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At least 865 records · Page 48
All sourcesNASA NTRSDOE OSTI
DOE OSTI2022

Heat Loss Characteristics and Energy Use of Piperazine with the Advanced Stripper (PZAS) at the UT-SRP Pilot Plant

Heat duty and heat loss were measured at the pilot plant at UT Austin. Heat loss was measured with energy balances using water. Heat loss was studied using surface temperature measurements over 68 different locations at the pilot plant. Surface temperature measurements indicated that bare metal surfaces were the primary source of heat loss from the pilot plant. Heat loss from bare metal surfaces was at least 50% controlled by natural convection and in many cases was as high as 75% natural convection controlled. Measured heat loss at the pilot plant was 20100 BTU/hr and overall heat loss did not show any dependence on the heat rate of the plant. Compared to PZAS™ at the National Carbon Capture Center, heat loss relative to heat rate was higher at 38%. The relative heat loss at the pilot plants was found to decrease by 20% per MW of added capacity. Measured net heat duty was found to be dependent on measured lean loading and cold rich bypass flow rate. Measured net heat duty was between 2.2 and 2.4 GJ/tonne at an optimum lean loading of 0.2–0.21 mol/mol. Data reconciliation by Aspen Plus® Data Fit™ underpredicted CO2 flow rate by 20% due to an overprediction of lean loading by 19%, indicating a necessary change in thermodynamic parameters in the model. This resulted in an over prediction of heat duty by 33% on average.

Amine scrubbing, stripper, energy requirement, hea↗
NASA NTRS1984

Dilution Jets in Accelerated Cross Flows

Results of flow visualization experiments and measurements of the temperature field produced by a single jet and a row of dilution jets issued into a reverse flow combustor are presented. The flow in such combustors is typified by transverse and longitudinal acceleration during the passage through its bending section. The flow visualization experiments were designed to examine the separate effects of longitudinal and transverse acceleration on the jet trajectory and spreading rate. A model describing a dense single jet in a lighter accelerating cross flow is developed. The model is based on integral conservation equations, including the pressure terms appropriate to accelerating flows. It uses a modified entrainment correlation obtained from previous experiments of a jet in a cross stream. The flow visualization results are compared with the model calculations in terms of trajectories and spreading rates. Each experiment is typified by a set of three parameters: momentum ratio, density ratio, and the densimetric Froude number. When injection velocities are large or densities are small, the Froude number becomes very large and hence, unimportant. Therefore, the Froude number is generally significant in describing liquid experiments but is unimportant for the gas experiments in the combustor. Agreement between test and calculated results is encouraging but tends to become poorer with increasing momentum ratio. The temperature measurements are presented primarily in the form of consecutive normalized temperature profiles. Some interpolated isothermal contours are also shown. The single jet trajectories are consistently found to be swept towards the inner wall of the bend, whether injection is from the outer or the inner wall. This behavior is explained by a drifting effect which consists of a transverse velocity component across the combustor due to the developing nature of the flow along it. Plots of lateral temperature distributions of the jet indicate that under longitudinal acceleration conditions the thermal spreading of the jet may be completely suppressed. Comparison between combustor experimental results and model calculations shows poor agreement due to the drifting effect which is not taken into consideration in the model calculations. The row of jets experiments are characterized by two additional parameters: spacing ratio and confinement parameter. The results are shown in the form of consecutive normalized temperature profiles. The confinement parameter appears to become increasingly important with decreasing spacing ratio, in particular when its effect is enhanced by the drifting phenomenon and associated pressure field. A tightly spaced row of jets injected from the inner wall, prior to the bend, is surprisingly kept attached to the inner wall in spite of the strong turning. A similar attachment for a jet injected from the outer wall is not observed.

Lipshitz, Abraham↗
NASA NTRS1987

Fiber-Optic Temperature Sensor

Proposed sensor measures temperatures over wide range, from cryogenic liquids to burning gases. Made in part of optical fibers, sensor lighter in weight than thermocouple and immune to electromagnetic interference. Device does not respond to temperatures elsewhere than at sensing tip. Thermal expansion and contraction of distance between fiber end and mirror alters interference between light reflected from those two surfaces, thereby giving interferometric indication of temperatures.

Maram, Jonathan M.↗
DOE OSTI2024

Distributed Temperature Profiles of Silicon Carbide Catalyst Bed in a Microwave Reactor using Fiber-optic Sensor

Microwave heating is of great interest for reducing greenhouse gas emissions of catalytic chemical conversion processes because it can heat up the reactants rapidly and efficiently and accelerate reaction rates. In microwave-assisted catalytic thermochemical conversion processes, accurate internal temperature measurement would help facilitate effective process control. Metallic thermocouples interfere and spark in the microwave heating environment, so they are not an option. Infrared pyrometers typically provide a single temperature value by averaging over a finite surface area of the catalyst bed. In this work, we use fiber-optic sensors passing through the catalyst bed to provide more accurate temperatures along the height of the catalyst bed. The fiber optic sensors are immune to the electromagnetic microwave radiation and provide temperature profiles along their length. Here, custom fiber-optic sensors were coupled to the optical distributed temperature sensing devices to measure the temperature profiles along the height of the catalyst bed at high temperatures with ~1 mm spatial resolution. The sensing devices use optical frequency domain reflectometry (OFDR) technique for distributed temperature measurement. This work shows the temperature profiles along the height of the silicon carbide powder catalyst bed in the variable and fixed frequency microwave reactors.

Thapa, Juddha↗
NASA NTRS2001

Use of a Multiwavelength Pyrometer in Several Elevated Temperature Aerospace Applications

A multiwavelength pyrometer was developed for applications unique to aerospace environments. It was shown to be a useful and versatile technique for measuring temperature, even when the emissivity is unknown. It has also been used to measure the surface temperatures of ceramic zircomia thermal barrier coatings and alumina. The close agreement between pyrometer and thin film thermocouple temperatures provided an independent check. Other applications of the multiwavelength pyrometer are simultaneous surface and bulk temperature measurements of a transparent material, and combustion gas temperature measurement using a special probe interfaced to the multiwavelength pyrometer via an optical fiber. The multiwavelength pyrometer determined temperature by transforming the radiation spectrum in a broad wavelength region to produce a straight line (in a certain spectral region), whose intercept in the vertical axis gives the temperature. Implicit in a two-color pyrometer is the assumption of wavelength independent emissivity. Though the two data points of a two-color pyrometer similarly processed would result immediately in a similar straight line to give the unknown temperature, the two-color pyrometer lacks the greater data redundancy of the multiwavelength pyrometer, which enables it to do so with improved accuracy. It also confirms that emissivity is indeed wavelength independent, as evidenced by a multitude of the data lying on a simple straight line. The multiwavelength pyrometer was also used to study the optical transmission properties of a nanostructured material from which a quadratic exponential functional frequency dependence of its spectral transmission was determined. Finally, by operating the multiwavelength pyrometer in a very wide field of view mode, the surface temperature distribution of a large hot surface was obtained through measurement of just a single radiation spectrum.

Ng, Daniel↗
DOE OSTI2023

Brewster angle-cavity ringdown spectroscopy for low temperature plasma measurements in multiphases

Here we report on the development of a Brewster angle-cavity ringdown spectroscopy (BA-CRDS) system for low temperature plasma diagnostics. The system can measure gas species in solutions, with a detection limit (minimum detectable absorbance) of 9.1 × 10 -5 , which is equivalent to a detection limit of 0.04 parts per billion for measuring OH radicals in water at 308 nm. With higher reflectivity ringdown mirrors and improved design of a Brewster angle cell, the detection limit can potentially be up to 10 -6 or lower. In this exploratory study, the absorption cross sections of HgBr 2 and H 2 O 2 in the aqueous phase at 256 nm are measured to be (1.8 ± 0.1) × 10 -18 cm 2 and (5.2 ± 0.5) × 10 -20 cm 2 , respectively. Furthermore, temporal profiles of absorbance from distilled water, HgBr 2 , and H 2 O 2 solutions when interacting with a helium atmospheric plasma jet are individually characterized at different plasma powers, gas flow rates, and/or solute concentrations. The observed linear temporal profiles of absorbance from the plasma-interacted water suggest formation of H 2 O 2 from plasma-generated OH radicals, while the nonlinear temporal profiles from the plasma-treated HgBr 2 solutions reveal possible removal of HgBr 2 by OH radicals. Our results demonstrate that the new BA-CRDS system is a powerful tool for quantification of reactive plasma species in multiphases or other complex settings.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
NASA NTRS2013

Temperature and Species Measurements of Combustion Produced by a 9-Point Lean Direct Injector

This paper presents measurements of temperature and relative species concentrations in the combustion flowfield of a 9-point swirl venturi lean direct injector fueled with JP-8. The temperature and relative species concentrations of the flame produced by the injector were measured using spontaneous Raman scattering (SRS). Results of measurements taken at four flame conditions are presented. The species concentrations reported are measured relative to nitrogen and include oxygen, carbon dioxide, and water.

Tedder, Sarah A.↗
NASA NTRS2006

Multiple Waveband Temperature Sensor (MWTS)

This slide presentation reviews the development of Multiple Waveband Temperature Sensor (MWTS). The MWTS project will result in a highly stable, monolithically integrated, high resolution infrared detector array sensor that records registered thermal imagery in four infrared wavebands to infer dynamic temperature profiles on a laser-irradiated ground target. An accurate surface temperature measurement of a target in extreme environments in a non-intrusive manner is required. The development challenge is to: determine optimum wavebands (suitable for target temperatures, nature of the targets and environments) to measure accurate target surface temperature independent of the emissivity, integrate simultaneously readable multiband Quantum Well Infrared Photodetectors (QWIPs) in a single monolithic focal plane array (FPA) sensor and to integrate the hardware/software and system calibration for remote temperature measurements. The charge was therefore to develop and demonstrate a multiband infrared imaging camera with the detectors simultaneously sensitive to multiple distinct color bands for front surface temperature measurements Wavelength ( m) measurements. Amongst the requirements are: that the measurement system will not affect target dynamics or response to the laser irradiation and that the simplest criterion for spectral band selection is to choose those practically feasible spectral bands that create the most contrast between the objects or scenes of interest in the expected environmental conditions. There is in the presentation a review of the modeling and simulation of multi-wave infrared temperature measurement and also a review of the detector development and QWIP capacities.

infrared photodector↗
NASA NTRS1994

Thermal balance testing of MSAT 2 spacecraft

The present work reports on the recently completed infrared thermal balance/thermal vacuum testing of a MSAT satellite, the first satellite to provide mobile communications service for all of continental North America. MSAT is a two spacecraft program, using a three-axis stabilized Hughes HS-601 series Bus as the vehicle for the Canadian designed Payload. The thermal tests which were performed at the Canadian Space Agency's David Florida Laboratory in Ottawa, Canada, lasted approximately 35 days. The infrared (IR) heating rig was designed to provide radiant heat inputs into seven spacecraft zones during Thermal Vacuum (TV) testing. The TV test was divided into multiple phases. It began with a thermal balance cold phase, followed by a thermal cold cycle and a hot balance phase, complemented by a thermal hot cycle to finish with a thermal cycle with continuous monitoring of the Bus and Payload. The spacecraft's external heat fluxes were provided by IR lamp sources. To ensure flux uniformity, highly reflective baffles and IR East and West faces; the Earth facing (Nadir); and the inside of the thrust cylinder. The aft-end panel heat fluxes were provided by a heated LN2 shroud. The radiation flux intensity on the spacecraft zones from the various rig elements was measured using Monitored Background Radiometers (MBR's) and compared with direct calculations and with pretest predictions. The temperature measurement system was based on Uniform Temperature References (UTR's) located inside the chamber such that all feedthroughs were copper-copper. This system was devised to achieve a temperature measurement accuracy of plus/minus 0.5 C for over 850 thermocouples used in the test. A PC-(QNX-based) based real-time data acquisition system was utilized to provide continuous monitoring of all channels based on a 30-second time scan. In addition, the data acquisition system was able to retrieve telemetry stream from the Satellite Test Equipments (STE) station for real-time data manipulation. Preliminary results showed the test to be successful from both the thermal balance side and the electrical testing side.

Samson, Serge↗
NASA NTRS1995

Study of the rotational-level and temperature dependence of the quenching rate of OH fluorescence due to collisions with water molecules

The importance of the OH radical as an intermediate in many combustion reactions and in atmospheric photochemistry has led many researchers to use it as a diagnostic tool in these processes. The amount of data that has been acquired over the years for this radical is quite considerable. However, the quenching rate of OH with water molecules as a function of temperature and the rotational level of the excited state is not very well understood. The motivation of the studies undertaken is to bridge the gap between the low temperature measurements and the high temperature ones reported in the literature. The technique generally employed in these diagnostics is laser-induced fluorescence (LIF), through which rotational state selective excitation of the radical is possible. Furthermore, in a combustion medium, water is produced in abundance so that knowledge of the quenching rate of OH due to water molecules plays a crucial role in interpreting the data. In general, the precursor to an understanding of the collisional quenching rates of OH involves a characterization of the mode in which the radical is produced; the resulting rotational and translational distribution, followed by a measurement of the OH temperature; and ultimately obtaining the rate constants from the pressure dependence of the fluorescence signal. The experimental implementation of these measurements therefore involved, as a first step, the production of the OH radicals in a microwave discharge cell using water vapor as the source, wherein a hydrogen atom is abstracted from H2O. The second step involved the absorption of photons from the frequency-doubled output of a pulsed amplified, single-frequency cw ring dye laser. By tuning the laser to the peak of the transition and observing the fluorescence decay after the laser pulse, the lifetime of the OH in a particular rotational electronic state was determined (tau = 1.4 microseconds for Q(sub 1)(3)). Knowledge of this parameter led to a determination of the quenching rate. By varying the water vapor pressure in the cell and measuring the lifetime as a function of pressure a linear plot of the quenching rate as a function of pressure was obtained. Using this plot, the quenching cross section was deduced. It has therefore been possible to measure the local translational temperature and the quenching cross section with one laser system.

Koker, Edmond B.↗
DOE OSTI2021

Brine Availability Test in Salt (BATS) FY21 Update

This report summarizes the 2021 fiscal year (FY21) status of ongoing borehole heater tests in salt funded by the disposal research and development (R&D) program of the Office of Spent Fuel & Waste Science and Technology (SFWST) of the US Department of Energy’s Office of Nuclear Energy’s (DOE-NE) Office of Spent Fuel and Waste Disposition (SFWD). This report satisfies SFWST milestone M2SF- 21SN010303052 by summarizing test activities and data collected during FY21. The Brine Availability Test in Salt (BATS) is fielded in a pair of similar arrays of horizontal boreholes in an experimental area at the Waste Isolation Pilot Plant (WIPP). One array is heated, the other unheated. Each array consists of 14 boreholes, including a central borehole with gas circulation to measure water production, a cement seal exposure test, thermocouples to measure temperature, electrodes to infer resistivity, a packer-isolated borehole to add tracers, fiber optics to measure temperature and strain, and piezoelectric transducers to measure acoustic emissions. The key new data collected during FY21 include a series of gas tracer tests (BATS phase 1b), a pair of liquid tracer tests (BATS phase 1c), and data collected under ambient conditions (including a period with limited access due to the ongoing pandemic) since BATS phase 1a in 2020. A comparison of heated and unheated gas tracer test results clearly shows a decrease in permeability of the salt upon heating (i.e., thermal expansion closes fractures, which reduces permeability).

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗
NASA NTRS2003

High Temperature Thermographic Phosphor Coatings Development

For many years, phosphor thermometry has been used for non-contact temperature measurements. A large number of applications have been associated with high temperatures, especially for aerospace systems where blackbody radiation backgrounds are large and in challenging environments, such as vibration, rotation, flame, or noise. These environments restrict the use of more common thermocouples or infrared thermometric techniques. In particular, temperature measurements inside jet turbines, rocket engines, or similar devices are especially amenable to phosphor techniques. Often the fluorescent materials are used as powders, either suspended in binders and applied like paint or applied as high-temperature sprays. Thin coatings that are less than 50 m thick are used on the surfaces of interest. These coatings will quickly assume the same temperature as the surface to which they are applied. The temperature dependence of fluorescent materials is a function of the base matrix atoms and a small quantity of added activator or dopant ions. Often for high temperature applications, the selected materials are refractory and include rare earth ions. Phosphors like Y3Al5O12 (YAG) doped with Eu, Dy, or Tm, Y2O3 doped with Eu, or similar rare earth compounds, will survive high temperatures and can be configured to emit light that changes rapidly in lifetime and intensity. For example, researchers at Oak Ridge National Laboratory recently observed fluorescence from YAG:Dy and YAG:Tm at temperatures above 1400 C. One of the biggest challenges is to locate a binder material that can withstand tremendous variations in temperature in an adverse aerospace environment. This poster will provide an overview into our attempt to utilize phosphors for thermometry purposes. Emphasis will be placed on the use of selected binder materials that can withstand high temperatures. This research was completed for the National Aeronautics and Space Administration's Glenn Research Center in Cleveland, Ohio.

Goedeke, Shawn↗
NASA NTRS1982

Containerless high temperature property measurements by atomic fluorescence

Laser induced fluorescence techniques were developed for the containerless study of high temperature processes, material properties, levitation, and heating techniques for containerless earth-based experimentation. Experiments were performed in which fluorescence of atomic aluminum, mercury, or tungsten were studied. These experiments include measurements of: (1) Al atom evaporation from CW CO2 laser heated and aerodynamically levitated sapphire and alumina spheres, and self-supported sapphire filaments, (2) Al atom reaction with ambient oxygen in the wake of a levitated specimen, (3) Hg atom concentrations in the wake of levitated alumina and sapphire spheres, relative to the ambient Hg atom concentration, (4) Hg atom concentrations in supersonic levitation jets, and (5) metastable, electronically excited W atom concentrations produced by evaporation of an electrically heated tungsten filament.

Nordine, P. C.↗
DOE OSTI2021

A Low Cost SIPM Evaluation and Control Prototyping System including accurate bias voltage generation, leakage current measurement, and temperature control using Peltier cooling

We describe an electronics system to operate SIPMs in the laboratory. The system is comprised of a single channel amplifier board (SIPM Amp) and a 4-channel control board to which up to 4 SIPM Amp boards can be connected. The control board supplies a common low voltage power for the amplifiers. All channels feature individually regulated bias and Peltier power voltages, along withPt10K RTD readout. A graphical user interface allows control of the bias voltages, amplifier voltage, Peltier voltages, and also provides for readback of leakage currents and other voltages. The GUI app has a feedback loop to measure the SIPM temperature (with the PT10K) and generate correction voltages to the Peltier to regulate the temperature. The temperatures, which can be achieved by Peltier cooling depend on the thermal design of the setup, the practical limit being about 50C below ambient. The SIPM Amp. board is a small (3x5cm) PCB that has a single SIPM readout channel. The SIPM scan be surface mounted on the pcb or connected to a 2-pin 0.100" socket. The area around the SIPM footprint is thermally isolated by perforations in the PCB. The RTD is located inside the thermal break. Onboard is BV and LV filtering. The 10X amplifier is based on MiniCircuits' GALI-S66+ integrated circuit, tweaked for a 6V power. The amplifier was selected for a combination of high bandwidth, low noise, and low power. An accoupled amplifier output is connected to an SMA connector. For best operation of this inverting amplifier the output signal should be in the range of 0 to -1V.The Amplifier board is connected to the Control board with a 10-conductor 0.025" pitch ribbon cable, carrying all the services. Peltier power for currents more than 1A should use a separate 2-contact connector.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
NASA NTRS1967

An Evaluation of Sea Surface Temperature as Measured by the Nimbus 1 High Resolution Infrared Radiometer

An analysis of Nimbus I HRIR data over various parts of the world indicated limited success in deriving sea surface temperatures to within 3 to 6 K of aircraft radiation measurements (8- 13 microns) and synoptic-climatological ship sea surface temperature data. The areas studied included the east, west and Gulf coasts of the United States, West Greenland, Nova Scotia, southern Japan, the eastern Mediterranean Sea, Caspian Sea, Persian Gulf, and the Indian Ocean. At night, thin clouds which may fill the radiometer's field of view make it difficult to interpret the absolute values of derived sea surface temperature. During the daytime, the HRIR data is unusable for oceanographic temperature analysis because the contamination by reflected solar radiation mixes with the emitted radiation. Future satellite instrumentation, consisting of a HFUR radiometer (10-11 microns) when used in conjunction with television. data, will delineate cloud free ocean areas and permit the daily derivation of sea surface temperatures from approximately 10 to 30 Percent of the world's oceanic regions.

Allison, Lewis J.↗
NASA NTRS1992

Simultaneous temperature and multispecies measurement in a lifted hydrogen diffusion flame

UV spontaneous vibrational Raman scattering and laser-induced predissociative fluorescence (LIPF) techniques are combined and applied to a lifted hydrogen jet diffusion flame. Simultaneous, temporally and spatially resolved point measurements of temperature, major species concentrations (H2, O2, N2, H2O), and absolute hydroxyl radical concentration (OH) are obtained with a 'single' excimer laser for the first time. For OH measurements, the use of LIPF makes quenching corrections unnecessary. Results demonstrate that fuel and oxidizer are in a rich, premixed, and unignited condition in the center core of the lifted flame base. In the lifted zone, combustion occurs in an intermittent annular turbulent flame brush and strong finite-rate chemistry effects result in nonequilibrium values of temperature, major species, and OH radicals. Downstream in the slow three-body recombination zone, the major species concentrations are in partial equilibrium, the OH concentrations are in superequilibrium, and the temperatures are in subequilibrium. Far downstream in the flame, equilibrium values of temperature, OH radical, and major species are found.

Cheng, T. S.↗
DOE OSTI2023

Fiber Optic Temperature Sensor System Using Air-Filled Fabry–Pérot Cavity with Variable Pressure

We report a high-resolution fiber optic temperature sensor system based on an air-filled Fabry–Pérot (FP) cavity, whose spectral fringes shift due to a precise pressure variation in the cavity. The absolute temperature can be deduced from the spectral shift and the pressure variation. For fabrication, a fused-silica tube is spliced with a single-mode fiber at one end and a side-hole fiber at the other to form the FP cavity. The pressure in the cavity can be changed by passing air through the side-hole fiber, causing the spectral shift. We analyzed the effect of sensor wavelength resolution and pressure fluctuation on the temperature measurement resolution. A computer-controlled pressure system and sensor interrogation system were developed with miniaturized instruments for the system operation. Experimental results show that the sensor had a high wavelength resolution (<0.2 pm) with minimal pressure fluctuation (~0.015 kPa), resulting in high-resolution (±0.32 ℃) temperature measurement. It shows good stability from the thermal cycle testing with the maximum testing temperature reaching 800 ℃.

47 OTHER INSTRUMENTATION↗