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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 811 records · Page 45
All sourcesNASA NTRSDOE OSTI
DOE OSTI2022

Time-dependent dynamical Bragg diffraction in deformed crystals by the beam propagation method

Herein, this paper describes how to efficiently solve time-dependent X-ray dynamic diffraction problems in distorted crystals with a fast Fourier transform based beam propagation method. Examples are given of using the technique to simulate the propagation of X-ray beams in deformed crystals in space and time domains relevant to the cavity-based X-ray free-electron lasers and X-ray free-electron laser self-seeding systems.

36 MATERIALS SCIENCE↗
DOE OSTI2021

Electronic and optical properties of Zn-doped β-Ga 2 O 3 Czochralski single crystals

β-Ga 2 O 3 has several soluble deep acceptors that impart insulating behavior. In this study, we investigate Zn doping (0.25at.%) in bulk Czochralski and vertical gradient freeze β-Ga 2 O 3 . Representative crystals were assessed for orientation (electron backscatter diffraction and Raman spectroscopy), purity (glow discharge mass spectrometry and secondary ion mass spectrometry), optical properties (ultraviolet to near infrared absorption), and electrical properties (resistivity and current–voltage). Purity measurements indicate that Zn evaporation is insufficient to inhibit doping of Zn into β-Ga 2 O 3 . Hybrid functional calculations show Zn substitutes nearly equally on tetrahedral and octahedral sites, with less than ~0.1eV preference for the octahedral (Ga II ) site. Furthermore, calculations show that Zn Ga acts as a deep acceptor with trapping levels ~1.3 and ~0.9eV above the valence band for one and two holes, respectively. The solubility and electronic behavior of Zn dopants are consistent with measured concentrations >1×10 18 atoms/cm 3 and electrical measurements that show resistivity 10 11 –10 13 Ωcm, with no p-type conduction.

36 MATERIALS SCIENCE↗
DOE OSTI2024

Photochemically induced acousto-optics in gases

Acousto-optics consists of launching acoustic waves in a medium (usually a crystal) in order to modulate its refractive index and create a tunable optical grating. Here, in this article, we present the theoretical basis of an alternative scheme to generate acousto-optics in a gas, where the acoustic waves are initiated by the localized absorption (and thus gas heating) of spatially modulated UV light, as was demonstrated by Michine and Yoneda [Commun. Phys. 3, 24 (2020)]. We identify the chemical reactions initiated by the absorption of UV light via the photodissociation of ozone molecules present in the gas, and calculate the resulting temperature increase in the gas as a function of space and time. Solving the Euler fluid equations shows that the modulated, isochoric heating initiates a mixed acoustic-entropy wave in the gas, whose high-amplitude density (and thus refractive index) modulation can be used to manipulate a high-power laser. We calculate that diffraction efficiencies near 100% can be obtained using only a few millimeters of gas containing a few percent ozone fraction at room temperature, with UV fluences of less than 100 mJ/cm 2 —consistent with the experimental measurements. Our analysis suggests possible ways to optimize the diffraction efficiency by changing the buffer gas composition. Gases have optics damage thresholds 2–3 orders of magnitude beyond those of solids; these optical elements should therefore be able to manipulate kilojoule-class lasers.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
NASA NTRS1981

E-beam generated holographic masks for optical vector-matrix multiplication

An optical vector matrix multiplication scheme that encodes the matrix elements as a holographic mask consisting of linear diffraction gratings is proposed. The binary, chrome on glass masks are fabricated by e-beam lithography. This approach results in a fairly simple optical system that promises both large numerical range and high accuracy. A partitioned computer generated hologram mask was fabricated and tested. This hologram was diagonally separated outputs, compact facets and symmetry about the axis. The resultant diffraction pattern at the output plane is shown. Since the grating fringes are written at 45 deg relative to the facet boundaries, the many on-axis sidelobes from each output are seen to be diagonally separated from the adjacent output signals.

Arnold, S. M.↗
NASA NTRS1988

Amorphous silicon carbide coatings for extreme ultraviolet optics

Amorphous silicon carbide films formed by sputtering techniques are shown to have high reflectance in the extreme ultraviolet spectral region. X-ray scattering verifies that the atomic arrangements in these films are amorphous, while Auger electron spectroscopy and Rutherford backscattering spectroscopy show that the films have composition close to stoichiometric SiC, although slightly C-rich, with low impurity levels. Reflectance vs incidence angle measurements from 24 to 1216 A were used to derive optical constants of this material, which are presented here. Additionally, the measured extreme ultraviolet efficiency of a diffraction grating overcoated with sputtered amorphous silicon carbide is presented, demonstrating the feasibility of using these films as coatings for EUV optics.

Kortright, J. B.↗
DOE OSTI2021

Anisotropic Transient Disordering of Colloidal, Two-Dimensional CdSe Nanoplatelets upon Optical Excitation

Nanoplatelets (NPLs)-colloidally synthesized, spatially anisotropic, two-dimensional semiconductor quantum wells-are of intense interest owing to exceptionally narrow transition line widths, coupled with solution processability and bandgap tunability. However, given large surface areas and undercoordinated bonding at facet corners and edges, excitation under sufficient intensities may induce anisotropic structural instabilities that impact desired properties. We employ time-resolved X-ray diffraction to study the crystal structure of CdSe NPLs in response to optical excitation. Photoexcitation induces greater out-of-plane than in-plane disordering in 4 and 5 monolayer (ML) NPLs, while 3 ML NPLs display the opposite behavior. Recovery dynamics suggest that out-of-plane cooling slightly outpaces in-plane cooling in 5 ML NPLs with recrystallization occurring on indistinguishable time scales. In comparison, for zero-dimensional CdSe nanocrystals, disordering is isotropic and recovery is faster. These results favor the use of NPLs in optoelectronic applications, where they are likely to exhibit superior performance over traditional, zero-dimensional nanocrystals.

77 NANOSCIENCE AND NANOTECHNOLOGY↗
DOE OSTI2021

Diamond channel-cut crystals for high-heat-load beam-multiplexing narrow-band X-ray monochromators

Next-generation high-brilliance X-ray photon sources call for new X-ray optics. Here we demonstrate the possibility of using monolithic diamond channel-cut crystals as high-heat-load beam-multiplexing narrow-band mechanically stable X-ray monochromators with high-power X-ray beams at cutting-edge high-repetition-rate X-ray free-electron laser (XFEL) facilities. The diamond channel-cut crystals fabricated and characterized in these studies are designed as two-bounce Bragg reflection monochromators directing 14.4 or 12.4 keV X-rays within a 15 meV bandwidth to 57 Fe or 45 Sc nuclear resonant scattering experiments, respectively. The crystal design allows out-of-band X-rays transmitted with minimal losses to alternative simultaneous experiments. Only ≲2% of the incident ∼100 W X-ray beam is absorbed in the 50 µm-thick first diamond crystal reflector, ensuring that the monochromator crystal is highly stable. Other X-ray optics applications of diamond channel-cut crystals are anticipated.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗
NASA NTRS1997

Construction of Prototype Lightweight Mirrors

This contract and the work described was in support of a Seven Segment Demonstrator (SSD) and demonstration of a different technology for construction of lightweight mirrors. The objectives of the SSD were to demonstrate functionality and performance of a seven segment prototype array of hexagonal mirrors and supporting electromechanical components which address design issues critical to space optics deployed in large space based telescopes for astronomy and for optics used in spaced based optical communications systems. The SSD was intended to demonstrate technologies which can support the following capabilities; Transportation in dense packaging to existing launcher payload envelopes, then deployable on orbit to form space telescope with large aperture. Provide very large (less than 10 meters) primary reflectors of low mass and cost. Demonstrate the capability to form a segmented primary or quaternary mirror into a quasi-continuous surface with individual subapertures phased so that near diffraction limited imaging in the visible wavelength region is achieved. Continuous compensation of optical wavefront due to perturbations caused by imperfections, natural disturbances, and equipment induced vibrations/deflections to provide near diffraction limited imaging performance in the visible wavelength region. Demonstrate the feasibility of fabricating such systems with reduced mass and cost compared to past approaches. While the SSD could not be expected to satisfy all of the above capabilities, the intent was to start identifying and understanding new technologies that might be applicable to these goals.

Robinson, William G.↗
DOE OSTI2022

To what extent can space be compressed? Bandwidth limits of spaceplates

Spaceplates are novel flat-optic devices that implement the optical response of a free-space volume over a smaller length, effectively “compressing space” for light propagation. Together with flat lenses such as metalenses or diffractive lenses, spaceplates have the potential to enable the miniaturization of any free-space optical system. While the fundamental and practical bounds on the performance metrics of flat lenses have been well studied in recent years, a similar understanding of the ultimate limits of spaceplates is lacking, especially regarding the issue of bandwidth, which remains as a crucial roadblock for the adoption of this platform. In this work, we derive fundamental bounds on the bandwidth of spaceplates as a function of their numerical aperture and compression ratio (ratio by which the free-space pathway is compressed). The general form of these bounds is universal and can be applied and specialized for different broad classes of space-compression devices, regardless of their particular implementation. Our findings also offer relevant insights into the physical mechanism at the origin of generic space-compression effects and may guide the design of higher performance spaceplates, opening new opportunities for ultra-compact, monolithic, planar optical systems for a variety of applications.

Shastri, Kunal (ORCID:0000000169282753)↗
NASA NTRS1997

Adaptive Full Aperture Wavefront Sensor Study

This grant and the work described was in support of a Seven Segment Demonstrator (SSD) and review of wavefront sensing techniques proposed by the Government and Contractors for the Next Generation Space Telescope (NGST) Program. A team developed the SSD concept. For completeness, some of the information included in this report has also been included in the final report of a follow-on contract (H-27657D) entitled "Construction of Prototype Lightweight Mirrors". The original purpose of this GTRI study was to investigate how various wavefront sensing techniques might be most effectively employed with large (greater than 10 meter) aperture space based telescopes used for commercial and scientific purposes. However, due to changes in the scope of the work performed on this grant and in light of the initial studies completed for the NGST program, only a portion of this report addresses wavefront sensing techniques. The wavefront sensing techniques proposed by the Government and Contractors for the NGST were summarized in proposals and briefing materials developed by three study teams including NASA Goddard Space Flight Center, TRW, and Lockheed-Martin. In this report, GTRI reviews these approaches and makes recommendations concerning the approaches. The objectives of the SSD were to demonstrate functionality and performance of a seven segment prototype array of hexagonal mirrors and supporting electromechanical components which address design issues critical to space optics deployed in large space based telescopes for astronomy and for optics used in spaced based optical communications systems. The SSD was intended to demonstrate technologies which can support the following capabilities: Transportation in dense packaging to existing launcher payload envelopes, then deployable on orbit to form a space telescope with large aperture. Provide very large (greater than 10 meters) primary reflectors of low mass and cost. Demonstrate the capability to form a segmented primary or quaternary mirror into a quasi-continuous surface with individual subapertures phased so that near diffraction limited imaging in the visible wavelength region is achieved. Continuous compensation of optical wavefront due to perturbations caused by imperfections, natural disturbances, and equipment induced vibrations/deflections to provide near diffraction limited imaging performance in the visible wavelength region. Demonstrate the feasibility of fabricating such systems with reduced mass and cost compared to past approaches.

Robinson, William G.↗
DOE OSTI2022

Laser-induced patterning for a diffraction grating using the phase change material of Ge 2 Sb 2 Te 5 (GST) as a spatial light modulator in X-ray optics: a proof of concept

The proposed X-ray spatial light modulator (SLM) concept is based on the difference of X-ray scattering from amorphous and crystalline regions of phase change materials (PCMs) such as Ge 2 Sb 2 Te 5 (GST). In our X-ray SLM design, the “ on” and “ off” states correspond to a patterned and homogeneous state of a GST thin film, respectively. The patterned state is obtained by exposing the homogeneous film to laser pulses. In this paper, we present patterning results in GST thin films characterized by microwave impedance microscopy and X-ray small-angle scattering at the Stanford Synchrotron Radiation Lightsource.

36 MATERIALS SCIENCE↗
NASA NTRS2008

Compact Two-Dimensional Spectrometer Optics

The figure is a simplified depiction of a proposed spectrometer optical unit that would be suitable for incorporation into a remote-sensing instrumentation system. Relative to prior spectrometer optical assemblies, this unit would be compact and simple, largely by virtue of its predominantly two-dimensional character. The proposed unit would be a combination of two optical components. One component would be an arrayed-waveguide grating (AWG) an integrated-optics device, developed for use in wavelength multiplexing in telecommunications. The other component would be a diffraction grating superimposed on part of the AWG. The function of an AWG is conceptually simple. Input light propagates along a single-mode optical waveguide to a point where it is split to propagate along some number (N) of side-by-side waveguides. The lengths of the optical paths along these waveguides differ such that, considering the paths in a sequence proceeding across the array of waveguides, the path length increases linearly. These waveguides launch quasi-free-space waves into a planar waveguide-coupling region. The waves propagate through this region to interfere onto an array of output waveguides. Through proper choice of key design parameters (waveguide lengths, size and shape of the waveguide coupling region, and lateral distances between waveguides), one can cause the input light to be channeled into wavelength bins nominally corresponding to the output waveguides.

Hong, John↗
DOE OSTI2023

Second Target Station (STS) Project: PIONEER Technical Report

PIONEER is a time-of-flight single-crystal neutron diffractometer at the Second Target Station (STS), aiming at providing the world-leading capability to measure tiny crystals (~0.001 mm 3 , i.e., X-ray diffraction size), ultra-thin epitaxial films (~10 nm thicknesses), and weak structural transitions and complex magnetism. The instrument will take advantage of STS source characteristics and utilize advancements in neutron optics to largely reduce the sample-volume requirement for single-crystal neutron diffraction. PIONEER will have a high-flux mode with multiple beam size options to improve the signal-to-background ratio in various sample environments. It will also provide a high Q-resolution mode by limiting beam divergence to study periodically modulated structures with characteristic lengths no less than 100 Å. Furthermore, it supports half-polarized neutron diffraction for investigating complex magnetism and local susceptibility. This report first overviews the proposed science case and the derived requirement. And then, the chosen technical solutions and expected performance will be described.

36 MATERIALS SCIENCE↗
NASA NTRS2004

WaFIRS, a Waveguide Far-IR Spectrometer: Enabling Space-Borne Spectroscopy of High-z Galaxies in the Far-IR and Submm

The discovery of galaxies beyond z approximately equal to 1 which emit the bulk of their luminosity at long wavelengths has demonstrated the need for high sensitivity, broadband spectroscopy in the far-IR/submm/mm bands. Because many of these sources are not detectable in the optical, long wavelength spectroscopy is key to measuring their redshifts and ISM conditions. The continuum source list will increase in the next decade with new ground-based instruments (SCUBA2, Bolocam, MAMBO) and the surveys of HSO and SIRTF. Yet the planned spectroscopic capabilities lag behind, primarily due to the difficulty in scaling existing IR spectrograph designs to longer wavelengths. To overcome these limitations, we are developing WaFIRS, a novel concept for long-wavelength spectroscopy which utilizes a parallel-plate waveguide and a curved diffraction grating. WaFIRS provides the large (approximately 60%) instantaneous bandwidth and high throughput of a conventional grating system, but offers a dramatic reduction in volume and mass. WaFIRS requires no space overheads for extra optical elements beyond the diffraction grating itself, and is two-dimensional because the propagation is confined between two parallel plates. Thus several modules could be stacked to multiplex either spatially or in different frequency bands. The size and mass savings provide opportunities for spectroscopy from space-borne observatories which would be impractical with conventional spectrographs. With background-limited detectors and a cooled 3.5 telescope, the line sensitivity would be better than that of ALMA, with instantaneous broad-band coverage. We have built and tested a WaFIRS prototype for 1-1.6 mm, and are currently constructing Z-Spec, a 100 mK model to be used as a ground-based lambda/DELTAlambda approximately equal to 350 submillimeter galaxy redshift machine.

Bradford, C. M.↗
NASA NTRS1970

Discrete control of linear distributed systems with application to the deformable primary mirror of a large orbiting telescope

One of the more significant technological problems associated with the orbital operation of large astronomical telescope's is the fabrication and maintenance of the primary mirror surface to the tolerance required for diffraction-limited performance. An interesting approach to the solution of this problem involves continuously measuring and automatically correcting the optical surface of a thin deformable mirror by means of discrete actuators located on its rear surface: The realization of diffraction-limited performance from a telescope in space by this method rests on the ability of the designer to achieve extremely accurate control of a highly complex, interacting, multivariable system. This paper presents the results of a detailed study of the discrete control of linear distributed systems with specific application to the design of a practical controller for a plant representative of a telescope primary mirror for an orbiting astronomical observatory. The problem of controlling the distributed plant is treated by employing modal techniques to represent variations in the optical figure. Distortion of the mirror surface, which arises primarily from thermal gradients, is countered by actuators working against a backing structure to apply a corrective force distribution to the controlled surface. Each displacement actuator is in series with a spring attached to the mirror by means of a pad intentionally introduced to restrict the excitation of high-order modes. Control is then exerted over a finite number (equal.to the number of actuators) of the most significant modes. Through the application of the modal expansion technique the mirror equation of motion is transformed tb a set of uncoupled, linear, time-invariant, ordinary differential equations. The desired dynamic response and static accuracy may then be achieved by the application of classical single-variable design techniques. The formulation of a quadratic performance index which incorporates a measure of image quality permits determination of the trade-off between the-number of actuators and optical purity. A criterion for defining actuator placement and pad size is presented which minimizes the tendency of the controller to excite the unmonitored modes.

Jeremiah F Creedon↗
NASA NTRS2006

Electromagnetic Considerations for Planar Bolometer Arrays in the Single Mode Limit

Filled arrays of planar bolometers are finding astronomical applications at wavelengths as long as several millimeters. In an effort to keep focal planes to a reasonable size while maintaining large numbers of detectors, a common strategy is to push these arrays to operate close to or at the single mode limit. Doing so introduces several new challenges that are not experienced in the multi-mode case of far-infrared detectors having similar pixel sizes. First, diffractive effects of the pixels themselves are no longer insignificant and will ultimately contribute to the resolution limit of the optical system in which they reside. We use the method of Withlngton et al. (2003) to model the polarized diffraction in this limit. Second, it is necessary to re-examine the coupling between the radiation and the absorbing element that is thermally connected to the bolometers. The small f-numbers that are often employed to make use of large focal planes makes backshort construction problematic. We introduce a new strategy to increase detector efficiency that uses an antireflective layer on the front side of the detector array. In addition, typical methods for stray light control that rely on multiple reflections in a lossy medium fail due to physical size constraints. For this application, we find that resonant absorbers are a more effective strategy that can be implemented in the space available.

Wollack, Edward J.↗
DOE OSTI2023

Assessing Manufacturability of the Oxide Dispersion Strengthened (ODS) 14YWT Alloy Fuel Cladding Tube Using SolidStir™ Technology

The 14YWT (Fe–14Cr–3W–0.4Ti–0.3Y2O3 (wt.%)) alloy is a potential candidatematerial for fabricating fuel cladding tubes and other structural components to be used in next-generation advanced nuclear reactors. Due to inherent limitations of current processing routes, this research explored a new variant of friction stir processing, commercially referred to as SolidStir™ Extrusion (patent pending) technology from Enabled Engineering to consolidate and extrude 14YWT powder into a fuel cladding tube. Several single-layer and multiple-layer consolidation experiments were carried out in an Inconel 625 die to determine the suitable processing parameters for SolidStir™ extrusion of the 14YWT alloy cladding tube. With these processing parameters, a 16–18 mm long tube of the 14YWT alloy with no visible defects was successfully extruded using this novel technology. Microstructural characterization results obtained using optical microscopy, scanning electron microscopy, energy dispersive spectroscopy, electron backscatter diffraction, and transmission electron microscopy will be presented.

Advanced Materials and Manufacturing Technology↗