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At least 829 records · Page 46
All sourcesNASA NTRSDOE OSTI
DOE OSTI2020

Stabilization of Low Valent Zirconium Nitrides in Titanium Nitride via Plasma-Enhanced Atomic Layer Deposition and Assessment of Electrochemical Properties

The increasing awareness of metal nitrides as feasible electrocatalysts in numerous energy-relevant transformations motivates greater synthetic control of mixed metal nitride compositions and their valence states. We report plasma-enhanced atomic layer deposition of titanium zirconium nitride, with an emphasis on the experimental parameters that influence the valence states of the two metal ions. We further examined the consequence of various ratios of Ti and Zr on the electrochemically active surface areas (ECSAs). Films with a Zr-to-Ti ratio of 1:2 or 1:1 yielded the highest ECSA; deviation from these values led to a large fraction of electrically insulating or semiconducting titanium or zirconium oxynitrides/oxides. The systematic examination establishes a fundamental structure-property relationship critical to assessing the electrochemical/electrocatalytic properties of metal nitrides.

36 MATERIALS SCIENCE↗
NASA NTRS1990

Ion Beam Heating in the Auroral Zone

Recent satellite observations at high altitudes (greater than 5000 km) in the auroral zone have shown the existence of hybrid or bimodal ion beam distributions that are evidence of both parallel and perpendicular ion acceleration. Acceleration parallel to the magnetic field is most likely due to quasi-static electric fields (double layers) which can create outflowing ion beams; since ions of different mass will have different drift speeds due to this acceleration, a plasma configuration unstable to the ion-ion two-stream acoustic mode develops. When the net drift velocity (U) between the two ion species is greater than the sound speed (C(sub 0)), the ion-ion instability has maximum growth at oblique wave propagation. To study the nonlinear effects of the ion-ion instability in terms of plasma heating, a numerical simulation parametric study has been performed. It was found that the parallel acceleration that forms the ion beams occurs on a time scale faster than ion- ion wave growth at low drifts; thus ion-ion wave growth is expected to occur primarily for higher drift speeds (U greater than C(sub 0)) which results in strong oblique heating of the ions (both hydrogen and oxygen) forming elevated ion conics (sometimes called 'bowl' distributions). Also, strong parallel electron heating in the direction of the ion beams can occur, and electrons near the top of the acceleration region may attain a net upward drift along with the elevated ion conics. Variation of the oxygen density greatly affects the ion heating due to the ion-ion instability; as the oxygen density decreases, oxygen heating increases, in agreement with observations (Collin et al., 1987). Ion-ion electrostatic wave properties and the plasma heating that results over a wide range of auroral zone parameters are included.

Schriver, David↗
NASA NTRS1998

Constraints on Nonlinear and Stochastic Growth Theories for Type 3 Solar Radio Bursts from the Corona to 1 AU

Existing, competing theories for coronal and interplanetary type III solar radio bursts appeal to one or more of modulational instability, electrostatic (ES) decay processes, or stochastic growth physics to preserve the electron beam, limit the levels of Langmuir-like waves driven by the beam, and produce wave spectra capable of coupling nonlinearly to generate the observed radio emission. Theoretical constraints exist on the wavenumbers and relative sizes of the wave bandwidth and nonlinear growth rate for which Langmuir waves are subject to modulational instability and the parametric and random phase versions of ES decay. A constraint also exists on whether stochastic growth theory (SGT) is appropriate. These constraints are evaluated here using the beam, plasma, and wave properties (1) observed in specific interplanetary type III sources, (2) predicted nominally for the corona, and (3) predicted at heliocentric distances greater than a few solar radii by power-law models based on interplanetary observations. It is found that the Langmuir waves driven directly by the beam have wavenumbers that are almost always too large for modulational instability but are appropriate to ES decay. Even for waves scattered to lower wavenumbers (by ES decay, for instance), the wave bandwidths are predicted to be too large and the nonlinear growth rates too small for modulational instability to occur for the specific interplanetary events studied or the great majority of Langmuir wave packets in type III sources at arbitrary heliocentric distances. Possible exceptions are for very rare, unusually intense, narrowband wave packets, predominantly close to the Sun, and for the front portion of very fast beams traveling through unusually dilute, cold solar wind plasmas. Similar arguments demonstrate that the ES decay should proceed almost always as a random phase process rather than a parametric process, with similar exceptions. These results imply that it is extremely rare for modulational instability or parametric decay to proceed in type III sources at any heliocentric distance: theories for type III bursts based on modulational instability or parametric decay are therefore not viable in general. In contrast, the constraint on SGT can be satisfied and random phase ES decay can proceed at all heliocentric distances under almost all circumstances. (The contrary circumstances involve unusually slow, broad beams moving through unusually hot regions of the Corona.) The analyses presented here strongly justify extending the existing SGT-based model for interplanetary type III bursts (which includes SGT physics, random phase ES decay, and specific electromagnetic emission mechanisms) into a general theory for type III bursts from the corona to beyond 1 AU. This extended theory enjoys strong theoretical support, explains the characteristics of specific interplanetary type III bursts very well, and can account for the detailed dynamic spectra of type III bursts from the lower corona and solar wind.

Cairns, Iver H.↗
NASA NTRS1972

Area influences and floating potentials in Langmuir probe measurements.

Analysis of the influence of a relatively small reference electrode on a Langmuir probe measurement of plasma density and temperature. The analysis employs the collisionless theory of Laframboise for spherical and cylindrical probes and in a completely general way includes a broad range of electron densities and temperatures, as well as all possible values of ion mass and multiplicity of ionization. It is shown that a ratio alpha of reference-electrode area to probe area of 10,000 will guarantee no distortion of the measurement as a result of a shifting reference-electrode potential. It is further shown that the constraint on alpha can be relaxed by approximately two orders of magnitude when the charge-normalized ion mass is decreased from 200 to 1 amu and the ratio of reference-electrode radius to Debye length is decreased from 100 to 0. An additional result of the analysis is the dependence of a probe's floating potential on its geometry and radius, as well as on the properties of the plasma. A discussion of the latter result reveals in a striking manner the significant differences between the ion-current responses of spherical and cylindrical probes.

Szuszczewicz, E. P.↗
DOE OSTI2020

Transport of High-energy Charged Particles through Spatially Intermittent Turbulent Magnetic Fields

Identifying the sources of the highest energy cosmic rays requires understanding how they are deflected by the stochastic, spatially intermittent intergalactic magnetic field. Here we report measurements of energetic charged-particle propagation through a laser-produced magnetized plasma with these properties. We characterize the diffusive transport of the particles experimentally. The results show that the transport is diffusive and that, for the regime of interest for the highest-energy cosmic rays, the diffusion coefficient is unaffected by the spatial intermittency of the magnetic field.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2020

2021 Stewardship Science Academic Programs Annual

I am a staff scientist at Sandia National Laboratories (SNL). I work on multiple fundamental-science projects and lead modeling/data-analysis for the stellar opacity experiments. I also work with theorists to refine plasma material-property calculations to make NNSA simulations more predictable. These are challenging and important problems for national security. In fact, our experiments raised questions about “opacity”, the property of matter that controls energy transport inside stars. This work was published by Nature due to its serious implication over broad applications, and our team received NNSA Defense Program Award of Excellence, both in 2015. Work at SNL is collegial and full of learning through interactions with the world’s finest experimentalists and theorists. When I started my Ph.D. program, working at a national lab was a dream position. Today, I collaborate with top scientists to solve mission-critical problems. The Stewardship Science Academic Programs (SSAP) and National Laser Users’ Facility (NLUF) played a vital role in the efficient learning and seamless transition to SNL.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
NASA NTRS2004

Properties of Minor Ions in the Solar Wind and Implications for the Background Solar Wind Plasma

The scope of the investigation is to extract information on the properties of the bulk solar wind from the minor ion observations that are provided by instruments on board NASA space craft and theoretical model studies. Ion charge states measured in situ in interplanetary space are formed in the inner coronal regions below 5 solar radii, hence they carry information on the properties of the solar wind plasma in that region. The plasma parameters that are important in the ion forming processes are the electron density, the electron temperature and the flow speeds of the individual ion species. In addition, if the electron distribution function deviates from a Maxwellian already in the inner corona, then the enhanced tail of that distribution function, also called halo, greatly effects the ion composition. This study is carried out using solar wind models, coronal observations, and ion calculations in conjunction with the in situ observations.

Wagner, William↗
DOE OSTI2022

Proton stopping measurements at low velocity in warm dense carbon

Abstract Ion stopping in warm dense matter is a process of fundamental importance for the understanding of the properties of dense plasmas, the realization and the interpretation of experiments involving ion-beam-heated warm dense matter samples, and for inertial confinement fusion research. The theoretical description of the ion stopping power in warm dense matter is difficult notably due to electron coupling and degeneracy, and measurements are still largely missing. In particular, the low-velocity stopping range, that features the largest modelling uncertainties, remains virtually unexplored. Here, we report proton energy-loss measurements in warm dense plasma at unprecedented low projectile velocities. Our energy-loss data, combined with a precise target characterization based on plasma-emission measurements using two independent spectroscopy diagnostics, demonstrate a significant deviation of the stopping power from classical models in this regime. In particular, we show that our results are in closest agreement with recent first-principles simulations based on time-dependent density functional theory.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2024

Nonlinear coupling of tearing modes in reversed field pinch plasmas with stepped pressure profiles

A theory of the three-wave coupling of triplets of tearing modes in toroidal pinches [i.e., either reversed field pinches (RFPs) or tokamaks] was proposed by R. Fitzpatrick [Phys. Plasmas 6, 1168 (1999)]. However, this theory only applies to toroidal pinches with negligible equilibrium plasma pressure gradients. Such a limitation is particularly inappropriate to RFPs. This paper generalizes the analysis of R. Fitzpatrick [Phys. Plasmas 6, 1168 (1999)] in order to take the equilibrium pressure gradient into account. However, for the sake of simplicity, a stepped pressure profile, rather than a continuous profile, is employed. In the limit in which the number of steps becomes very large, the results obtained from the generalized theory are presumably equivalent to those that would have been achieved using a continuous pressure profile. The generalized theory is used to investigate the formation of the characteristic toroidally localized pattern of phase-locked m = 1 and m = 0 tearing modes in RFP plasmas that is known as the “slinky” pattern. The incorporation of the equilibrium plasma pressure into the analysis is found to be of crucial importance when determining the properties of the pattern. This is the case because the plasma pressure controls the number of unstable m = 1 and m = 0 tearing modes, and also significantly affects the strength of three-wave coupling, as well as the phase relation between the phase-locked m = 1 and m = 0 modes.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2023

Growth or Decay – I: universality of the turbulent dynamo saturation

The turbulent small-scale dynamo (SSD) is likely to be responsible for the magnetisation of the interstellar medium (ISM) that we observe in the Universe today. The SSD efficiently converts kinetic energy E kin into magnetic energy E mag , and is often used to explain how an initially weak magnetic field with E mag $\ll$ E kin is amplified, and then maintained at a level E mag ≲ E kin . Usually, this process is studied by initialising a weak seed magnetic field and letting the turbulence grow it to saturation. However, in this Part I of the Growth or Decay series, using three-dimensional, visco-resistive magnetohydrodynamical turbulence simulations up to magnetic Reynolds numbers of 2000, here we show that the same final state in the integral quantities, energy spectra, and characteristic scales of the magnetic field can also be achieved if initially E mag ~ E kin or even if initially E mag $\gg$ E kin . This suggests that the final saturated state of the turbulent dynamo is set by the turbulence and the material properties of the plasma, independent of the initial structure or amplitude of the magnetic field. We discuss the implications this has for the maintenance of magnetic fields in turbulent plasmas and future studies exploring the dynamo saturation.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2022

Microstructural Transitions during Powder Metallurgical Processing of Solute Stabilized Nanostructured Tungsten Alloys

Exploiting grain boundary engineering in the design of alloys for extreme environments provides a promising pathway for enhancing performance relative to coarse-grained counterparts. Due to its attractive properties as a plasma facing material for fusion devices, tungsten presents an opportunity to exploit this approach in addressing the significant materials challenges imposed by the fusion environment. Here, we employ a ternary alloy design approach for stabilizing W against recrystallization and grain growth while simultaneously enhancing its manufacturability through powder metallurgical processing. Mechanical alloying and grain refinement in W-10 at.% Ti-(10,20) at.% Cr alloys are accomplished through high-energy ball milling with transitions in the microstructure mapped as a function of milling time. We demonstrate the multi-modal nature of the resulting nanocrystalline grain structure and its stability up to 1300 °C with the coarser grain size population correlated to transitions in crystallographic texture that result from the preferred slip systems in BCC W. Field-assisted sintering is employed to consolidate the alloy powders into bulk samples, which, due to the deliberately designed compositional features, are shown to retain ultrafine grain structures despite the presence of minor carbides formed during sintering due to carbon impurities in the ball-milled powders.

36 MATERIALS SCIENCE↗
NASA NTRS1964

Interplanetary magnetic fields.

Interplanetary magnetic fields discussing effects of solar plasma on origin, properties, irregularities and disturbances

SOLAR WIND↗
NASA NTRS1983

An experimental investigation and numerical prediction of thermomechanical phenomena in high speed rotor tip rubbing

A thermomechanical study of the intermittent rubbing of a rotor blade tip and a casing seal is carried out taking into account the existence of thermal contact resistance. The effect of the thermal properties of a plasma sprayed coating on the blade tip is studied. The influence of a variable heat generation and variable thermal contact resistance at the blade tip as it passes along the path of rubbing is also discussed.

Emery, A. F.↗