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At least 865 records · Page 48

Simulated space environmental effects on some experimental high performance polymers

Organic polymeric materials are currently being considered for long term use (more than 10 years) in structural (adhesives and composite matrices) and functional (films and coatings) applications on spacecraft. Although organic polymers have been utilized successfully in short term missions, the long term durability of these materials in space is of concern. As part of a NASA effort on high performance polymers for potential space applications, various experimental polymeric materials recently synthesized at NASA Langley Research Center were evaluated under simulated space environmental conditions. Experimental resins from blends of acetylene terminated materials, poly(arylene ether)s and low color polyimides were exposed to high energy electron and ultraviolet radiation in an attempt to simulate space environmental effects. Thin films, neat resin moldings and carbon fiber reinforced composites were exposed and the effect on certain polymer properties were determined. This paper reviews recent research involving the effects of various radiation exposures on the physical, optical and mechanical properties of several experimental polymer systems.

Connell, John W.↗

Effect of Heat Treatment on the Microstructure and Mechanical Properties of Monel K500 Alloy Fabricated Via L-PBF and LP-DED

This study examines and compares the effect of different heat treatments (HT) on the microstructure and mechanical properties of Monel K500 fabricated using laser powder bed fusion (L-PBF) and laser powder directed energy deposition (LP-DED) technologies. The as-fabricated Monel K500 specimens exhibited dendritic microstructure and elemental micro-segregation due to high cooling rates induced during the fabrication process. The applicability of HT proposed in the literature for wrought Monel K500 was investigated for L-PBF and LP-DED using four different HT procedures involving hot isostatic pressing (HIP), solution annealing (SA), and aging. The mechanical properties of test specimens were evaluated using uniaxial tensile testing at room temperature. The microstructural evolution of test specimens during HT was analyzed using a scanning electron microscope. For all HT conditions investigated, L-PBF Monel K500 specimens consistently displayed higher strength and lower ductility compared to the LP-DED counterparts. The HT procedure involving HIP at 1160°C for 3hr at 100 MPa, SA at 1100°C for 15 min, and three step aging at 610°C for 16 hr, 540°C for 6 hr, and 480°C for 8 hr resulted in highest strength for both L-PBF and LP-DED fabricated Monel K500.

Additive manufacturing↗

High Speed Thermal Imaging on Ballistic Impact of Triaxially Braided Composites

Ballistic impact experiments were performed on triaxially braided polymer matrix composites to study the heat generated in the material due to projectile velocity and penetration damage. Quantifying the heat generation phenomenon is crucial for attaining a better understanding of composite behavior and failure under impact loading. The knowledge gained can also be used to improve physics-based models which can numerically simulate impact of composites. Triaxially braided (0/+60/-60) composite panels were manufactured with T700S standard modulus carbon fiber and two epoxy resins. The PR520 (toughened) and 3502 (untoughened) resin systems were used to make different panels to study the effects of resin properties on temperature rise. Ballistic impact tests were conducted on these composite panels using a gas gun, and different projectile velocities were applied to study the effect on the temperature results. Temperature contours were obtained from the rear surface of the panel during the test through a high speed, infrared (IR) thermal imaging system. The contours show that high temperatures were locally generated and more pronounced along the axial tows for the T700S/PR520 composite specimens; whereas, tests performed on T700S/3502 composite panels using similar impact velocities demonstrated a widespread area of lower temperature rises. Nondestructive, ultrasonic C-scan analyses were performed to observe and verify the failure patterns in the impacted panels. Overall, the impact experimentation showed temperatures exceeding 525 K (485degF) in both composites which is well above the respective glass transition temperatures for the polymer constituents. This expresses the need for further high strain rate testing and measurement of the temperature and deformation fields to fully understand the complex behavior and failure of the material in order to improve the confidence in designing aerospace components with these materials.

thermal imaging↗

Study of advanced fuel system concepts for commercial aircraft and engines

The impact on a commercial transport aircraft of using fuels which have relaxed property limits relative to current commercial jet fuel was assessed. The methodology of the study is outlined, fuel properties are discussed, and the effect of the relaxation of fuel properties analyzed. Advanced fuel system component designs that permit the satisfactory use of fuel with the candidate relaxed properties in the subject aircraft are described. The two fuel properties considered in detail are freezing point and thermal stability. Three candidate fuel system concepts were selected and evaluated in terms of performance, cost, weight, safety, and maintainability. A fuel system that incorporates insulation and electrical heating elements on fuel tank lower surfaces was found to be most cost effective for the long term.

Versaw, E. F.↗

Effect of heat treatment on the flexural properties of a titanium matrix composite

Titanium matrix composites (TMC) reinforced with carbon fibers are widely used in the aerospace industry due to their light weight, high strength and modulus and the retention of their strength and modulus at elevated temperatures. Liquid infiltration, a low cost technique for making TMCs, has been little used due to the extent of the reaction between titanium and carbon during fabrication. Rapid infrared processing (RIP) has been developed as a technique for reducing interfacial reaction during composite fabrication. The strength and modulus of composites produced using RIP were higher than or comparable to those for other composites. This paper examines the effect of heat treatment on the room temperature flexural strength and modulus of TMC produced using RIP. The experiments carried out are described and results are presented. Results showed increased flexural strength of the composites upon aging at temperatures of 800 and 900 degrees C. This increased strength may be due to increased strength of the matrix.

Warrier, S. G.↗

Nonlinear analysis of laminated fibrous composites

A computerized analysis of the nonlinear behavior of fibrous composite laminates including axial loading, thermal loading, temperature dependent properties, and edge effects is presented. Ramberg-Osgood approximations are used to represent lamina stress-strain behavior and percent retention curves are employed to model the variation of properties with temperature. Balanced, symmetric laminates comprised of either boron/epoxy, graphite/epoxy, or borsic-aluminum are analyzed using a quasi-three-dimensional finite element analysis. Results are presented for the interlaminar stress distributions in cross-ply, angle-ply, and more complex laminates. Nonlinear stress-strain curves for a variety of composite laminates in tension and compression are obtained and compared to other existing theories and experimental results.

Renieri, G. D.↗

Micrometeoroid/space debris effects on materials

The Long Duration Exposure Facility (LDEF) micrometeoroid/space debris impact data has been reduced in terms that are convenient for evaluating the overall quantitative effect on material properties. Impact crater flux has been evaluated as a function of angle from velocity vector and as a function of crater size. This data is combined with spall data from flight and ground testing to calculate effective solar absorption and emittance values versus time. Results indicate that the surface damage from micrometeoroid/space debris does not significantly affect the overall surface optical thermal physical properties. Of course the local damage around impact craters radically alter optical properties. Damage to composites and solar cells on an overall basis was minimal.

Zwiener, James M.↗

Low-energy electron effects on tensile modulus and infrared transmission properties of a polypyromellitimide film

Infrared (IR) spectroscopy and tensile modulus testing were used to evaluate the importance of experimental procedure on changes in properties of pyromellitic dianhydride-p,p prime-oxydianiline film exposed to electron radiation. The radiation exposures were accelerated, approximate equivalents to the total dose expected for a 30 year mission in geosynchronous Earth orbit. The change in the tensile modulus depends more on the dose rate and the time interval between exposure and testing than on total dose. The IR data vary with both total dose and dose rate. A threshold dose rate exists below which reversible radiation effects on the IR spectra occur. Above the threshold dose rate, irreversible effects occur with the appearance of a new band. Post-irradiation and in situ IR absorption bands are significantly different. It is suggested that the electron radiation induced metastable, excites molecular states.

Ferl, J. E.↗

The effects of high-temperature brazing and thermal cycling on the mechanical properties of Hastelloy X

Data are presented on the effects of brazing alloy, brazing operation, thermal cycling, and combinations of these on the yield strength, elongation, tensile strength, and fatigue life of thin gage Hastelloy X. These data show that brazing at 1461 K (2170 F) with a Ni-Pd-Au alloy and subsequent exposure to 200 service thermal cycles between 533 and 1144 K (500 and 1600 F) result in reduction of as much as 39 percent in yield strength, 33 percent in elongation, 14 percent in tensile strength, and 26 percent in fatigue limit of Hastelloy X, as compared to as-received materials. These property losses are primarily caused by the brazing operation rather than the subsequent service thermal cycles.

Dicus, D. L.↗

The effects of small ice crystals on the infrared radiative properties of cirrus clouds

To be successful in the development of satellite retrieval methodologies for the determination of cirrus cloud properties, we must have fundamental scattering and absorption data on nonspherical ice crystals that are found in cirrus clouds. Recent aircraft observations (Platt et al. 1989) reveal that there is a large amount of small ice particles, on the order of 10 micron, in cirrus clouds. Thus it is important to explore the potential differences in the scattering and absorption properties of ice crystals with respect to their sizes and shapes. In this study the effects of nonspherical small ice crystals on the infrared radiative properties of cirrus clouds are investigated using light scattering properties of spheroidal particles. In Section 2, using the anomalous diffraction theory for spheres and results from the exact spheroid scattering program, efficient parameterization equations are developed for calculations of the scattering and absorption properties for small ice crystals. Parameterization formulas are also developed for large ice crystals using results computed from the geometric ray-tracing technique and the Fraunhofer diffraction theory for spheroids and hexagonal crystals. This is presented in Section 3. Finally, applications to the satellite remote sensing are described in Section 4.

Takano, Y.↗

A New Approach to Identify Optimal Properties of Shunting Elements for Maximum Damping of Structural Vibration Using Piezoelectric Patches

The use of shunted piezoelectric patches in reducing vibration and sound radiation of structures has several advantages over passive viscoelastic elements, e.g., lower weight with increased controllability. The performance of the piezoelectric patches depends on the shunting electronics that are designed to dissipate vibration energy through a resistive element. In past efforts most of the proposed tuning methods were based on modal properties of the structure. In these cases, the tuning applies only to one mode of interest and maximum tuning is limited to invariant points when based on den Hartog's invariant points concept. In this study, a design method based on the wave propagation approach is proposed. Optimal tuning is investigated depending on the dynamic and geometric properties that include effects from boundary conditions and position of the shunted piezoelectric patch relative to the structure. Active filters are proposed as shunting electronics to implement the tuning criteria. The developed tuning methods resulted in superior capabilities in minimizing structural vibration and noise radiation compared to other tuning methods. The tuned circuits are relatively insensitive to changes in modal properties and boundary conditions, and can applied to frequency ranges in which multiple modes have effects.

Park, Junhong↗

A designed experiment in stitched/RTM composites

The damage tolerance of composite laminates can be significantly improved by the addition of through-the-thickness fibrous reinforcement such as stitching. However, there are numerous stitching parameters which can be independently varied, and their separate and combined effects on mechanical properties need to be determined. A statistically designed experiment (a 2(sup 5-1) fractional factorial, also known as a Taguchi L16 test matrix) used to evaluate five important parameters is described. The effects and interactions of stitch thread material, stitch thread strength, stitch row spacing and stitch pitch are examined for both thick (48 ply) and thin (16 ply) carbon/epoxy (AS4/E905L) composites. Tension, compression and compression after impact tests are described. Preliminary results of completed tension testing are discussed. Larger threads decreased tensile strength. Panel thickness was found not to be an important stitching parameter for tensile properties. Tensile modulus was unaffected by stitching.

Dickinson, Larry C.↗

The effects of scattering geometry on the spectrophotometric properties of powdered material

The characteristics of reflectance spectra are being used as a basis in investigations to infer the composition of planetary surfaces. However, the reflectance spectra of powdered materials depend not only on the composition of these materials, but also on other variables. A description is presented of the results of an exploratory series of measurements designed to investigate the importance of scattering geometry as a variable in determining the shapes of spectral reflectance curves, taking into account half a dozen materials of planetary interest. It is noted that the considered results are consistent with those reported by Adams and Felice (1967), especially the results on the variation with phase angle of the Red/Blue color ratio for various silicate materials. The measurements demonstrate in detail that scattering geometry does affect the shapes of spectral reflectance curve. In some cases this effect is quite significant.

Gradie, J.↗

Effects of through-the-thickness stitching on impact and interlaminar fracture properties of textile graphite/epoxy laminates

This study investigated the effects of through-the-thickness stitching on impact damage resistance, impact damage tolerance, and mode I and mode II fracture toughness of textile graphite/epoxy laminates. Uniweave resin-transfer-molded 48 ply graphite/epoxy (AS4/3501-6) laminates were stitched with Kevlar and glass yarns of different linear densities and stitch spacings. Delaminations were implanted during processing to simulate impact damage. Sublaminate buckling tests were performed to determine the effects of stitching on the compressive strength. The results showed outstanding improvements of up to 400 percent in the compression strength over the unstitched laminates. In impact and static indentation tests the onset of damage occurred at the same level, but the extent of damage was less in stitched laminates. Mode I fracture toughness of 24 ply Uniweave unidirectional (AS4/3501-6) stitched laminates was measured by conducting double-cantilever-beam tests. The critical strain energy release rate (G(sub Ic)) was found to be up to 30 times higher than the unstitched laminates. Mode II fracture toughness of the Uniweave laminates was measured by performing end-notched-flexure tests. Two new methods to compute the apparent G(sub IIc) are presented. The apparent G(sub IIc) was found to be at least 5-15 times higher for the stitched laminates.

Sharma, Suresh K.↗

Polyvinyl alcohol membranes as alkaline battery separators

Polyvinly alcohol (PVA) cross-linked with aldehyde reagents yields membranes that demonstrate properties that make them suitable for use as alkaline battery separators. Film properties can be controlled by the choice of cross-linker, cross-link density and the method of cross-linking. Three methods of cross-linking and their effects on film properties are discussed. Film properties can also be modified by using a copolymer of vinyl alcohol and acrylic acid as the base for the separator and cross-linking it similarly to the PVA. Fillers can be incorporated into the films to further modify film properties. Results of separator screening tests and cell tests for several variations of PBA films are discussed.

Sheibley, D. W.↗

Superelement methods in high temperature metal matrix composites

A study into fiber fracture and debonding in metal matrix composites is conducted using the finite element method. The superelement finite element technique was used to model a metal matrix composite under various loading condition and with varying degrees of fiber debonding. The use of superelement saved many man hours by allowing for alteration of only the primary superelement to manipulate partial bonding for the entire model. The composite's material properties were calculated and the effects of fiber debonding on these properties were noted. The internal stress state of the composite while under various loads was also studied. Special interest was devoted to the change in stress state as a result of increasing fiber debonding.

Trowbridge, Daniel↗