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NASA NTRS2022

Ultraviolet Photooxidation of Smectite-Bound Fe(II) and Implications for the Origin of Martian Nontronites

Clay minerals detected with orbital and in situ instruments in ancient Martian terrains constrain Mars' climate and aqueous alteration history. Early in its history, Mars experienced an atmospheric redox change and iron-bearing clay minerals may preserve the effects of that transition. Ferrous smectites, the thermodynamically predicted product of chemical weathering of basalts under anoxic conditions, may have undergone oxidation by exposure to chemical oxidants in the atmosphere or regolith, or by direct photooxidation at the surface. To assess these potential oxidation pathways, ferrous trioctahedral smectites of varying initial iron content were synthesized and subjected to oxidation by ultraviolet (UV) irradiation. Experimental UV irradiation under an anoxic atmosphere equivalent to approximately 7 years of flux on the Martian surface caused partial oxidation of smectite-bound Fe (Fe3+/ΣFe = 16–18%) and octahedral sheet contraction. Metal-OH vibrational bands in visible/near infrared (VNIR) reflectance spectra of oxidized smectites changed in band depth and asymmetry with higher iron content. X-ray diffraction patterns of UV irradiated samples indicate the formation of a mixed di- and trioctahedral smectite or a secondary nontronite phase, possibly on the surfaces of higher iron content smectites. These experiments suggest that UV irradiation is able to oxidize structurally bound iron in smectites without the presence of other chemical oxidants. Photooxidation may have influenced the mineralogy, both syndepositionally and postdepositionally, of Martian alteration assemblages formed near the surface and this process needs not be limited to one part of their formation history. Plain Language Summary: Martian mineral assemblages observed with orbiters and rover instruments allow us to understand the planet's past climate and aqueous activity. Hydrated minerals that contain Fe(II) are of particular interest as they would have been affected by the early atmosphere becoming more oxidizing overtime, changing the structural iron into Fe(III). In this study, we synthesized Fe(II) smectites with varying iron content and irradiated them with an ultraviolet (UV) light source to test whether they could be photooxidized. Iron in the smectite minerals was incompletely oxidized by UV radiation after being exposed for the equivalent of approximately 7 years of exposure on the early Mars surface. The smectites with higher iron content showed more changes with photooxidation in their visible/near infrared spectra as well as in their X-ray diffraction patterns, two datasets collected by instruments on currently active Martian missions. These results suggest that UV photooxidation is a plausible contributor to the mineralogy and redox state of clay mineral assemblages observed at the Martian surface.

V. B. Rivera Banuchi↗

NASA NTRS2011

Characterization of Axial Inducer Cavitation Instabilities via High Speed Video Recordings

Sub-scale water tests were undertaken to assess the viability of utilizing high resolution, high frame-rate digital video recordings of a liquid rocket engine turbopump axial inducer to characterize cavitation instabilities. These high speed video (HSV) images of various cavitation phenomena, including higher order cavitation, rotating cavitation, alternating blade cavitation, and asymmetric cavitation, as well as non-cavitating flows for comparison, were recorded from various orientations through an acrylic tunnel using one and two cameras at digital recording rates ranging from 6,000 to 15,700 frames per second. The physical characteristics of these cavitation forms, including the mechanisms that define the cavitation frequency, were identified. Additionally, these images showed how the cavitation forms changed and transitioned from one type (tip vortex) to another (sheet cavitation) as the inducer boundary conditions (inlet pressures) were changed. Image processing techniques were developed which tracked the formation and collapse of cavitating fluid in a specified target area, both in the temporal and frequency domains, in order to characterize the cavitation instability frequency. The accuracy of the analysis techniques was found to be very dependent on target size for higher order cavitation, but much less so for the other phenomena. Tunnel-mounted piezoelectric, dynamic pressure transducers were present throughout these tests and were used as references in correlating the results obtained by image processing. Results showed good agreement between image processing and dynamic pressure spectral data. The test set-up, test program, and test results including H-Q and suction performance, dynamic environment and cavitation characterization, and image processing techniques and results will be discussed.

Arellano, Patrick↗

NASA NTRS1974

Cosmic-ray streaming perpendicular to the mean magnetic field

Starting from a quasi-linear approximation for the ensemble-averaged particle distribution function in a random magnetic field, the complete diffusion tensor is derived. This is done by assuming a simple form for the ensemble-averaged distribution function, explicitly retaining all components of the streaming flux. This derivation obtains the antisymmetric terms in a natural manner. The necessary dropping of higher-order terms gives a criterion for the lower-energy limit of validity of the perpendicular and antisymmetric diffusion coefficients. The limit for the assumed distribution function is about 0.8 GV rigidity in the interplanetary field near 1 AU.

Forman, M. A.↗

NASA NTRS1978

Friction and wear behavior of single-crystal silicon carbide in sliding contact with various metals

Sliding friction experiments were conducted with single-crystal silicon carbide in contact with various metals. Results indicate the coefficient of friction is related to the relative chemical activity of the metals. The more active the metal, the higher the coefficient of friction. All the metals examined transferred to silicon carbide. The chemical activity of the metal and its shear modulus may play important roles in metal transfer, the form of the wear debris and the surface roughness of the metal wear scar. The more active the metal, and the less resistance to shear, the greater the transfer to silicon carbide and the rougher the wear scar on the surface of the metal. Hexagon shaped cracking and fracturing formed by cleavage of both prismatic and basal planes is observed on the silicon carbide surface.

Miyoshi, K.↗

NASA NTRS1985

Making Stronger Twine With Matched Strands

Higher tensil strength achieved with same production equipment. Strong twine made by using spools in one of two-step manufacturing process. Three primary strands twisted together in opposite direction to form threeply twine. Technique used successfully in manufacture of safety netting with 600- to 700-lb (2,700-to 3,100-N) tensil strength and 60-ton (54 x 10 to third power kg) tuna seine with area of 86 acres (3.5 x 10 to fifth power m2). Increase in tensil strength of completed twine found experimentally 10 to 12 percent.

Kirkland, W. L.↗

NASA NTRS1987

The ionization structure of planetary nebulae. 8: NGC 6826

Spectrophotometric observations of emission-line intensities over the spectral range 1400 to 1700 A were made in seven positions in the planetary nebulae NCG 6826. The O(++) electron temperature varies little from 8900 K throughout the nebula; the Balmer continuum electron temperature averages 1500 K higher. The wavelength 4267 C II line intensities imply C(++) abundances that are systematically higher than those determined from the wavelength 1906, 1909 C III lines, but because of uncertainties in the intensities of the ultraviolet lines relative to the optical ones, this discrepancy is less conclusively demonstrated in NGC 6826 than in other planetaries in this series. Standard equations used to correct for the existence of elements in other than the optically observable ionization stages give results that are consistent and also in approximate agreement with abundances calculated using ultraviolet lines in the few cases where the relevant ultraviolet lines are measurable. The results of the logarithmic abundances differ somewhat from the recent study by Aller and Czyzak, in part because their measured electron temperatures are somewhat higher. The Ar, Ne, and, to some extent, O and S abundances appear to be somewhat low, suggesting that the progenitor to NGC 6826 like that to NGC 7662, may have formed out of somewhat metal-poor material.

Barker, Timothy↗

NASA NTRS1988

Changing styles of crustal growth in Southern Africa: Constraints from geochemical and Sr-Nd isotope studies in Archaean to Pan African terrains

Nd isotopic data was presented for southern Africa in support of episodic crustal growth. Over 50 percent of the continental crust there had formed before 2.5 Ga, and less than 10 percent was produced after about 1.0 Ga. The data imply a mean crustal age of about 2.4 Ga for southern Africa, and a higher rate of crustal growth than that derived from Australian shale data, particularly during the Proterozoic. Isotopic data from Damara metasediments imply that there is no need to invoke decoupling of the Rb-Sr and Sm-Nd systems in the continental crust.

Mcdermott, F.↗

NASA NTRS1988

The ionization structure of planetary nebulae. VIII - NGC 6826

Spectrophotometric observations of emission-line intensities over the spectral range 1400 to 1700 A were made in seven positions in the planetary nebulae NGC 6826. The O(++) electron temperature varies little from 8900 K throughout the nebula; the Balmer continuum electron temperature averages 1500 K higher. The wavelength 4267 C II line intensities imply C(++) abundances that are systematically higher than those determined from the wavelength 1906, 1909 C III lines, but because of uncertainties in the intensities of the ultraviolet lines relative to the optical ones, this discrepancy is less conclusively demonstrated in NGC 6826 than in other planetaries in this series. Standard equations used to correct for the existence of elements in other than the optically observable ionization stages give results that are consistent and also in approximate agreement with abundances calculated using ultraviolet lines in the few cases where the relevant ultraviolet lines are measurable. The results of the logarithmic abundances differ somewhat from the recent study by Aller and Czyzak, in part because their measured electron temperatures are somewhat higher. The Ar, Ne, and, to some extent, O and S abundances appear to be somewhat low, suggesting that the progenitor to NGC 6826 like that to NGC 7662, may have formed out of somewhat metal-poor material.

Barker, Timothy↗

NASA NTRS1990

Superplastically Formed Titanium Hat-Stiffened Panels

Recent advances in superplastic forming of some metals make it possible to fabricate new shapes. Superplastic forming enables design of structures using mass more efficiently. Parts having intersecting compound contour surfaces made; impossible to fabricate such parts by more conventional methods. Beaded hat-stiffened panel has higher critical buckling strain than conventional hat-stiffened panel.

Davis, Randall C.↗

NASA NTRS1990

Advanced tube-bundle rocket thrust chamber

An advanced rocket thrust chamber for future space application is described along with an improved method of fabrication. Potential benefits of the concept are improved cyclic life, reusability, and performance. Performance improvements are anticipated because of the enhanced heat transfer into the coolant which will enable higher chamber pressure in expander cycle engines. Cyclic life, reusability and reliability improvements are anticipated because of the enhanced structural compliance inherent in the construction. The method of construction involves the forming of the combustion chamber with a tube-bundle of high conductivity copper or copper alloy tubes, and the bonding of these tubes by an electroforming operation. Further, the method of fabrication reduces chamber complexity by incorporating manifolds, jackets, and structural stiffeners while having the potential for thrust chamber cost and weight reduction.

Kazaroff, John M.↗

NASA NTRS1990

Advanced tube-bundle rocket thrust chamber

Kazaroff, John M.↗

NASA NTRS1991

Distribution of silicon between kamacite and taenite

Meteorites formed under highly reducing conditions can incorporate substantial amounts of Si in solid solution in their metallic phases. In enstatite meteorites, reduced Si appears in shreibersite, perryite and, in variable amounts, in the kamacite, taenite, and tetrataenite. Microprobe bulk analysis of Si in Fe,Ni particles of aubrites show a large variation from grain to grain; this large compositional range has been attributed to local equilibrium conditions in the specific T and/or fO2 environments in which they are formed. Si concentrations are homogeneous in the kamacite; in contrast, the Ni-rich phases (taenite and tetrataenite) show a characteristic Si profile. Concentrations of this element in tetrataenite are substantially higher than in the adjacent kamacite, and decrease smoothly towards the center of the taenite grain, matching very closely the M-shaped profile of Ni. Other elements with similar distribution patterns are Ge and Cu. A satisfactory explanation for this behavior cannot be given in the absence of experimental data for the diffusion of Si between alpha and gamma-Fe alloys. However, two end-member possibilities can be envisioned: the distribution of Si between kamacite and taenite may be controlled by (1) the crystallographic structure or (2) the chemical composition of the host phases. These possibilities are explored.

Casanova, Ignacio↗

NASA NTRS1958

Investigation of the Static Lateral Stability and Aileron Characteristics of a 0.067-Scale Model of the Bell X-2 Airplane at Mach Numbers of 2.29, 2.78, 3.22, and 3.71

Tests were performed in the high. Mach number test section of the Langley Unitary Plan wind tunnel to determine the static lateral stability. and aileron characteristics of a 0.067-scale model of the Bell X-2 airplane at Mach numbers of 2.29, 2. 78, 3.22, and. 3.71. The results of this investigation indicated that the directional stability of the model was low with directional instability occurring at Mach numbers higher than 3.1 and. angles of attack higher than about 5.0 deg (equivalent lift coefficient of about 0.18). The yaw due to aileron deflection was adverse and, with 10 deg of differential aileron deflection, large enough to overbalance the available directional restoring moment at all angles of attack higher than about 5.0 deg (equivalent lift coefficient of about 0.21) and Mach numbers higher than 2. 5. The model also had positive effective dihedral for all test attitudes and. Mach numbers. A combination of the lateral-stability parameters with the aileron characteristics to form a lateral-stability criterion for a maneuver using ailerons alone indicated that the model has characteristics which would. give unstable aperiodic behavior (divergence) over a large part of the test Mach number and angle-of-attack range.

Fournier, Roger H.↗

NASA NTRS1997

A Unique Test Facility to Measure Liner Performance with a Summary of Initial Test Results

A very ambitious study was initiated to obtain detailed acoustic and flow data with and without a liner in a duct containing a mean flow so that available theoretical models of duct liners can be validated. A unique flow-duct facility equipped with a sound source, liner box, flush-walled microphones, traversable microphones and traversable pressure and temperature probes was built. A unique set of instrumentation boxes equipped with computer controlled traverses were designed and built that allowed measurements of Mach number, temperature, SPLs and phases in two planes upstream of a liner section and two planes downstream at a large number of measurement points. Each pair of planes provided acoustic pressure gradients for use in estimating the particle velocities. Specially-built microphone probes were employed to make measurements in the presence of the flow. A microphone traverse was also designed to measure the distribution of SPLs and phases from the beginning of the liner to its end along the duct axis. All measurements were made with the help of cross-correlation techniques to reject flow noise and/or other obtrusive noise, if any. The facility was designed for future use at temperatures as high as 1500 F. In order to validate 2-D models in the presence of mean flow, the flow duct was equipped with a device to modify boundary layer flow on the smaller sides of a rectangular duct to simulate 2-D flow. A massive amount of data was acquired for use in validating duct liner models and will be provided to NASA in an electronic form. It was found that the sound in the plane-wave regime is well behaved within the duct and the results are repeatable from one run to another. At the higher frequencies corresponding to the higher-order modes, the SPLs within a duct are not repeatable from run to run. In fact, when two or more modes have the same frequency (i.e., for the degenerate modes), the SPLs in the duct varied between 2 dB to 12 dB from run to run. This made the calibration of the microphone probes extremely difficult at the higher frequencies.

Ahuja, K. K.↗

NASA NTRS1997

Flow Quality and Boundary Layer Transition

The widely held view is that transition to turbulence in the Blasius boundary layer occurs via amplification and eventual nonlinear breakdown of initially small amplitude instabilities i.e. Tollmien-Schlichting (TS) waves. However this scenario is only observed for low amplitude free-stream turbulence levels, i.e. u/U < 0.1%. Bypass of linear TS instability mechanism occurs for higher EST levels, yet considerable differences exist between the few experiments carefully designed to assess the effect of EST on transition. The consensus is that EST leads to longitudinal streaks that form near the leading edge in the boundary layer . These streaks appeal to be regions of concentrated streamwise vorticity and they are often referred to as Klebanoff modes. The importance of mean flow free-stream nonuniformity (FSN) is not as widely appreciated as EST for characterizing wind tunnel flow quality. Here it is shown that, although the v like generated by a d=50micron wire located upstream of the contraction (Re(sub d)=6.6, x/d=45,000) is immeasurably small by the time it interacts with the leading edge in the test section, it is responsible for generation of a pair of weak streamwise vortices in the boundary layer downstream. The characteristics of these wake-induced vortices and their effect on TS waves are demonstrated. Small remnant FSN variations are also shown to exist downstream of a turbulence grid. The question arises Are the adverse effects introduced by the turbulence grid caused by FST or by small remnant FSN variations?

Watmuff, Jonathan H↗

NASA NTRS2002

High Precision Grids for Neutron, Hard X-Ray, and Gamma-Ray Imaging Systems

Fourier telescopes permit observations over a very broad band of energy. They generally include synthetic spatial filtering structures, known as multilayer grids or grid pairs consisting of alternate layers of absorbing and transparent materials depending on whether neutrons or photons are being imaged. For hard x-rays and gamma rays high (absorbing) and low (transparent) atomic number elements, termed high-Z and low-Z materials may be used. Fabrication of these multilayer grid structures is not without its difficulties. Herein the alternate layers of the higher material and the lower material are inserted in a polyhedron, transparent to photons of interest, through an open face of the polyhedron. The inserted layers are then uniformly compressed to form a multilayer grid.

Jonathan W Campbell↗

NASA NTRS2006

The NASA Software Research Infusion Initiative: Successful Technology Transfer for Software Assurance

New processes, methods and tools are constantly appearing in the field of software engineering. Many of these augur great potential in improving software development processes, resulting in higher quality software with greater levels of assurance. However, there are a number of obstacles that impede their infusion into software development practices. These are the recurring obstacles common to many forms of research. Practitioners cannot readily identify the emerging techniques that may most benefit them, and cannot afford to risk time and effort in evaluating and experimenting with them while there is still uncertainty about whether they will have payoff in this particular context. Similarly, researchers cannot readily identify those practitioners whose problems would be amenable to their techniques and lack the feedback from practical applications necessary to help them to evolve their techniques to make them more likely to be successful. This paper describes an ongoing effort conducted by a software engineering research infusion team, and the NASA Research Infusion Initiative, established by NASA s Software Engineering Initiative, to overcome these obstacles.

Hinchey, Michael G.↗

NASA NTRS2006

Geology of the Gusec cratered plains from the Spirit rover transverse

The cratered plains of Gusev traversed by Spirit are generally low-relief rocky plains dominated by impact and eolian processes. Ubiquitous shallow, soil-filled, circular depressions, called hollows, are modified impact craters. Rocks are dark, fine-grained basalts, and the upper 10 m of the cratered plains appears to be an impact-generated regolith developed over intact basalt flows. Systematic field observations across the cratered plains identified vesicular clasts and rare scoria similar to original lava flow tops, consistent with an upper inflated surface of lava flows with adjacent collapse depressions. Crater and hollow morphometry are consistent with most being secondaries. The size frequency distribution of rocks >0.1 m diameter generally follows exponential functions similar to other landing sites for total rock abundances of 5-35%. Systematic clast counts show that areas with higher rock abundance and more large rocks have higher thermal inertia. Plains with lower thermal inertia have fewer rocks and substantially more pebbles that are well sorted and evenly spaced, similar to a desert pavement or lag. Eolian bed forms (ripples and wind tails) have coarse surface lags, and many are dust covered and thus likely inactive. Deflation of the surface _5-25 cm likely exposed two-toned rocks and elevated ventifacts and transported fines into craters creating the hollows. This observed redistribution yields extremely slow average erosion rates of _0.03 nm/yr and argues for very little long-term net change of the surface and a dry and desiccating environment similar to today's since the Hesperian (or _3 Ga).

Spirit↗