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At least 811 records · Page 45

Accounting For Compressibility In Viscous Flow In Pipes

Method developed to account for effects of compressibility in viscous flows through long, circular pipes of uniform diameter. Based on approximation of variations in density and velocity across pipe cross section by profile equations developed for boundary-layer flow between flat plates.

Steinle, Frank W.↗

A visual study of radial inward choked flow of liquid nitrogen

A visual study of the radial inward choked flow of liquid nitrogen was conducted. Data and high speed moving pictures were obtained. The study indicated the following: (1) steady radial inward choked flow seems equivalent to steady choked flow through axisymmetric nozzles, (2) transient choked flows through the radial gap are not uniform and the discharge pattern appears as nonuniform impinging jets, and (3) the critical mass flow rate data for the transient case appear different from those of the steady case.

Hendricks, R. C.↗

Weakly Magnetized, Hall Dominated Plasma Couette Flow

A novel plasma equilibrium in the high-β, Hall regime that produces centrally peaked, high Mach number Couette flow is described. Flow is driven using a weak, uniform magnetic field and large, cross field currents. Large magnetic field amplification (factor 20) due to the Hall effect is observed when electrons are flowing radially inward, and near perfect field expulsion is observed when the flow is reversed. In conclusion, a dynamic equilibrium is reached between the amplified (removed) field and extended density gradients.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Weakly Magnetized, Hall Dominated Plasma Couette Flow

A novel plasma equilibrium in the high-β, Hall regime that produces centrally-peaked, high Mach number Couette flow is described. Flow is driven using a weak, uniform magnetic field and large, cross field currents. Large magnetic field amplification (factor 20) due to the Hall effect is observed when electrons are flowing radially inward, and near perfect field expulsion is observed when the flow is reversed. A dynamic equilibrium is reached between the amplified (removed) field and extended density gradients.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Computational And Experimental Studies Of Three-Dimensional Flame Spread Over Liquid Fuel Pools

Schiller, Ross, and Sirignano (1996) studied ignition and flame spread above liquid fuels initially below the flashpoint temperature by using a two-dimensional computational fluid dynamics code that solves the coupled equations of both the gas and the liquid phases. Pulsating flame spread was attributed to the establishment of a gas-phase recirculation cell that forms just ahead of the flame leading edge because of the opposing effect of buoyancy-driven flow in the gas phase and the thermocapillary-driven flow in the liquid phase. Schiller and Sirignano (1996) extended the same study to include flame spread with forced opposed flow in the gas phase. A transitional flow velocity was found above which an originally uniform spreading flame pulsates. The same type of gas-phase recirculation cell caused by the combination of forced opposed flow, buoyancy-driven flow, and thermocapillary-driven concurrent flow was responsible for the pulsating flame spread. Ross and Miller (1998) and Miller and Ross (1998) performed experimental work that corroborates the computational findings of Schiller, Ross, and Sirignano (1996) and Schiller and Sirignano (1996). Cai, Liu, and Sirignano (2002) developed a more comprehensive three-dimensional model and computer code for the flame spread problem. Many improvements in modeling and numerical algorithms were incorporated in the three-dimensional model. Pools of finite width and length were studied in air channels of prescribed height and width. Significant three-dimensional effects around and along the pool edge were observed. The same three-dimensional code is used to study the detailed effects of pool depth, pool width, opposed air flow velocity, and different levels of air oxygen concentration (Cai, Liu, and Sirignano, 2003). Significant three-dimensional effects showing an unsteady wavy flame front for cases of wide pool width are found for the first time in computation, after being noted previously by experimental observers (Ross and Miller, 1999). Regions of uniform and pulsating flame spread are mapped for the flow conditions of pool depth, opposed flow velocity, initial pool temperature, and air oxygen concentration under both normal and microgravity conditions. Details can be found in Cai et al. (2002, 2003). Experimental results recently performed at NASA Glenn of flame spread across a wide, shallow pool as a function of liquid temperature are also presented here.

Ross, Howard D.↗

Laser Doppler velocity measurements of swirling flows with upstream influence

Swirling flow in a rotating tube is studied by flow visualization at a moderate Reynolds number, and its velocity field is measured by laser-Doppler anemometry. The tube has constant diameter, and approximately uniform initial rigid rotation of the flow is assured by passing the flow through a rotating plug of porous metal before it enters the test section. At moderate swirl values, an object mounted on the tube centerline causes a closed bubble to form upstream of the obstacle, with a clearly defined stagnation point on the axis, and recirculating flow inside the bubble. The bubble length grows upstream as the swirl is increased, until it breaks up into a Taylor column reaching all the way upstream and downstream at swirl values above a certain critical value. A vortex jump (in the sense of Benjamin) occurs downstream of the obstacle except when the Taylor column is present. Using a laser-Doppler anemometer, axial and swirl velocity profiles are obtained at several stations upstream and downstream of the bubble, and in and around the bubble.

Rloff, K. L.↗

High-capacity rotary drum for atomic layer deposition onto powders and small mechanical parts in a hot-walled viscous flow reactor

Atomic layer deposition (ALD) is uniquely capable of providing uniform thin-film coatings on powder substrates, but powder processing has historically required an ALD reactor designed specifically for powders-e.g., a fluidized bed. Tubular hot-walled viscous-flow reactors commonly employed in laboratory-scale ALD research for coating planar substrates such as silicon have been employed previously to coat gram quantities of powder spread out in a thin layer on a tray, but larger quantities of powder introduce long diffusion pathways where reactants are unable to percolate to the bottom of the powder bed to provide uniform coating in reasonable time periods. In this work, we report a rotary drum with a capacity of 100s of grams that is compatible with conventional tubular hot-walled ALD reactors and provides uniform coatings on powders in viscous flow operation. We benchmark this system using Al 2 O 3 ALD with trimethylaluminum and water. We examine the effect of rotation speed and powder quantity on saturation time via in situ quadrupole mass spectroscopy measurements and gravimetric analysis. Finally, the rotary drum we report is able to provide homogenous coating of up to 75g of silica gel powder with a total surface area of similar to 1500m 2 in viscous flow operation with precursor utilization as high as 70%.

47 OTHER INSTRUMENTATION↗

Analysis of coolant entrance boundary shape of porous region to control cooling along exit boundary

A cooled porous region has a plane surface exposed to a specified spatially varying heat flux. The coolant leaves the region through this surface, and it is desired to control the flow distribution to maintain a specified uniform surface temperature. This is accomplished by having the coolant entrance surface shaped to provide in the region the necessary variation of path length and, hence, flow resistance. The surface shape at the coolant entrance is found by solving a Cauchy boundary value problem. An exact solution is obtained that will deal with a wide variety of heating distributions for both two- and three-dimensional shapes.

Siegel, R.↗

Miniature Arcs for Synthesis of Carbon Nanotubes in Microgravity

Although many methods are available for producing single-walled carbon nanotubes (SWNTs), the conventional carbon arc process remains the most popular due to its simplicity and large production rate. In the carbon arc, SWNTs are catalytically synthesized by rapidly evaporating a graphite anode impregnated with NiN metal catalyst from which the nanotubes grow in an inert atmosphere. However, high temperatures inside the carbon arc generate strong buoyancy driven convection, and it is hypothesized that the non-uniform environment created by this flow has a large effect on the growth and morphology of the SWNTs. To study the effect of buoyancy on the arc process, a miniature carbon arc apparatus was developed to synthesize SWNTs in a microgravity environment substantially free from these strong convective flows. The reactor was operated for either 2.2 or 5 seconds during free-fall in the drop towers at the NASA Glenn Research Center. Two apparatus designs differing mainly in their production rate and power capacity were investigated. The first consisted of a miniaturized carbon arc employing a 1 mm diameter graphite anode and powered by a 0.54 F capacitor bank charged to 65 V. The second, larger apparatus employed a 4 mm diameter anode and was powered by a portable battery pack capable of providing in excess of 300 amps at 30 volts to the arc for the duration of a 5 second drop. Initial results indicated that transient heating is a very large effect in the short-duration drop tower carbon arcs, and thermal equilibrium of the arc plasma, buffer gas, and apparatus was not attained during the short microgravity periods. In addition, removal of the buoyant convection by the microgravity now allowed clear observation of large jets of evaporated carbon vapor streaming from the anode and mixing with the inert buffer gas. The initial mixing of these jets with the cold buffer gas combined with the thermal transient made it difficult to establish a uniform high temperature environment around the arc in the 2.1 to 5 second microgravity time interval, and even with a very high-powered arc, the arc region was cooler than in continuously operated arcs. Despite these difficulties, the miniature arc produced SWNTs in microgravity. However, given the large thermal transient to overcome, no dramatic difference in sample yield or composition was noted between normal gravity and q2-,andL%econd long microgravity runs.

Alford, J. M.↗

Laminar free convection over two-dimensional bodies with uniform surface heat flux

A general analysis is presented of the steady nondissipative constant-property laminar boundary layer flow over a two-dimensional body of uniform surface heat flux situated in an infinite ambient fluid of undisturbed temperature. The analysis is then applied to a long horizontal circular cylinder. Numerical solutions to the universal functions associated with the first two terms in the derived series are given for Prandtl numbers 0.7, 1, 3, 5, 7, and 10. The results are compared with those obtained by Koh (1964) whose method is patterned after the Blasius-Frossling procedure for forced convection flow. The study reveals that Wilks' (1972) analysis concerning the external natural convection about two-dimensional bodies with constant heat flux is in error.

Lin, F. N.↗

Impact of Porous Transport Layer In-Plane Conduction on Spatially Resolved Current and EIS Measurements in a Proton Exchange Membrane Water Electrolyzer

An XY segmented cell was developed for low temperature PEM water electrolysis (PEMWE). The system can assess the local performance by enabling in situ measurements of spatial currents and impedances. In this work, we show through experiments, as well as through modelling work, that the porous transport layer (PTL) must be segmented to eliminate crosstalk. Accurate measurements are only possible when crosstalk is fully eliminated. The XY segmented cell is applied to a case study characterizing the impact of a PTL platinum coating void on spatial performance. The localized performance impact of the coating void is found to be orientation specific: coating voids facing the catalyst layer reduce performance significantly more than coating voids facing the flow field. The results suggest that the tolerances for PTL coating uniformity can be lower at the side facing the flow field. The work showcases the feasibility of the XY segmented cell for impact assessment studies. The presented XY segmented cell enables the characterization of spatial phenomena in PEMWE devices and is envisioned to support modeling efforts and the investigation of manufacturing related tolerances for mass produced PEMWE devices.

08 HYDROGEN↗

Nonthermal plasma synthesis of silicon carbonitride

Abstract The use of a low‐temperature plasma for the synthesis of amorphous silicon carbonitride (SiCN) nanoparticles enables the realization of sintered bulk samples with high thermal stability. Amorphous SiCN nanoparticles are produced from a mixture of silane, methane, and ammonia utilizing a mid‐pressure, radio‐frequency, continuous flow reactor. Particle characterization shows that the nanoparticles are largely amorphous with some crystalline silicon and silicon carbide domains <10 nm in size. Compositional tuning, controlled by varying the precursor flow rates, coupled with the uniform mixing of elements at the nanoscale, results in samples that resist crystallization even when sintered at temperatures as high as 2000°C. This study suggests that the low‐temperature plasma synthesis of nanoparticles has great potential to produce bulk structural materials for application in harsh environments.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Nondestructive neutron imaging diagnosis of acidic gas reduction catalyst after 400-Hour operation in natural gas furnace

Residential natural gas furnaces are the primary space-heating devices in US homes, leading to substantial environmental impact caused by the acidic components in the furnace combustion gases. Here, to experimentally demonstrate acidic gas reduction in a furnace, a monolithic catalyst was fabricated and was called the AGR. A commercially-available condensing furnace was retrofitted with the AGR, and a 400-hour reliability and durability test was conducted. The results showed that the AGR significantly reduced acidic gases in the flue gas and produced condensate with neutral pH. Challenges were also revealed: inappropriate condensate drainage caused incomplete combustion and amorphous carbon deposits. To nondestructively survey the internal state of the AGR, neutron computed tomography (NCT) was employed to produce spatially resolved 2D and 3D representations of the 2-L, aged AGR component. The NCT results confirm the integrity of the AGR component, which consists of two blocks, without deformation or damage to AGR channels. The distribution of the particle accumulation in the middle of the top block was visibly heavier than the entrance and exit of the top block. The representative cross-section views revealed significant aggregation in the central region but not at the rim. The spatially resolved details provide in-depth diagnosis, evaluation, and understanding of the AGR. The insights can enable new AGR designs that realize a uniform and self-cleaning flow pattern, alleviate significant particle aggregation, and thus enhance AGR-enabled furnace performance. The neutron imaging method demonstrates the good potential that can diagnose faults and improve the design, optimization, and production processes of novel catalysts and other components or systems with heavy metal shell.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Thermal volatilization studies on lunar samples.

The results of thermal volatilization studies on lunar basalts, breccias, and soils, carried out to measure the depletion of selected elemental abundances during heating under vacuum, are evaluated. The kinetics of K, Rb, and Pb loss are found to be sufficiently fast to permit vaporization and loss of these elements during the production of impact glasses. There is little probability that lunar basalt flows have lost a significant percentage of K, Rb, and Na by volatilization, unless the flow is extensively stirred. The uniformly low Na concentrations of mare basalts cannot be attributed to post eruption vaporization and loss on Na.

Gibson, E. K., Jr.↗

The influence of wind shear on aerodynamic coefficients

The purpose of this study is to investigate the influence of wind shear on the lift, drag, roll and yaw moments of a wing in a horizontal wind gradient at various elevations and roll angles. The models of wind shear considered are those proposed by Leurs (1973) for atmospheric flow over horizontally homogeneous and uniform terrain. A general series solution for the distribution of lift along the wing span following the method of Houghton and Brock (1970) is employed to compute the loads and moments on the airfoil. Results of the computations indicate that wind shear can have a significant effect on the rolling and yawing moments of the wing of an aircraft flying with one wing low in the atmospheric boundary layer. These moments are directly influenced by the magnitude of the wind gradient in the neutral atmosphere reflected by the magnitude of the friction velocity. The effect of wind shear on lift and drag is negligible. Stability of the atmosphere tends to increase the magnitude of the rolling moment while decreasing its variation with elevation.

Frost, W.↗

First results from the six-axis electron spectrometer on ISEE-1

A survey, using results from the first 25 orbits of ISEE-1, was made of some aspects of electrons in the dawn magnetosheath. There are indications that the flow of plasma is not uniformly turbulent over this region. The electron heat flux is observed to be directed away from the shock and to have an average value of about twice the interplanetary heat flux. Many magnetopause crossings were observed and usually resemble abrupt transitions from one well-defined plasma state to another. The ejection of plasma from flux tubes convected up against the magnetopause is observed for about half the time, and its thickness and dependance on the solar wind Mach number agrees with theoretical predictions. A full traversal of the whole forward hemisphere of the magnetosheath is required to fully confirm these deductions.

Ogilvie, K. W.↗

Chemical vapor deposition reactor

An improved chemical vapor deposition reactor is characterized by a vapor deposition chamber configured to substantially eliminate non-uniformities in films deposited on substrates by control of gas flow and removing gas phase reaction materials from the chamber. Uniformity in the thickness of films is produced by having reactive gases injected through multiple jets which are placed at uniformally distributed locations. Gas phase reaction materials are removed through an exhaust chimney which is positioned above the centrally located, heated pad or platform on which substrates are placed. A baffle is situated above the heated platform below the mouth of the chimney to prevent downdraft dispersion and scattering of gas phase reactant materials.

Chern, S. S.↗

First results from the six-axis electron spectrometer on ISEE-1

A survey, using results from the first 25 orbits of ISEE-1, has been made of some aspects of electrons in the dawn magnetosheath. There are indications that the flow of plasma is not uniformly turbulent over this region. The electron heat flux is observed to be directed away from the shock and to have an average value of about twice the interplanetary heat flux. Many magnetopause crossings were observed and usually resemble abrupt transitions from one well-defined plasma state to another. The ejection of plasma from flux tubes convected up against the magnetopause is observed for about half the time, and its thickness and dependence on the solar wind Mach number agree with theoretical predictions. A full traversal of the whole forward hemisphere of the magnetosheath is required to fully confirm these deductions

Ogilvie, K. W.↗