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At least 865 records · Page 48

Predicting melt pool depth and grain length using multiple signatures from in-situ single camera two-wavelength imaging pyrometry for laser powder bed fusion

In laser powder bed fusion (LPBF), the in-situ process signatures are known to have a direct correlation with the microstructural properties of the solidified melt pool (MP). It is known that the MP cooling and heating rates, and laser processing parameters can critically determine the grain structure and thereby affect the part properties. The objective of this work is to study the feasibility of using in-process, high-speed imaging pyrometry for evaluating the solidified MP properties “below” the surface, such as depth and microstructural properties. To accomplish this, we employ an in-house single camera-based two-wavelength imaging pyrometry (STWIP) system for monitoring the printing of single-scan tracks with Inconel 718 on a commercial LPBF printer (EOS M290). Further, the lab designed STWIP system is a coaxial high-speed (>10,000 fps) imaging system capable of monitoring MP temperature, morphology, and intensity profiles. The temperature measurements from STWIP are emissivity independent. The STWIP measured MP signatures of the printed tracks are correlated with the ex-situ microscopy characterized MP depth and the average grain lengths. From the data analysis, using support vector machine (SVM)-based regression models, we found that the MP temperature signatures are crucial for an accurate prediction of MP depth and the grain length, thus validating the novelty and necessity of the developed in-situ monitoring methods and analysis.

36 MATERIALS SCIENCE↗

Wisconsin In Situ Penning (WISP) gauge: A versatile neutral pressure gauge to measure partial pressures in strong magnetic fields

A new type of in-vessel Penning gauge, the Wisconsin In Situ Penning (WISP) gauge, has been developed and successfully operated in the Wendelstein 7-X (W7-X) island divertor baffle and vacuum vessel. The capacity of the quantitative measurements of the neutral reservoir for light impurities, in particular, helium, is important for tokamaks as well as stellarator divertors in order to avoid fuel dilution and radiative energy loss. Penning gauges assisted by spectroscopy are a powerful tool to obtain the total neutral pressure as well as fractional neutral pressures of specific impurities. The WISP gauge is a miniaturized Penning gauge arrangement, which exploits the ambient magnetic field of magnetic confinement fusion experiments to establish the Penning discharge. Then, in situ spectroscopy is conducted to separate the fractional neutral pressures of hydrogen, helium, and possibly also other impurities. The WISP probe head was qualified using the magnetic field of the Magnetized Dusty Plasma Experiment at Auburn University between 0.25 T and 3.5 T [E. Thomas et al ., J. Plasma Phys. 81, 345810206 (2015)]. The in-depth quantitative evaluation for hydrogen and helium will be shown as well as an exploration of nitrogen, argon, and neon. A power law scaling between current I and pressure p, I = f (Gas,V) p n⁽Gas, B⁾ , was shown. The factor f is gas and anode potential dependent, while n is gas and magnetic field strength dependent. Pressure measurements from 0.1 mbar and down to 1 × 10 -5 mbar were achieved, demonstrating a reliable operating range for relevant pressure levels in the divertor and main vessel regions in current and future fusion devices, with a time resolution of up to 1 kHz. The lowest achievable pressure measurement increases with an increase in B and can be shifted with the anode potential V . At W7-X, the WISP probe head was mounted on an immersion tube setup that passes through the cryostat and places the probe head close to the plasma. Two probe heads were positioned in different divertor pump gaps, top and bottom, and one close to the plasma on the midplane in one module. The gauges were in situ calibrated together with the ASDEX pressure gauges [G. Haas and H.-S. Bosch, Vacuum 51, 39 (1998)]. Data were taken during the entire operation phase 1.2b, and measurements were coherent with other neutral gas pressure gauges. For the spectroscopic partial pressure measurements, channels of a spectroscopic detection system based on photo-multipliers, a so-called filterscope [R. J. Colchin et al ., Rev. Sci. Instrum. 74, 2068 (2003)], provided by the Oak Ridge National Lab were used.

47 OTHER INSTRUMENTATION↗

A 15-Year Retrospective on Immersive Visualization Lessons from the Applied Visualization Laboratory

This article shares the experiences of operating an immersive visualization laboratory over a 15-year period. The paper discusses valuable insights into the lessons learned from various projects, including the challenges they faced, such as technical difficulties, user adoption, and opportunities, and practical solutions for overcoming them. One crucial element for successful immersive visualization projects is interdisciplinary collaboration. The paper presents the advantages of immersive visualization technology, such as improved data comprehension, enhanced communication, and increased engagement in complex scenarios. We present the dynamic realm of virtual and augmented truth (VR/AR) technology in the context of a immersive laboratory system. We spotlight rising trends inside the integration of VR/AR tools for visualization. We also present our experience in dealing with the hardware and software additives in an immersive VR/AR labs, dropping light on the demanding situations and successes encountered throughout everyday operations. Furthermore, it offers practical knowledge and guidance based on years of experience in the field, which can help you overcome challenges and achieve success in your project.

99 GENERAL AND MISCELLANEOUS↗

TRANSFER LEARNING FOR FIELD EMISSION MITIGATION IN CEBAF SRF CAVITIES

The Continuous Electron Beam Accelerator Facility (CEBAF) at Jefferson Lab operates hundreds of super-conducting radio frequency (SRF) cavities in its two linear accelerators (linacs). Field emission (FE) is an ongoing operational challenge in higher gradient SRF cavities. FE generates high levels of neutron and gamma radiation leading to damaged accelerator hardware and a radiation hazard environment. During machine development periods, we performed gradient scans to record data capturing the relationship between cavity gradients and radiation levels measured throughout the linacs. However, the field emission environment at CEBAF varies considerably over time as the configuration of the radio frequency (RF) gradients changes and due to the changing behaviour of field emitters. An artificial intelligence/machine learning (AI/ML) approach with transfer learning could be a valuable tool to mitigate FE and lower the radiation levels. In this work, we mainly focus on leveraging the RF trip data gathered during CEBAF operations. We develop a transfer learning-based surrogate model for radiation detector readings given RF cavity gradients to track the CEBAF?s changing configuration and environment. Then, we could use the developed model as an optimization process for redistributing the RF gradients within a linac to minimize radiation levels.

Ahammed, K.↗

Universal Solvent Viscosity Reduction via Hydrogen Bonding Disruptors

Liquid Ion Solutions LLC (DBA RoCo Global) in partnership with Carnegie Mellon University and Carbon Capture Scientific LLC, has performed lab-scale development and evaluation of novel additives that lower the viscosity of water-lean amine solvents for post-combustion carbon dioxide capture. This project focuses on developing additives that minimize the formation of long-range electrostatic and hydrogen bonding (HB) networks, decreasing the solvent viscosity, improving diffusion, and improving the process economics. The project objectives included: 1) performing computer simulation to understand the molecular interactions of the additive molecules in water-lean CO 2 capture solvents, 2) design and synthesis of HB disruptors additives, 3) performance testing with additive molecules on model amine solvents, and 4) demonstration of the effectiveness of the optimized additives in the presence of synthetic flue gas. To meet the abovementioned objectives, the project team utilized a holistic approach that combines molecular simulation, experimental testing, and economic analysis studies. The project team developed ab initio molecular model and then perform computer simulation to develop relationship between hydrogen bonding, viscosity, and performed quantitative analysis of additive on the viscosity of the solvent. The team completed computational comparative study on a range of organic functional groups such as ethers, esters, cyclic carbonates, alkanes, and ammonium salts for their effect on viscosity gaining key insights into molecular interactions and the impact of various functional groups and molecular shapes on viscosity. Assisted with molecular simulation insights, the project team conducted additive synthesis and testing, including a proof-of-concept study, additive screening, optimization, and synthetic flue gas testing. The experimental proof-of-concept study proved that the hydrogen bonding acceptors result in significant decrease of viscosities. Detailed additive screening (exploring various functionalities and molecular structures) has been performed. Several promising additives showed excellent reduction in viscosity (30-41%) at 5% additive loading, and over 50% viscosity reduction at 10% additive loading for the model solvents. The team also performed complex screening studies on additive loadings and mixing effect among additives using the design of experiments. Based on multiple screening experiments, one additive-solvent candidate was down-selected for synthetic flue gas testing. A 100-hour continuous absorption/desorption study was conducted under simulated flue gas using a lab-scale continuous capture and separation system. No degradation (for both solvent and additive) was observed based on the GC results of the solvent samples collected from the continuous study. The team conducted preliminary engineering analyses and cost-benefit analyses to quantify the potential economic benefits of the additive approach for solvent viscosity reduction. Based on the experimental data, CO 2 capture cost savings from the capital and operating cost savings are estimated at $\$$4.7/tonne and $\$$0.3/tonne CO 2 captured, respectively. Considering the additive cost, the net benefit is estimated to be between $\$$4.32~$\$$4.86/tonne CO 2 captured.

20 FOSSIL-FUELED POWER PLANTS↗

TRANSFER LEARNING FOR FIELD EMISSION MITIGATION IN CEBAF SRF CAVITIES

The Continuous Electron Beam Accelerator Facility (CEBAF) at Jefferson Lab operates hundreds of super-conducting radio frequency (SRF) cavities in its two linear accelerators (linacs). Field emission (FE) is an ongoing operational challenge in higher gradient SRF cavities. FE generates high levels of neutron and gamma radiation leading to damaged accelerator hardware and a radiation hazard environment. During machine development periods, we performed gradient scans to record data capturing the relationship between cavity gradients and radiation levels measured throughout the linacs. However, the field emission environment at CEBAF varies considerably over time as the configuration of the radio frequency (RF) gradients changes and due to the changing behaviour of field emitters. An artificial intelligence/machine learning (AI/ML) approach with transfer learning could be a valuable tool to mitigate FE and lower the radiation levels. In this work, we mainly focus on leveraging the RF trip data gathered during CEBAF operations. We develop a transfer learning-based surrogate model for radiation detector readings given RF cavity gradients to track the CEBAF?s changing configuration and environment. Then, we could use the developed model as an optimization process for redistributing the RF gradients within a linac to minimize radiation levels.

Ahammed, K.↗

DOE Advanced Gas Reactor Fuel Development and Qualification Program Overview

Slides discussing the DOE Advanced Gas Reactor Fuel Development and Qualification Program Overview to include focus on LEU UCO TRISO fuel in cylindrical compacts, with data for fuel qualification in support of reactor licensing and a path to establish a domestic commercial TRISO fuel fabrication capability. Timelines from 2004 through 2029. Major program highlights include: Developed fuel performance models based on past observed behavior, Study to understand differences between US and German (“good”) fuel, Developed and improved fuel fabrication and characterization methods, Fabricated lab-scale fuel (AGR-1) with very high quality; excellent in-pile and post-irradiation high-temperature fuel performance, Scale-up coating fabrication (AGR-2) with excellent in-pile performance, AGR-3/4 fuel fabrication and irradiation experiment to assess FP transport behavior, Scale-up matrix fabrication (AGR-5/6/7); & fuel performance evaluation in progress.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Denoising Seismograms in the Time Domain Using a Deep Learning Model

Deep learning has emerged as a transformative tool for enhancing the extraction of reliable information from seismograms, addressing the increasing demand for precise and efficient seismic data analysis. We introduce an innovative encoder–decoder deep learning model, named WaveDenoiser, designed for noise reduction in the time domain, thereby eliminating the need for spectrogram computations that have been used for existing deep learning tools and significantly improving processing speed. Utilizing the benchmark dataset that is Stanford Earthquake Dataset, we developed three models of varying sizes: base, medium, and large. Notably, the large (referred to as WaveDenoiser) model demonstrated superior performance, achieving a median signal‐to‐noise ratio improvement of 8.8 dB on in‐distribution unseen data (in the same geographic region) and 7.7 dB on out‐distribution unseen data (in a new geographic region), outpacing both the base and medium models. Further evaluation of the WaveDenoiser model revealed a reduction in median arrival‐time errors by 0.02 s for P waves and 0.01 s for S waves when processing waveforms prior to phase picking using PhaseNet on in‐distribution unseen data. When tested on out‐distribution unseen data, the model also effectively reduced the P‐wave median arrival‐time error by 0.02 and 0.01 s in median arrival‐time error for S waves. Importantly, the application of WaveDenoiser resulted in a significant reduction of phase picking outliers by 1.1% to 3.6% for both P and S waves. In addition, we achieved over five times acceleration in processing speed compared with the seisBench implementation of DeepDenoiser. Our findings underscore the potential of WaveDenoiser as a powerful tool for improving seismic data analysis and processing efficiency.

P-waves↗

Measurement of the beam-normal single-spin asymmetry for elastic electron scattering from 12 C and 27 Al

We report measurements of the parity-conserving beam-normal single-spin elastic scattering asymmetries B n on 12 C and 27 Al, obtained with an electron beam polarized transverse to its momentum direction. These measurements add an additional kinematic point to a series of previous measurements of B n on 12 C and provide a first measurement on 27 Al. The experiment utilized the Q weak apparatus at Jefferson Lab with a beam energy of 1.158 GeV. The average lab scattering angle for both targets was 7.7°, and the average Q 2 for both targets was 0.02437 GeV 2 (Q = 0.1561 GeV). The asymmetries are B n = -10.68 ± 0.90 (stat) ± 0.57 (syst) ppm 12 C and B n = -12.16 ± 0.58 (stat) ± 0.62 (syst) ppm for 27 Al. The results are consistent with theoretical predictions, and are compared to existing data. When scaled by Z/A, the Q dependence of all the far-forward angle (θ < 10°) data from 1 H to 27 Al can be described by the same slope out to Q ≈ 0.35 GeV. Larger-angle data from other experiments in the same Q range are consistent with a slope about twice as steep.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

Characterization of Uranium Foil Irradiations at the WSU TRIGA Reactor Using a New Reactor Model in Scale

A new reactor model of the Washington State University TRIGA was developed in the SCALE neutron transport code, and its fidelity was verified by comparison to MCNP and available data for several reactor parameters. The model was used to characterize irradiations designed to produce the short-lived actinides 237 U and 239 U, two key isotopes for nuclear forensics. These short-lived actinides, their decay daughters 237Np and 239Pu, and total fissions (via 99 Mo) were measured in irradiated foils at Los Alamos National Laboratory and other labs with good agreement among parent/daughter pairs and among labs. The laboratory-measured isotope ratios were used as a benchmark for the model determination of reaction rates. The flux distribution in the foils was also determined. Finally, using the continuous energy TSUNAMI-3D module of SCALE, a sensitivity/uncertainty analysis was performed to determine the effects on foil reactions caused by other system-wide reactions and by uncertainties in the known cross-sections.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

NNSA/CEA Workflow Workshop Report 2021

Researchers from three NNSA labs plus CEA recently met for a half-day workshop on scientific and engineering workflows in March of 2021. Tools, projects and use cases from each institution were described. A wide range of unique capabilities and requirements were represented. The workshop highlights the fact that the CEA/NNSA workflows space mirrors the broader open science workflows community, with multiple technologies under development in a number of science domains and under a number of funding streams, with differing capabilities and focuses. Despite the number of tools, presentations and discussions have shown that these tools cover specific mission spaces at the four labs, each with distinctive capabilities that do not completely overlap with each other. We believe there is a strong interest in the short term for sharing lessons learned and collaborating on benchmarks and site evaluation of projects. This report, prepared by the NNSA/CEA Workflows Working Group, briefly summarizes the presentations in the areas of domain specific workflows, end user environments, data management, job and resource management, and infrastructure, and then identifies six broad areas for potential collaboration. A key finding is that users could benefit from greater interoperability, compatibility, and composability of the workflow technologies under development and that point-to-point collaboration opportunities should be identified to explore these aspects.

97 MATHEMATICS AND COMPUTING↗

Nuclear Data for Spallation Neutron Radioisotope Production (Final Technical Report)

Over 50 million nuclear medicine procedures are performed annually, leading to a multi-billion dollar market for radioisotope production. The demand for new medical and research isotopes is growing, and radioisotope supply is insufficient. Most radioisotope production today utilizes charged particle or low-energy neutron irradiation of a target. Isotope production with tens to hundred MeV incident energies is a relatively unexplored option. There is a tremendous opportunity associated with a growing number of suitable domestic and international facilities buttressed by hundred million dollar global investments (e.g., the Los Alamos and Brookhaven Isotope Production Facilities, the European Spallation Source in Lund, and the Korean Multi-purpose Accelerator Complex in Gyeongbuk). In part due to a lack of supporting nuclear data that would make modeling radioisotope yields and purities possible, these facilities do not utilize their high-energy neutron fluxes for isotope production. This project attempted to measure neutron reaction excitation functions relevant to the large-scale production of critical radioisotopes, enabling development of cost-efficient isotope production methods, contributing to the improvement of theoretical models, and enhancing the value of national isotope production facilities. Reactions which form 67 Cu, 32 Si, and alpha-emitting isotopes like 225 Ac were chosen for their consistent prioritization by expert panels, representation of diverse reaction mechanisms, and relative lack of supporting nuclear data. Accurate measurement of these data is presently made only using quasi-monoenergetic neutron beams, which are produced by bombarding thin lithium targets with protons at only a few laboratories in the world. Ultimately, the projects efforts were incompletely accomplished due to a combination of multi-year technical issues at the only laboratory in the world which can make the proposed measurements, iThemba Labs in South Africa, and the onset of a global pandemic, which precluded the significant effort and time required to develop an independent measurement capability in the United States.

38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEA↗

The Jefferson Lab Eta Factory Experiment and Applications of PbWO4 Calorimeters in Future Experimental Facilities

The goal of the new JLab Eta Factory (JEF) experiment, conducted with the GlueX detector in Hall D at Jefferson Lab, is to perform measurements of various ¿(') decays with a primary focus on rare neutral modes. The experiment’s physics program ranges from precision tests of low-energy QCD to searches for gauge bosons with masses below 1 GeV that could couple the Standard Model (SM) sector to the dark sector. The experiment will collect a high-statistics data sample of ¿(') mesons produced via a beam of tagged photons. The GlueX detector features a large, nearly uniform acceptance for both neutral and charged particles, enabling efficient identification of complex multi-particle final states. To meet the requirements of the JEF experiment, the inner section of the forward lead-glass calorimeter in the GlueX detector has been upgraded with lead tungstate (PbWO4) scintillating crystals. PbWO4 offers exceptional characteristics, such as a small radiation length and Molire radius, and large light yield, that make it ideal for constructing high- granularity, high-resolution, radiation-hard detectors. These properties enable excellent spatial separation and energy resolution of reconstructed electromagnetic showers, establishing PbWO4 as the material of choice for many high-precision experiments. The JEF experiment began data collection in April 2025 and will operate concurrently with the GlueX experiment, whose primary objective is the search for gluonic excitations in the meson spectrum. I will give an overview of the JEF experiment, the GlueX detector, and the feasibility of further upgrades to support future ¿ physics studies. Special attention will be given to the newly constructed PbWO4 scintillating calorimeter and recent advancements in calorimeter instrumentation.

Somov, Alexander↗

Accessing glue through photoproduction measurements at GlueX

Photoproduction experiments are a key tool in the investigation of the spectrum of hadronic states and the way gluons contribute to this spectrum. The GlueX experiment, located at Jefferson Lab, features a linearly polarized tagged photon beam and its detector system is optimized to measure a wide range of neutral and charged final states. GlueX offers unique capabilities to study the spectrum of hadrons and is dedicated to the search for hybrid mesons, states with gluonic degrees of freedom. This talk presents first results from our initial campaign of data taking which finished in 2018.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

New Report Highlights LAMP's Role as a Robust and Reliable System for Wave Energy Converter Testing

Harnessing the power of waves requires more than just putting devices in the ocean - it takes tools that can refine and accelerate innovation before the first deployment. That's where NLR's largeamplitude motion platform, or LAMP, comes in. LAMP is a six-degree-of-freedom motion system designed to replicate the response of a wave energy converter (WEC) device in realistic ocean conditions. By letting researchers evaluate WEC performance in a safe, controlled lab environment before moving offshore, LAMP helps accelerate innovation while reducing risk. An NLR report, titled Initial Characterization of the NLR LargeAmplitude Motion Platform (https://www.nrel.gov/docs/fy26osti/93733.pdf), provides a deeper understanding of LAMP's capabilities and also lays the groundwork for future advancements in WEC testing methodologies. Researchers studied LAMP's amplitude and frequency limits across different payloads and collected data from 16 test profiles. Testing demonstrated that platform accuracy remained consistent across all payloads evaluated; researchers expect similar accuracy up to LAMP's 10,000-kilogram capacity limit. The measured position limits for single degrees of freedom experienced by WECs, including surge, sway, heave, roll, pitch, and yaw, also exceeded the original manufacturer specifications, providing new insight into the true boundaries of the system.

16 TIDAL AND WAVE POWER↗

Machine learning with knowledge constraints for process optimization of open-air perovskite solar cell manufacturing

Perovskite photovoltaics (PV) have achieved rapid development in the past decade in terms of power conversion efficiency of small-area lab-scale devices; however, successful commercialization still requires further development of low-cost, scalable, and high-throughput manufacturing techniques. One of the critical challenges of developing a new fabrication technique is the high-dimensional parameter space for optimization, but machine learning (ML) can readily be used to accelerate perovskite PV scaling. Herein, we present an ML-guided framework of sequential learning for manufacturing process optimization. We apply our methodology to the Rapid Spray Plasma Processing (RSPP) technique for perovskite thin films in ambient conditions. With a limited experimental budget of screening 100 process conditions, we demonstrated an efficiency improvement to 18.5% as the best-in-our-lab device fabricated by RSPP, and we also experimentally found 10 unique process conditions to produce the top-performing devices of more than 17% efficiency, which is 5 times higher rate of success than the control experiments with pseudo-random Latin hypercube sampling. Our model is enabled by three innovations: (a) flexible knowledge transfer between experimental processes by incorporating data from prior experimental data as a probabilistic constraint; (b) incorporation of both subjective human observations and ML insights when selecting next experiments; (c) adaptive strategy of locating the region of interest using Bayesian optimization first, and then conducting local exploration for high-efficiency devices. Furthermore, in virtual benchmarking, our framework achieves faster improvements with limited experimental budgets than traditional design-of-experiments methods (e.g., one-variable-at-a-time sampling). This framework shows the capability of incorporating researchers’ domain knowledge into the ML-guided optimization loop; therefore, it has the potential to facilitate the wider adoption of ML in scaling to perovskite PV manufacturing.

14 SOLAR ENERGY↗

Isotopically resolved neutron total cross sections at intermediate energies

The neutron total cross sections σ tot of 16,18 O, 58 64 Ni, 103 Rh, and 112,124 Sn have been measured at the Los Alamos Neutron Science Center from low to intermediate energies (3 ≤ E lab ≤ 450 MeV) by leveraging wave-form-digitizer technology. The σ tot relative differences between isotopes are presented, revealing additional information about the isovector components needed for an accurate optical-model description away from stability. Digitizer-enabled σ tot -measurement techniques are discussed and a series of uncertainty-quantified dispersive optical model (DOM) analyses using these new data is presented, validating the use of the DOM for modeling light systems ( 16,18 O) and systems with open neutron shells ( 58,64 Ni and 112,124 Sn). Here, the valence-nucleon spectroscopic factors extracted for each isotope reaffirm the usefulness of high-energy proton reaction cross sections for characterizing depletion from the mean-field expectation.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗