge-mode coherent phonon excitation is employed as the standard candle. The high temporal resolution and the significant visibility to very low dynamical contrast in diffraction signals via high-precision phase-space manipulation give strong support to the working principle for the new high-brightness femtosecond electron microscope systems.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2020

High-precision shock equation of state measurements for metallic fluid carbon between 15 and 20 Mbar

Diamond is an efficient ablator material to convert the energy of high-power giant lasers into ablation pressure with applications for High-Energy-Density (HED) science, planetary science, and Inertial Confinement Fusion (ICF) research at the National Ignition Facility (NIF). Unfortunately, current theoretical equation of state models cannot reproduce all the observed experimental data in the multi-megabar regime particularly relevant for HED and ICF research. New experimental data on the behavior of carbon at extreme pressures and temperatures are, therefore, essential to improve our predictive capability to design and analyze dynamic compression experiments for HED or ICF research and build improved equation of state models in the future. In this paper, we report high-precision laser-driven shock compression measurements on diamond single crystals at the Omega Laser Facility. Using ultrafast Doppler optical Velocimetry Interferometer System for Any Reflector (VISAR) to track the leading shock front and a quartz plate as an in situ reference, we obtain relative pressure-density shock equation-of-state measurements between 15 and 20 Mbar with an impedance-matching procedure. We also report shock-and-release measurements in a spherical geometry at the NIF. The new data provide tight constraints on the compressibility of warm dense carbon along the Hugoniot of full density diamond, allowing us to discriminate between existing theoretical equation-of-state models. We find that both LLNL LEOS 9061 and LANL Sesame 7835 models capture well the shock compressibility in the explored range. LANL Sesame 7835 also reproduces well the observed shock-and-release behavior of diamond near 10–20 Mbar.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2021

Using millimeter-sized carbon–deuterium foils for high-precision deuterium–tritium neutron spectrum measurements in direct-drive inertial confinement fusion at the OMEGA laser facility

Millimeter-sized CD foils fielded close (order mm) to inertial confinement fusion (ICF) implosions have been proposed as a game-changer for improving energy resolution and allowing time-resolution in neutron spectrum measurements using the magnetic recoil technique. This paper presents results from initial experiments testing this concept for direct drive ICF at the OMEGA Laser Facility. Additionally, while the foils are shown to produce reasonable signals, inferred spectral broadening is seen to be high (~5 keV) and signal levels are low (by ~20%) compared to expectation. Before this type of foil is used for precision experiments, the foil mount must be improved, oxygen uptake in the foils must be better characterized, and impact of uncontrolled foil motion prior to detection must be investigated.

47 OTHER INSTRUMENTATION↗
DOE OSTI2025

Exploring transport mechanisms in atomic precision advanced manufacturing enabled pn junctions

We investigate the different transport mechanisms that can occur in pn junction devices made using atomic precision advanced manufacturing at temperatures ranging from cryogenic to room temperature. We first elucidate the potential cause of the anomalous behavior observed in the forward-bias response of these devices in recent cryogenic temperature measurements, which deviates from the theoretical response of a silicon Esaki diode. These anomalous behaviors include current suppression at low voltages in the forward-bias response and a much lower valley voltage at cryogenic temperatures than theoretically expected for a silicon diode. To investigate the potential causes of these anomalies, we studied the effects of a few possible transport mechanisms, including band-to-band tunneling, bandgap narrowing, potential impact of non-Ohmic contacts, band quantization, impact of leakage, and inelastic trap-assisted tunneling, through semi-classical simulations. We find that a combination of two sets of band-to-band tunneling (BTBT) parameters can qualitatively approximate the shape of the tunneling current at low bias. This can arise from band quantization and realignment due to the strong potential confinement in δ-layers. We also find that the lower-than-theoretically-expected valley voltage can be attributed to modifications in the electronic band structure within the δ-layer regions, leading to a significant bandgap narrowing induced by the high density of dopants. Finally, we extend our analyses to room temperature operation and predict that trap-assisted tunneling (TAT) facilitated by phonon interactions may become significant, leading to a complex superposition of BTBT and TAT transport mechanisms in the electrical measurements.

band gap↗
DOE OSTI2026

Precision ultranarrow-linewidth resonance excitation (PURE) preparation of a molecular beam of nitric oxide molecules for inelastic scattering with argon

We recently reported a novel technique that utilizes narrow-linewidth lasers to selectively excite molecules into a pure quantum state with a well-resolved, tunable distribution of velocities [O. A. Krohn and D. W. Chandler, J. Phys. Chem. Lett. 15(50), 12455–12463 (2024)]. We refer to the preparation of molecules by this technique as precision ultranarrow-linewidth resonant excitation (PURE) preparation. Here, in this study, we pair this PURE preparation methodology with active frequency stabilization of the quantum cascade laser that drives the excitation. In doing so, highly velocity-resolved packets of molecules are possible, with the limitations of this velocity resolution set by the stability of the laser locking and the spectral linewidth of the transition. We show that side-of-fringe locking to a Doppler-broadened absorption spectrum of our target molecule is sufficiently stable for PURE preparation of molecules for long timescales (several hours) with highly resolved velocity spreads (σ < 3 m/s). To demonstrate the scientific utility of this new capability, we present differential cross sections from scattering between a neat molecular beam of argon and a velocity-selected beam of nitric oxide (NO) in a pure quantum state. We observe well-resolved quantum diffraction oscillations in the forward-scattered collisions as well as general trends consistent with prior characterized collisions of NO + Ar.

Krohn, Olivia A. [Sandia National Laboratories (SN↗
DOE OSTI2013

Development of precision laser goniometer systems

The concept of constructing precision laser goniometer systems, based on integrating a ring laser and an optical angle sensor with the holographic principle of angular scale recording is considered. The concept implies the application of the cross-calibration procedure, aimed at determination of systematic components of the errors of angle sensors, used in the system. The results of the presented system studies demonstrate the error of angular measurements amounting to {approx}0.01''. The results of implementing the proposed concept in the creation of a standard system of the plane angle unit of rigid rotation and the measuring and computing complex for automated control of digital angle transducers with high digit capacity are briefly presented. (laser optics 2012)

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2014

A highly efficient, compact Yb:KYW laser for mobile precision systems

We have developed a promising scheme of a multimodediode-pumped ytterbium laser. The Yb:KYW laser in the cw regime demonstrates record-high differential (40%) and total optical (35%) efficiencies. Mode locking is realised, which allows the scheme to be used for the development of compact laser systems, such as mobile femtosecond precision synthesisers. The peculiarities of the laser operation and ways of further improving its efficiency are discussed. (lasers)

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2016

Precise modulation of laser radiation by an acousto-optic modulator for stabilisation of the Nd : YAG laser on optical resonances in molecular iodine

A system of precise frequency modulation of laser radiation by an acousto-optic modulator, which makes it possible to stabilise the radiation power and simultaneously suppress the residual amplitude modulation to a level of 10{sup -8} of the total laser power at the third harmonic of modulation frequency (∼500 Hz), is presented. The use of this system for the Nd : YAG/I{sub 2} optical frequency standard and application of digital signal synthesis and processing methods provided a level of frequency standard instability as small as ∼10{sup -15} for ∼6 × 10{sup 4} s. (frequency standards)

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2019

Diode laser spectrometer for high-precision measurements

The issues of the development, calibration and putting into operation of a diode laser spectrometer for high-precision measurements are considered. The tests rely on the use of an isolated P20 line of the 00031 – 00001 band of the {sup 12}C{sup 16}O{sub 2} molecule. The spectrometer error budget is analysed. A software programme for the approximation of a spectral line contour is designed and the procedure is analysed. It is shown that, for a baseline with a relative level of 2.3 × 10{sup −5}, it is optimal to use no more than six fitting parameters in the line contour approximation. The measured integral intensity of the analytical line constitutes 5.3865(85) × 10{sup −23} cm per molecule. (laser spectroscopy)

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2019

Magic wavelengths near 800 nm for precision spectroscopy of an inner-shell transition in thulium atoms

Differential dynamic polarisability of the inner-shell clock transition at a wavelength of 1.14 μm in the thulium atom is measured by the method of precision laser spectroscopy in the spectral range of 800 – 860 nm. Experimental data approximated by a theoretical model yield the probability of the transition at λ = 809.5 nm: A{sub 809.5} = 460(70) s{sup −1}. The values of two magic wavelengths are obtained experimentally, namely, λ{sub m1} = 807.727(18) nm and λ{sub m2} = 813.3(2) nm, the wavelength of λ{sub m1} being determined for the first time. Main parameters of an optical lattice at these wavelengths are compared and a conclusion is made that trapping thulium atoms in an optical lattice at λ{sub m2} is preferable for optical clock operation. (laser frequency standards)

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2020

457-nm radiation source based on a diode laser for precision spectroscopy of magnesium atoms

We report on the development of a highly stable source of 457-nm radiation based on a diode laser and a tapered amplifier operating in a double-pass scheme. The diode laser frequency was stabilised by a high-Q reference Fabry – Perot interferometer and doubled in a PPSLT nonlinear crystal placed in an enhancement cavity. At a maximum output power of 200 mW at a wavelength of 457 nm, the laser linewidth was less than 5 kHz. The radiation source operation was demonstrated in experiments on precision spectroscopy of cold magnesium atoms in a magneto-optical trap. (lasers)

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2022

Precise stellarator quasi-symmetry can be achieved with electromagnetic coils

Magnetic fields with quasi-symmetry are known to provide good confinement of charged particles and plasmas, but the extent to which quasi-symmetry can be achieved in practice has remained an open question. Recent work [M. Landreman and E. Paul, Phys. Rev. Lett. 128, 035001, 2022] reports the discovery of toroidal magnetic fields that are quasi-symmetric to orders-of-magnitude higher precision than previously known fields. We show that these fields can be accurately produced using electromagnetic coils of only moderate engineering complexity, that is, coils that have low curvature and that are sufficiently separated from each other. Our results demonstrate that these new quasi-symmetric fields are relevant for applications requiring the confinement of energetic charged particles for long time scales, such as nuclear fusion. The coils’ length plays an important role for how well the quasi-symmetric fields can be approximated. For the longest coil set considered and a mean field strength of 1 T, the departure from quasi-symmetry is of the order of Earth’s magnetic field. Additionally, we find that magnetic surfaces extend far outside the plasma boundary used by Landreman and Paul, providing confinement far from the core. Simulations confirm that the magnetic fields generated by the new coils confine particles with high kinetic energy substantially longer than previously known coil configurations. In particular, when scaled to a reactor, the best found configuration loses only 0.04% of energetic particles born at midradius when following guiding center trajectories for 200 ms.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2020

An Improved Boosting to Amplify Signal with Isobaric Labeling (iBASIL) Strategy for Precise Quantitative Single-cell Proteomics

Mass spectrometry (MS)-based proteomics has great potential for overcoming the limitations of antibody-based immunoassays for antibody-independent, comprehensive, and quantitative proteomic analysis of single cells. Indeed, recent advances in nanoscale sample preparation have enabled effective processing of single cells. In particular, the concept of using boosting/carrier channels in isobaric labeling to increase the sensitivity in MS detection has also been increasingly used for quantitative proteomic analysis of small-sized samples including single cells. However, the full potential of such boosting/carrier approaches has not been significantly explored, nor has the resulting quantitation quality been carefully evaluated. Herein, we have further evaluated and optimized our recent boosting to amplify signal with isobaric labeling (BASIL) approach, originally developed for quantifying phosphorylation in small number of cells, for highly effective analysis of proteins in single cells. This improved BASIL (iBASIL) approach enables reliable quantitative single-cell proteomics analysis with greater proteome coverage by carefully controlling the boosting-to-sample ratio (e.g. in general <100×) and optimizing MS automatic gain control (AGC) and ion injection time settings in MS/MS analysis (e.g. 5E5 and 300 ms, respectively, which is significantly higher than that used in typical bulk analysis). By coupling with a nanodroplet-based single cell preparation (nanoPOTS) platform, iBASIL enabled identification of ~2500 proteins and precise quantification of ~1500 proteins in the analysis of 104 FACS-isolated single cells, with the resulting protein profiles robustly clustering the cells from three different acute myeloid leukemia cell lines. This study highlights the importance of carefully evaluating and optimizing the boosting ratios and MS data acquisition conditions for achieving robust, comprehensive proteomic analysis of single cells.

59 BASIC BIOLOGICAL SCIENCES↗
DOE OSTI2024

Precision Polishing of Ablator Capsules via in situ Process Monitoring and Machine Learning–Based Optimization

In inertial confinement fusion (ICF) experiments seeking output gains of unity and beyond, the quality of the ablator capsule is paramount for minimizing the hydrodynamic mix that quenches the central hot spot. Defects in the form of foreign particles or missing mass on the surface and within the wall of the capsule are primary offenders. High-density carbon capsules made for ICF experiments at the National Ignition Facility are precision polished to achieve surface smoothness on the order of a few nanometers as well as to minimize isolated defects in the form of pits. Given the critical role of this process, we are developing smart manufacturing techniques with the goal of elevating the efficiency of this process. Our approach is to use MEMS (micro-electromechanical systems)–based sensors to capture the fine vibration signals generated during the polishing process and combine them with synchronized visual feedback as needed. Beyond using these sensors for process monitoring, we use specific deep learning methods to analyze the data and extract correlations with both the process parameters and the final performance of the polishing run. Here, in this work, we describe the multiple fronts we have explored in this regard and the results we have gotten so far. This approach promises to have the potential to ultimately provide real-time feedback that can be used to ensure the progress of the run as well as a means for faster optimization.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2011

CLOSE TO THE DREDGE: PRECISE X-RAY C AND N ABUNDANCES IN {lambda} ANDROMEDA AND ITS PRECOCIOUS RED GIANT BRANCH MIXING PROBLEM

Chandra LETG+HRC-S and XMM-Newton RGS spectra of H-like C and N lines formed in the corona of the primary star of the RS CVn-type binary {lambda} And, a mildly metal-poor G8 III-IV first ascent giant that completed dredge-up {approx}50 Myr ago, have been used to make a precise measurement of its surface C/N ratio. We obtain the formal result [C/N] = 0.03 {+-} 0.07, which is typical of old disk giants and in agreement with standard dredge-up theory for stars {approx}< 1 M{sub sun}. In contrast, these stars as a group, including {lambda} And, have {sup 12}C/{sup 13}C {approx}< 20, which is much lower than standard model predictions. We show that the abundances of the old disk giants are consistent with models including thermohaline mixing that begins at the red giant branch luminosity function 'bump'. Instead, {lambda} And indicates that the {sup 12}C/{sup 13}C anomaly can be present immediately following dredge-up, contrary to current models of extra mixing on the red giant branch. In the context of other recent C and N abundance results for RS CVn-type binaries it seems likely that the anomaly is associated with either strong magnetic activity, fast rotation, or both, rather than close binarity itself.

79 ASTRONOMY AND ASTROPHYSICS↗