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NASA NTRSDate not supplied

Fabrication and Characterization of A Lunar Simulant-Based Sintered Construction Material

In-situ resource utilization (ISRU) is critical to enable future efforts to have a long-term human presence on the Moon as well as Mars. ISRU technologies are being developed for radiation protection, dust mitigation, thermal insulation, and other applications. One such ISRU technology for creating construction materials out of lunar and Martian regolith is sintering, which is a thermal-based construction process that bonds finely grained material together at temperatures below the melting point. However, the conditions employed during the sintering, such as temperature, atmospheric composition, duration of the process, and pressure, can have a significant impact on the quality and strength of the resulting materials. In parallel, the development of methods for characterizing the quality, porosity, density, and other properties of these materials is critical. X-ray computed tomography (X-ray CT) can image large changes in density within a material, such as the presence of pores throughout an otherwise uniform medium, with relatively high spatial resolution. Similarly, Terahertz time-domain spectroscopic (THz-TDS) imaging is sensitive to density variations within samples, but is restricted to non-conducting materials. Specifically, previous work has shown that the refractive index (n eff ) values obtained through the analysis of THz-TDS images increases with increasing density within plastic samples. Even further, this work showed that it is possible to create a calibration curve for a given material from samples of different, but known density, which can enable one to directly convert n eff to density for samples having the same composition, but unknown density. Here, we report on the fabrication of a lunar simulant-based sintered construction material using vacuum hot pressed (VHP) sintering, then show X-ray CT and THz-TDS imaging results of the sample, which show spatial variations in the material. This has important implications for efforts to improve these types of lunar construction material processes and verify the quality of these materials in terms of consolidation. To the best of our knowledge, there is no previous work utilizing VHP sintering to make lunar simulant-based construction materials or exploring the feasibility of THz imaging to spatially map the density variation through a lunar simulant-based construction material.

Terahertz time-domain spectroscopic imaging↗
NASA NTRS1993

Thermally altered palagonitic tephra - A spectral and process analog to the soil and dust of Mars

Six palagonitic soil samples (PH-1 through PH-6) which were collected at 30-cm intervals from a lava slab on Mauna Kea, Hawaii, are studied. The samples present an alteration sequence caused by heating during emplacement of molten lava over a preexisting tephra cone. Techniques employed include visible and near-IUR spectroscopy, Moessbauer spectroscopy, and magnetic analysis. The four samples closest to the slab (PH-1 through PH-4) were strongly altered in response to heating during its emplacement; their iron oxide mineralogy is dominated by nanophase ferric oxide. The sample adjacent to the slab (PH-1) has a factor of 3 less H2O and contains crystalline hematite and magnetite in addition to nanophase ferric oxide. It is argued that localized thermal alteration events may provide a volumetrically important mechanism for the palagonitization of basaltic glass and the production of crystalline ferric oxides on Mars.

Bell, James F., III↗
NASA NTRS2004

Genesis failure investigation report : JPL Failure Review Board, Avionics Sub-Team

On January 7, 2001, the Genesis spacecraft lifted off from Cape Canaveral. Its mission was to collect solar wind samples and return those samples to Earth for detailed analysis by scientists. The mission proceeded successfully for three-and-a-half years. On September 8, 2004, the spacecraft approached Earth, pointed the Sample Return Capsule (SRC) at its entry target, and then fired pyros that jettisoned the SRC. The SRC carried the valuable samples collected over the prior 29 months. The SRC also contained the requisite hardware (mechanisms, parachutes, and electronics) to manage the process of entry, descent, and landing (EDL). After entering Earthas atmosphere, the SRC was expected to open a drogue parachute. This should have been followed by a pyro event to release the drogue chute, and then by a pyro event to deploy the main parachute at an approximate elevation of 6.7 kilometers. As the SRC descended to the Utah landing site, helicopters were in position to capture the SRC before the capsule touched down. On September 8, 2004, observers of the SRCas triumphant return became concerned as the NASA announcer fell silent, and then became even more alarmed as they watched the spacecraft tumble as it streaked across the sky. Long-distance cameras clearly showed that the drogue parachute had not deployed properly. On September 9, 2004, General Eugene Tattini, Deputy Director of the Jet Propulsion Laboratory formed a Failure Review Board (FRB). This board was charged with investigating the cause of the Genesis mishap in close concert with the NASA Mishap Investigation Board (MIB). The JPL-FRB was populated with experts from within and external to the Jet Propulsion Laboratory. The JPL-FRB participated with the NASA-MIB through all phases of the investigation, working jointly and concurrently as one team to discover the facts of the mishap.

solar wind↗
NASA NTRS1972

Testing relativistic gravity theories using radio tracking data from planetary orbiting spacecraft.

We present a thorough analysis of a computational method for determining the numerical values of the relativity and other related dynamical parameters using two-way Doppler and ranging data from planetary orbiting spacecraft. The computational method consists of two parts. From Doppler data we first determine the earth-planet components of the position of the orbiting spacecraft relative to the center of gravity of the planet to high accuracy; adding the observed spacecraft range yields a range value to the center of the planet. These constructed earth-planet range data, referred to as normal points, are then treated as raw data in a regression analysis combined with planetary radar delay and meridian circle measurements to solve for the significant solar system dynamical parameters. The major errors sources in the planetary orbiter process are enumerated and their individual effects on the overall accuracy of the normal point accuracies are presented. The accuracies of the parameter estimates as a function of time, data sampling, and a priori assumptions are illustrated.

Jordan, J. F.↗
NASA NTRS1980

Actinide crystal-liquid partitioning for clinopyroxene and Ca3/PO4/2

Coefficients for the partitioning of the actinide elements Th, U and Pu, which are used as indicators of r-process nucleosynthesis and the ages of meteorite and lunar samples, between diopsidic clinopyroxene, whitlockite and silicate liquid at 20 kbar are measured. Fission and alpha track radiography techniques are employed to detect element concentrations in synthetic crystals made using spiked starting materials, under the assumptions of equilibrium partitioning at the crystal-liquid interface and actinide zoning. Analysis of the data indicates results to be consistent with interface equilibrium except at high cooling rates. Th/U/Pu partition coefficients of about 0.002/0.002/O.06 are measured for clinopyroxene and 1.2/0.5/3.4 for whitlockite. The greater incorporation of Pu into the crystalline phases is attributed to the importance of trivalent Pu, and the similarity of its partition coefficient into clinopyroxene to that of the light rare earths supports the concept of Pu/rare earth dating.

Benjamin, T.↗
NASA NTRS2006

BOUSSOLE: A Joint CNRS-INSU, ESA, CNES, and NASA Ocean Color Calibration and Validation Activity

This report presents the Bouee pour l'acquisition de Series Optiques a Long Terme (BOUSSOLE) project, the primary objectives of which are to provide a long-term time series of optical properties in support of a) calibration and validation activities associated with satellite ocean color missions, and b) bio-optical research in oceanic waters. The following are included in the report: 1) an introduction to the rationale for establishing the project; 2) a definition of vicarious calibration and the specific requirements attached to it; 3) the organization of the project and the characteristics of the measurement site--in the northwestern Mediterranean Sea; 4) a qualitative overview of the collected data; 5) details about the buoy that was specifically designed and built for this project; 6) data collection protocols and data processing techniques; 7) a quantitative summary of the collected data, and a discussion of some sample results, including match-up analyses for the currently operational ocean color sensors, namely MERIS, SeaWiFS, and MODIS; and 8) preliminary results of the vicarious radiometric calibration of MERIS, including a tentative uncertainty budget. The results of this match-up analysis allow performance comparisons of various ocean color sensors to be performed, demonstrating the ability of the BOUSSOLE activity, i.e., combining a dedicated platform and commercial-off-the-shelf instrumentation, to provide data qualified to monitor the quality of ocean color products on the long term.

Antoine, David↗
NASA NTRS2008

Fluid control structures in microfluidic devices

Methods and apparatus for implementing microfluidic analysis devices are provided. A monolithic elastomer membrane associated with an integrated pneumatic manifold allows the placement and actuation of a variety of fluid control structures, such as structures for pumping, isolating, mixing, routing, merging, splitting, preparing, and storing volumes of fluid. The fluid control structures can be used to implement a variety of sample introduction, preparation, processing, and storage techniques.

Mathies, Richard A.↗
NASA NTRS2011

PMA-PhyloChip DNA Microarray to Elucidate Viable Microbial Community Structure

Since the Viking missions in the mid-1970s, traditional culture-based methods have been used for microbial enumeration by various NASA programs. Viable microbes are of particular concern for spacecraft cleanliness, for forward contamination of extraterrestrial bodies (proliferation of microbes), and for crew health/safety (viable pathogenic microbes). However, a "true" estimation of viable microbial population and differentiation from their dead cells using the most sensitive molecular methods is a challenge, because of the stability of DNA from dead cells. The goal of this research is to evaluate a rapid and sensitive microbial detection concept that will selectively estimate viable microbes. Nucleic acid amplification approaches such as the polymerase chain reaction (PCR) have shown promise for reducing time to detection for a wide range of applications. The proposed method is based on the use of a fluorescent DNA intercalating agent, propidium monoazide (PMA), which can only penetrate the membrane of dead cells. The PMA-quenched reaction mixtures can be screened, where only the DNA from live cells will be available for subsequent PCR reaction and microarray detection, and be identified as part of the viable microbial community. An additional advantage of the proposed rapid method is that it will detect viable microbes and differentiate from dead cells in only a few hours, as opposed to less comprehensive culture-based assays, which take days to complete. This novel combination approach is called the PMA-Microarray method. DNA intercalating agents such as PMA have previously been used to selectively distinguish between viable and dead bacterial cells. Once in the cell, the dye intercalates with the DNA and, upon photolysis under visible light, produces stable DNA adducts. DNA cross-linked in this way is unavailable for PCR. Environmental samples suspected of containing a mixture of live and dead microbial cells/spores will be treated with PMA, and then incubated in the dark. Thereafter, the sample is exposed to visible light for five minutes, so that the DNA from dead cells will be cross-linked. Following this PMA treatment step, the sample is concentrated by centrifugation and washed (to remove excessive PMA) before DNA is extracted. The 16S rRNA gene fragments will be amplified by PCR to screen the total microbial community using PhyloChip DNA microarray analysis. This approach will detect only the viable microbial community since the PMA intercalated DNA from dead cells would be unavailable for PCR amplification. The total detection time including PCR reaction for low biomass samples will be a few hours. Numerous markets may use this technology. The food industry uses spore detection to validate new alternative food processing technologies, sterility, and quality. Pharmaceutical and medical equipment companies also detect spores as a marker for sterility. This system can be used for validating sterilization processes, water treatment systems, and in various public health and homeland security applications.

Venkateswaran, Kasthuri J.↗
NASA NTRS2013

Mars Atmospheric Escape Recorded by H, C and O Isotope Ratios in Carbon Dioxide and Water Measured by the Sam Tunable Laser Spectrometer on the Curiosity Rover

Stable isotope ratios in C, H, N, O and S are powerful indicators of a wide variety of planetary geophysical processes that can identify origin, transport, temperature history, radiation exposure, atmospheric escape, environmental habitability and biological activity [2]. For Mars, measurements to date have indicated enrichment in all the heavier isotopes consistent with atmospheric escape processes, but with uncertainty too high to tie the results with the more precise isotopic ratios achieved from SNC meteoritic analyses. We will present results to date of H, C and O isotope ratios in CO2 and H2O made to high precision (few per mil) using the Tunable Laser Spectrometer (TLS) that is part of the Sample Analysis at Mars (SAM) instrument suite on MSL s Curiosity Rover.

Webster, C. R.↗
NASA NTRS2019

Refining Lucy Mission Delta-V During Spacecraft Design Using Trajectory Optimization Within High-Fidelity Monte Carlo Maneuver Analysis

Recent advances linking medium-fidelity trajectory optimization and high-fidelity trajectory propagation/maneuver design software with Monte Carlo maneuver analysis and parallel processing enabled realistic statistical delta-V estimation well before launch. Completing this high-confidence, refined statistical maneuver analysis early enabled release of excess delta-V margin for increased dry mass margin for the Lucy Jupiter Trojan flyby mission. By 3.3 years before launch, 16 of 34 TCMs had 1000 re-optimized trajectory design samples, yielding tens of m/s lower 99%-probability delta-V versus targeting maneuvers to one optimal trajectory. One year later, 1000 re-optimized samples of all deterministic maneuvers and subsequent flybys further lowered estimated delta-V.

Trojan↗
NASA NTRS2001

Modulation of lens cell adhesion molecules by particle beams

Cell adhesion molecules (CAMs) are proteins which anchor cells to each other and to the extracellular matrix (ECM), but whose functions also include signal transduction, differentiation, and apoptosis. We are testing a hypothesis that particle radiations modulate CAM expression and this contributes to radiation-induced lens opacification. We observed dose-dependent changes in the expression of beta 1-integrin and ICAM-1 in exponentially-growing and confluent cells of a differentiating human lens epithelial cell model after exposure to particle beams. Human lens epithelial (HLE) cells, less than 10 passages after their initial culture from fetal tissue, were grown on bovine corneal endothelial cell-derived ECM in medium containing 15% fetal bovine serum and supplemented with 5 ng/ml basic fibroblast growth factor (FGF-2). Multiple cell populations at three different stages of differentiation were prepared for experiment: cells in exponential growth, and cells at 5 and 10 days post-confluence. The differentiation status of cells was characterized morphologically by digital image analysis, and biochemically by Western blotting using lens epithelial and fiber cell-specific markers. Cultures were irradiated with single doses (4, 8 or 12 Gy) of 55 MeV protons and, along with unirradiated control samples, were fixed using -20 degrees C methanol at 6 hours after exposure. Replicate experiments and similar experiments with helium ions are in progress. The intracellular localization of beta 1-integrin and ICAM-1 was detected by immunofluorescence using monoclonal antibodies specific for each CAM. Cells known to express each CAM were also processed as positive controls. Both exponentially-growing and confluent, differentiating cells demonstrated a dramatic proton-dose-dependent modulation (upregulation for exponential cells, downregulation for confluent cells) and a change in the intracellular distribution of the beta 1-integrin, compared to unirradiated controls. In contrast, there was a dose-dependent increase in ICAM-1 immunofluorescence in confluent, but not exponentially-growing cells. These results suggest that proton irradiation downregulates beta 1-integrin and upregulates ICAM-1, potentially contributing to cell death or to aberrant differentiation via modulation of anchorage and/or signal transduction functions. Quantification of the expression levels of the CAMs by Western analysis is in progress.

NASA Discipline Radiation Health↗
NASA NTRS2014

Exact and Approximate Probabilistic Symbolic Execution

Probabilistic software analysis seeks to quantify the likelihood of reaching a target event under uncertain environments. Recent approaches compute probabilities of execution paths using symbolic execution, but do not support nondeterminism. Nondeterminism arises naturally when no suitable probabilistic model can capture a program behavior, e.g., for multithreading or distributed systems. In this work, we propose a technique, based on symbolic execution, to synthesize schedulers that resolve nondeterminism to maximize the probability of reaching a target event. To scale to large systems, we also introduce approximate algorithms to search for good schedulers, speeding up established random sampling and reinforcement learning results through the quantification of path probabilities based on symbolic execution. We implemented the techniques in Symbolic PathFinder and evaluated them on nondeterministic Java programs. We show that our algorithms significantly improve upon a state-of- the-art statistical model checking algorithm, originally developed for Markov Decision Processes.

Symbolic Execution↗
NASA NTRS1970

Results of scatterometer systems analysis for NASA/MSC Earth observation sensor evaluation program

A systems evaluation of the 13.3 GHz scatterometer system is presented. The effects of phase error between the scatterometer channels, antenna pattern deviations, aircraft attitude deviations, environmental changes, and other related factors such as processing errors, system repeatability, and propeller modulation, are established. Furthermore, the reduction in system errors and calibration improvement is investigated by taking into account these parameter deviations. Typical scatterometer data samples are presented.

Krishen, K.↗
NASA NTRS2020

Aqueous Processes and Microbial Habitability of Gale Crater Sediments from the Blunts Point to the Glenn Torridon Clay Unit

A driving factor for sending the Mars Science Laboratory, Curiosity rover to Gale Crater was the orbital detection of clay minerals in the Glen Torridon (GT) clay unit. Clay mineral detections in GT suggested a past aqueous environment that was habitable, and could contain organic evidence of past microbiology. The mission of the Sample Analysis at Mars (SAM) instrument onboard Curiosity was to detect organic evidence of past microbiology and to detect volatile bearing mineralogy that can inform on whether past geochemical conditions would have supported microbiological activity. The objective of this work was to 1) evaluate the depositional/alteration conditions of Blunt’s Point (BP) to GT sediments 2) search for evidence of organics, and 3) evaluate microbial habitability in the BP, Vera Rubin Ridge (VRR), and GT sedimentary rock.

Sutter, Brad↗
NASA NTRS1981

Raingage network sampling statistics

Sampling problems raise large difficulties for the precipitation measurements from space. In the tropics rainfall processes are organized in scales which are hardly resolved by the microwave radiometers on board of satellites. Even in the cloud clusters, which mark significant, large extended signals in the visible and infrared images, the precipitation areas cover only a small region. Our analysis of the cloud clusters over the W Pacific Ocean revealed that more than 50% of the area of a typical Western Pacific cluster are without rain. The radar observations during GATE generally confirmed those results. The rainfall was calculated from Nimbus V microwave data at 19.35 GHz and the results were compared with the GATE radar rainfall. The results are improved if the rain areas within the field of view are determined by additional observations and lead to a correction of the microwave brightness temperature.

Vogel, J. L.↗
NASA NTRS1987

Chemical interactions in Low Earth Orbit (LEO)

Although several observations of material changes on-orbit have been reported, mechanistic understanding has not yet become clear because new sets of non-intuitive processes are occurring on orbit. Reactant kinetic energy, low collision rates and surface/adsorbate interactions must be considered in the analysis of these observations. The specific example of oxide formation of elemental materials is examined in terms of thermodynamics and possible reaction pathways. On the basis of this approach, a rational trend emerges from the orbital behavior of these samples. The role of reactant kinetic energy as opposed to internal energy in chemiluminescent product formation is also presented. Development of a systematic thermochemical approach may be useful in making screening predictions of long-term material behavior on-orbit.

Green, B. D.↗
NASA NTRS1989

Consort 1 flight results - A synopsis

All six experiments performed onboard Consort 1, the first low gravity materials processing payload to be launched by a commercially licensed rocket in the U.S., are evaluated. The six experiments were carried out as planned, during approximately seven minutes of suborbital, low gravity flight and returned in excellent condition within four hour of launch. Nearly 150 physical samples supported by measurements and photographs made during the flight were taken for analysis. The rocket flight and payload configuration is described, along with experiment objectives, methods, results, and conclusions.

Wessling, Francis C.↗
NASA NTRS1990

A superelement methodology for coupled loads analysis of Space Station Freedom

A technique for calculating the effects of on-orbit loads on the structural dynamics of the International Space Station is developed on the basis of MSC/NASTRAN superelement solution sequences. The complexity of the Space Station program with its multiple configurations, international partners, and contractors is stressed, and the impact of this complexity on the dynamic-load analysis process is indicated. The MSC/NASTRAN-based approach is outlined, and its application to two versions of the Permanent Manned Capability configuration is described in detail, including component mode synthesis, GFSC/FLAME coupled-loads analysis (with components from the system FEM model or from the Work Package), and ISI/MATRIX-X generation of closed-loop forcing functions. The results of these sample analyses are presented in extensive tables and graphs and briefly characterized.

Del Basso, Steve↗