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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 829 records · Page 46
All sourcesNASA NTRSDOE OSTI
DOE OSTI2017

Mathematical Calibration of Modular Plastic Scintillators for Various Assay Applications - 17322

Plastic scintillators provide an inexpensive option to assay and characterize radioactive material. Due to the low cost it is generally possible to an array of large numbers of plastic scintillators to achieve high measurement efficiencies. The beta only thin plastic scintillators used in the Argos contamination monitors provide a convenient and reliable scintillator package that can be grouped together to form an assay system. Mathematical calibrations, using MCNP, have been produced for this detector that allow for rapid construction of various custom measurement geometries. The calibrations were constructed by comparing a series of measurements made with a number of beta and beta/gamma emitting nuclides. Characterization of the beta scintillators utilized beta emitting nuclides that included spectra from low average energy, e.g. C-14, to relatively high average energy, e.g. Sr/Y-90. In order to perform the calibration, custom versions of the standard Argos scintillators were produced that provide an MCA output for spectroscopic investigation. The spectra were then compared to detailed MCNP models in an iterative process to energy calibrate and efficiency calibrate each detector type. The validated models and energy calibrations were then tested against a number of volumetric geometries to confirm that the model would translate well to any other geometry. These validated models can then be used to rapidly construct custom measurement geometries for material measurement and screening. Two examples of measurement applications include a beta screening system for dirt on a conveyor belt and a flow through beta liquid assay system. The mathematical calibration process, validation results, and a number of application examples are discussed. (authors)

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2026

A Comprehensive Calibration Framework for the Northwest River Forecast Center

We present a comprehensive framework developed by the Northwest River Forecast Center for calibrating hydrologically diverse basins. The framework includes models for snow, soil moisture, routing, channel loss, and consumptive use. Data inputs include a wide range of open-access datasets for meteorology, land use, topography, and land cover. The framework uses conceptual hydrologic models to handle basins with various hydrologic regimes including rain-driven and snowmelt-dominated basins. We also develop a flexible automatic calibration system that can handle numerous unobservable model parameters in a computationally efficient manner. A single-basin automatic calibration run can typically be completed on a modern laptop in under 10 min. We found that model performance metrics for this new approach match the quality of the NWRFC's previous labor-intensive manual calibrations. The model performance also rivals that of a state-of-the-art deep learning model at a fraction of the computational cost. This framework presents a new standard for the quality of calibrations possible with lumped conceptual hydrologic models, combining careful data curation, an objective calibration framework, and expert local knowledge. In addition, we have made software packages available for the entire suite of National Weather Service River Forecast System models, including SAC-SMA, SNOW-17, and Lag-K. These modern interfaces are intended to increase accessibility and facilitate future research.

Forecasting↗
NASA NTRS1971

Calibration of solar cells using high-altitude aircraft.

A high altitude airplane has been used to obtain the outer space short circuit current of solar cells. The solar cells are mounted in a collimating tube and are measured at approximately 5000 foot intervals between 12,000 and 47,000 feet. The air mass is calculated for each altitude using the standard formula and the resulting curve is extrapolated to air mass zero. The effects on the solar cell output of a haze layer located at the tropopause has been observed. It is necessary to fly above this layer to ensure accurate results. Airplane calibrations of several primary standard cells calibrated on high altitude balloons show agreement within 0.5 per cent. Prediction of the output of satellite power supplies using airplane calibrated cells shows an accuracy of better than 1 per cent.

Brandhorst, H. W., Jr.↗
DOE OSTI2022

Methods—A Practical Approach to the Reversible Hydrogen Electrode Scale

Accurately quantifying applied potential is important to ensuring the comparability, accuracy, and precision of electrochemical studies. Reference electrodes (REs) enable knowledge/determination of the applied potential at electrodes in electrochemical systems. Ultimately, the choice of RE will depend on the particular requirements of a given electrochemical system, however, we note it is imperative to ensure the accuracy of the RE potential and its proper translation to a standardized scale. In this work, we highlight that while there are many commercially available REs, these must be experimentally calibrated to a reliable and practical standard potential scale, for instance the reversible hydrogen electrode (RHE) scale for aqueous systems. With representative data, we provide streamlined instructions on how to calibrate any RE to the RHE scale. We also provide guidance to mitigate and/or avoid possible electrolyte contamination issues arising from REs. Moreover, we offer a step-by-step guide on how to build a practical RHE RE, which may be a suitable and desirable option in certain applications. Our work emphasizes the need for the continuous adoption of standardized reference potential scales and demonstrates the versatility of the RHE scale, particularly in aqueous electrochemistry.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
NASA NTRS1996

Spectral Irradiance Calibration in the Infrared. 7. 5-14 microns Spectroscopy of the Asteroids Ceres, Vesta, and Pallas

We describe our efforts to seek "closure" in our infrared absolute calibration scheme by comparing spectra of asteroids, absolutely calibrated through reference stars, with "Standard Thermal Models" and "Thermophysical Models" for these bodies. Our use of continuous 5-14 microns airborne spectra provides complete sampling of the rise to, and peak, of the infrared spectral energy distribution and constrains these models. Such models currently support the absolute calibration of ISO-PHOT at far-infrared wave- lengths (as far as 300 microns), and contribute to that of the Mid-Infrared Spectrometer on the "Infrared Telescope in Space" in the 6-12 microns region. The best match to our observed spectra of Ceres and Vesta is a, standard thermal model using a beaming factor of unity. We also report the presence of three emissivity features in Ceres which may complicate the traditional model extrapolation to the far-infrared from contemporaneous ground-based N-band photometry that is used to support calibration of, for example, ISO-PHOT. While identification of specific materials that cause these features is not made, we discuss families of minerals that may be responsible.

Cohen, Martin↗
NASA NTRS1998

Spectral Irradiance Calibration in the Infrared: 5-14 Micron Spectroscopy of the Asteroids Ceres, Vesta, and Pallas - 8

We describe our efforts to seek "closure" in our infrared absolute calibration scheme by comparing spectra of asteroids, absolutely calibrated through reference stars, with "standard thermal models" and "thermophysical models" for these bodies. Our use of continuous 5-14 microns airborne spectra provides complete sampling of the rise to, and peak, of the infrared spectral energy distribution and constrains these models. Such models currently support the absolute calibration of the Infrared Space Observatory Imaging Photopolarimeter (ISOPHOT) at far-infrared wavelengths (as far as 300 microns) and contribute to that of the Mid-Infrared Spectrometer on the Infrared Telescope in Space in the 6 - 12 microns region. The best match to our observed spectra of Ceres and Vesta is a standard thermal model using a beaming factor of unity. We also report the presence of three emissivity features in Ceres that may complicate the traditional model extrapolation to the far-infrared from contemporaneous ground-based N-band photometry that is used to support calibration of, for example, ISOPHOT. While identification of specific materials that cause these features is not made, we discuss families of minerals that may be responsible.

Cohen, Martin↗
DOE OSTI2017

In Pursuit of a High-Temperature, High-Pressure, High-Viscosity Standard: The Case of Tris(2-ethylhexyl) Trimellitate

This study presents a reference correlation for the viscosity of tris(2-ethylhexyl) trimellitate designed to serve in industrial applications for the calibration of viscometers at elevated temperatures and pressures such as those encountered in the exploration of oil reservoirs and in lubrication. Tris(2-ethylhexyl) trimellitate has been examined with respect to the criteria necessary for an industrial standard reference material such as toxicity, thermal stability, and variability among manufactured lots. The viscosity correlation has been based upon all of the data collected in a multinational project and is supported by careful measurements and analysis of all the supporting thermophysical property data that are needed to apply the standard for calibration to a wide variety of viscometers. The standard reference viscosity data cover temperatures from 303 to 473 K, pressures from 0.1 to 200 MPa, and viscosities from approximately 1.6 to 755 mPa s. The uncertainty in the data provided is of the order of 3.2% at 95% confidence level, which is thought to be adequate for most industrial applications.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2022

Maximum Likelihood Spectrum Decomposition for Isotope Identification and Quantification

A spectral decomposition method has been implemented to identify and quantify isotopic source terms in high-resolution gamma-ray spectroscopy in static geometry and shielding scenarios. Monte Carlo simulations were used to build the response matrix of a shielded high-purity germanium detector monitoring an effluent stream with a Marinelli configuration. The decomposition technique was applied to a series of calibration spectra taken with the detector using a multi-nuclide standard. These results are compared with decay-corrected values from the calibration certificate. For most nuclei in the standard ( 241 Am, 109 Cd, 137 Cs, and 60 Co), the deviations from the certificate values were generally no more than 6% with a few outliers as high as 10%. Furthermore, for 57 Co, the radionuclide with the lowest activity, the deviations from the standard reached as high as 25%, driven by the meager statistics in the calibration spectra. In addition, a complete treatment of error propagation for the technique is presented.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗
DOE OSTI2014

SU-E-QI-06: Design and Initial Validation of a Precise Capillary Phantom to Test Perfusion Systems

Purpose: To design a precise perfusion phantom mimicking capillaries of the brain vasculature which could be used to test various perfusion protocols and algorithms which generate perfusion maps. Methods: A perfusion phantom was designed in Solidworks and built using additive manufacturing. The phantom was an overall cylindrical shape of diameter and height 20mm and containing capillaries of 200μm or 300μm which were parallel and in contact making up the inside volume where flow was allowed. We created a flow loop using a peristaltic pump and contrast agent was injected manually. Digital Subtraction Angiographic images and low contrast images with cone beam CT were acquired after the contrast was injected. These images were analyzed by our own code in LabVIEW software and Time-Density Curve, MTT and TTP was calculated. Results: Perfused area was visible in the cone beam CT images; however, individual capillaries were not distinguishable. The Time-Density Curve acquired was accurate, sensitive and repeatable. The parameters MTT, and TTP offered by the phantom were very sensitive to slight changes in the TDC shape. Conclusion: We have created a robust calibrating model for evaluation of existing perfusion data analysis systems. This approach is extremely sensitive to changes in the flow due to the high temporal resolution and could be used as a golden standard to assist developers in calibrating and testing of imaging perfusion systems and software algorithms. Supported by NIH Grant: 2R01EB002873 and an equipment grant from Toshiba Medical Systems Corporation.

62 RADIOLOGY AND NUCLEAR MEDICINE↗
DOE OSTI2017

Variations in AmLi source spectra and their estimation utilizing the 5 Ring Multiplicity Counter

Active-mode assay systems are widely used for the safeguards of uranium items to verify compliance with the Non-Proliferation Treaty. Systems such as the Active-Well Coincidence Counter (AWCC) and the Uranium Neutron Coincidence Collar (UNCL) use americium-lithium (AmLi) neutron sources to induce fissions which are measured to determine the sample mass. These systems have historically relied on calibrations derived from well-defined standards. Recently, restricted access to standards or more difficult measurements have resulted in a reliance on modeling and simulation for the calibration of systems, which introduces potential simulation biases. Furthermore, the AmLi source energy spectra commonly used in the safeguards community do not accurately represent measurement results and the spectrum uncertainty can represent a large contribution to the total modeling uncertainty in active-mode systems.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
NASA NTRS2006

Results and Lessons from MODIS Thermal Emissive Bands Calibration: Pre-launch to On-orbit

MODIS is a major instrument for the NASA EOS Terra (launched in December 1999) and Aqua (launched in May 2002) missions. It was designed and built to enhance and extend its heritage sensors' measurements and data records with applications covering a wide range of studies of the Earth's land, oceans, and atmosphere. Its 16 thermal emissive bands (TEB), each with 10 detectors, are located on the two cold focal plane assemblies (FPAs) controlled by a passive radiative cooler. Because of instrument design complexity and stringent calibration requirements, extensive calibration and characterization activities were conducted pre-launch by the sensor vendor for both Terra and Aqua MODIS. For TEB, these activities include characterization of detectors' noise and non-linearity and evaluation of their radiometric performance in thermal vacuum at difference instrument temperatures and FPA temperatures. In addition TEB system level response versus scan-angle (RVS) and relative spectral response (RSR) were characterized. MODIS TEB radiometric calibration transfer from pre-launch to on-orbit was performed using spectral bands' responses to the instrument on-board blackbody and a laboratory blackbody calibration source (BCS) traceable to NIST standards. This paper provides a summary of MODIS TEB pre-launch and on-orbit calibration and characterization activities, challenges, data analysis results, and lessons learned with focus on sensors' radiometric performance. A comparison between Terra and Aqua MODIS TEB performance is also presented. A similar summary for the reflective solar bands (RSB) is reported in a separate paper in these proceedings.

Xiong, X.↗
NASA NTRS1999

Radiometric Calibration of the NASA Advanced X-Ray Astrophysics Facility

We present the results of absolute calibration of the quantum efficiency of soft x-ray detectors performed at the PTB/BESSY beam lines. The accuracy goal is 1%. We discuss the implementation of that goal. These detectors were used as transfer standards to provide the radiometric calibration of the AXAF X-ray observatory, to be launched in April 1999.

Kellogg, Edwin M.↗
NASA NTRS2002

The Use of Transfer Radiometers in Validating the Visible through Shortwave Infrared Calibrations of Radiance Sources Used by Instruments in NASA's Earth Observing System

The detection and study of climate change over a time frame of decades requires successive generations of satellite, airborne, and ground-based instrumentation carefully calibrated against a common radiance scale. In NASA s Earth Observing System (EOS) program, the pre-launch radiometric calibration of these instruments in the wavelength region from 400 nm to 2500 nm is accomplished using internally illuminated integrating spheres and diffuse reflectance panels illuminated by irradiance standard lamps. Since 1995, the EOS Calibration Program operating within the EOS Project Science Office (PSO) has enlisted the expertise of national standards laboratories and government and university metrology laboratories in an effort to validate the radiance scales assigned to sphere and panel radiance sources by EOS instrument calibration facilities. This state-of-the-art program has been accomplished using ultra-stable transfer radiometers independently calibrated by the above participating institutions. In ten comparisons since February 1995, the agreement between the radiance measurements of the transfer radiometers is plus or minus 1.80% at 411 nm, plus or minus 1.31% at 552.5 nm, plus or minus 1.32% at 868.0 nm, plus or minus 2.54% at 1622nm, and plus or minus 2.81% at 2200nm (sigma =1).

Butler, James J.↗
DOE OSTI2026

Strong Lensing Cosmology with Population-level Calibrated Neural Ratio Estimation

Strong gravitational lensing contains key information about cosmic acceleration. Modern and next-generation galaxy imaging surveys are expected to provide high-quality data on $\mathcal{O}(10^5)$ galaxy-galaxy lensing systems. The plethora and complexity of the data are likely to present computational challenges for parameter inference methods for fitting high-dimensional likelihoods, which are often analytically intractable. Neural Ratio Estimation (NRE) efficiently computes individual likelihood ratios that can be combined into population-level posteriors. We use simulations to study the capacity of NRE to jointly predict the dark energy equation-of-state parameter $w$ and the total matter density $Ω_{m}$ from lensing images and companion spectroscopic information. We also introduce a post hoc posterior coverage calibration procedure that mitigates the model overconfidence that is typically found in neural density estimation applications. Our experiments show that the errors on both parameters decrease with increasing inference population sizes. In particular, for 100 lenses in a standard $Λ$CDM Universe, our calibrated NRE model achieves median fractional uncertainty of $22.8\%$ in $w$ and $2.9\%$ in $Ω_{m}$. This proof of concept demonstrates a potentially scalable approach for efficient cosmological parameter inference with large populations of galaxy-scale lenses observed in future surveys.

Jarugula, Sreevani [Fermilab] (ORCID:0000000253867↗
NASA NTRS1993

Wavelength dependence of limb-darkening of Mars from visible and near-IR telescopic spectral imaging

We are investigating the photometric properties of Mars using Earthbased telescopic spectral imaging obtained during 1988. Each spatial pixel consists of 300 spectral channels from 0.44 to 1.02 microns, calibrated to radiance factor (r(sub F)) through a careful procedure involving standard star observations in 1988 and 1990. Calibrated data include 3 spectral images with solar phase angle (g) of 12 degrees and 4 images with g of 4 degrees. Pixels near the sub-Earth point have a spatial footprint of about 280 x 150 km. Preliminary work using Hapke photometric function reveals a dependence of both single-scattering albedo and roughness parameter on wavelength. The former is in agreement with observed spectra of the martian surface, but the latter is unexpected.

Pierazzo, E.↗
DOE OSTI2020

Specifying Calibration of Environmental Sensors

The emergence of the Internet of Things is resulting in an increased ability of devices and systems to share data and is generating increasing interest in integrating sensors into a variety of devices deployed in the built environment. The value of such data is a function of how the data can be used. Data-producing devices and systems that enable valuable use-cases in turn can be seen as more valuable. Lighting systems are particularly interesting platforms for integrated sensors. Both indoor and outdoor lighting devices are becoming more connected, and their location is often ideally suited for hosting environmental sensors that can characterize the properties of indoor or outdoor spaces in ways that support a wide variety of use cases, from improving air quality to supporting fault diagnostics and prediction. The value of environmental-sensor-driven use-cases and the lighting systems that house them is dependent to some degree on sensor accuracy. Environmental sensors utilize a wide variety of sensing techniques or technologies and have varying accuracy. More-accurate, laboratory-grade products or reference standards are often used to characterize, refine, calibrate, adjust, and monitor devices that are deployed, or are intended to be deployed, in physical spaces of interest. Sensors or reference standards need to be calibrated periodically to ensure that their use yields accurate measurements. Calibration needs, however, vary in sophistication, based on user and use-case requirements. This paper provides guidance for evaluating the performance of environmental sensors so as to ensure that they meet user or use-case needs. It describes best practices that have been developed for a) calibrating sensors to ensure some known level of accuracy, and b) determining whether calibration-laboratory accreditation meets user or use-case needs. Excerpts from laboratory scopes of accreditation are shared to reveal the diversity of terminology and format among them. In an effort to aid those who currently have sensors calibrated or who have new or changing needs for sensor calibration, rationale is provided for why a specification might be used to request calibration services that meet specific needs. Commercially available calibration-service providers that are accredited for environmental-sensor calibration are compared and contrasted, and a specification template that might be used for requesting this calibration is presented. The specification template should be tailored to meet each user’s needs. To illustrate, an example set of environmental-sensor test conditions (reflecting the planned usage of the device to be calibrated) is used to develop a customized calibration specification, and commercially available service providers are assessed in terms of their qualifications for calibration to that particular implementation of the specification template.

42 ENGINEERING↗
DOE OSTI2013

NREL Pyrheliometer Comparison: September 16 to 27, 2013 (NPC-2013)

Accurate measurements of direct normal (beam) solar irradiance from pyrheliometers are important for the development and deployment of solar energy conversion systems, improving our understanding of the Earth's energy budget for climate change studies, and for other science and technology applications involving solar flux. Providing these measurements places many demands on the quality system used by the operator of commercially available radiometers. Maintaining accurate radiometer calibrations traceable to an international standard is the first step in producing research-quality solar irradiance measurements. As with all measurement systems, absolute cavity radiometers and other types of pyrheliometers are subject to performance changes over time. NREL has developed and maintained a group of absolute cavity radiometers with direct calibration traceability to the World Radiometric Reference (WRR). These reference instruments are used by NREL to calibrate pyrheliometers and pyranometers using the ISO 17025 accredited Broadband Outdoor Radiometer Calibration (BORCAL) process (Reda et al. 2008). NPCs are held annually at the Solar Radiation Research Laboratory (SRRL) in Golden, Colorado. Open to all pyrheliometer owners/operators, e.g. NREL, NASA, NIST, NOAA, USA industry and academia, USA-DOE and other national laboratories, and national and international organizations. Each NPC provides an opportunity to determine the unique World Radiometric Reference (WRR) transfer factor (WRR-TF) for each participating pyrheliometer. By adjusting all subsequent pyrheliometer measurements by the appropriate WRR-TF, the solar irradiance data are traceable to the International System of Units through WRR.

14 SOLAR ENERGY↗
NASA NTRS1971

Absolute ultraviolet spectrophotometry of: alpha CMa, gamma Ori, kappa Ori, and alpha Leo; and a continuing calibration program and some preliminary results

Spectral observations of the stars alpha CMa, gamma Ori, kappa Ori, and alpha Leo have been obtained in the range 1150 to 4000 Angstroms, using rocket borne spectrometers. The payloads have a 13-inch diameter telescope, a rotatable concave diffraction grating, and three pulse counting photomultiplier photometers. The laboratory standards used as photometric references derive their primary calibration directly or indirectly from the National Bureau of Standards. An error range of up to + or - 10 percent is attributed to these laboratory standards; + or - 8 percent to the calibration procedure; and + or - 10 percent is assigned as an accidental error range.

Evans, D. C.↗